Improved proton decoupling in NMR spectroscopy of crystalline solids using the SPINAL-64 sequence
(2002)
Journal Article
Brauniger, T., Wormald, P., & Hodgkinson, P. (2002). Improved proton decoupling in NMR spectroscopy of crystalline solids using the SPINAL-64 sequence. Monatshefte für Chemie - Chemical Monthly, 133(12), 1549-1554
The performance of three different spin decoupling schemes, CW, TPPM, and SPINAL-64 is compared, by recording proton decoupled C-13 NMR spectra of a crystalline glycine sample, with 20% isotopic labelling. At a magnetic field of B-0 = 14.1 T, the two... Read More about Improved proton decoupling in NMR spectroscopy of crystalline solids using the SPINAL-64 sequence.