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Controlled Flow Precipitation as a Valuable Tool for Synthesis

Filipponi, Paolo; Gioiello, Antimo; Baxendale, Ian R.

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Authors

Paolo Filipponi

Antimo Gioiello



Abstract

In most standard flow process, the formation of solids represents a major problem often leading to obstruction of the flow device and reactor shutdown. However, many reactions produce solid products, and therefore finding ways to process these materials is an important area of research. In this article we demonstrate how a dynamically agitated flow reactor can be a powerful tool to facilitate workup and processing of biphasic solid–liquid flow streams at scale.

Journal Article Type Article
Acceptance Date Oct 17, 2015
Online Publication Date Nov 17, 2015
Publication Date Feb 19, 2016
Deposit Date Nov 20, 2015
Publicly Available Date Nov 17, 2016
Journal Organic Process Research and Development
Print ISSN 1083-6160
Electronic ISSN 1520-586X
Publisher American Chemical Society
Peer Reviewed Peer Reviewed
Volume 20
Issue 2
Pages 371-375
DOI https://doi.org/10.1021/acs.oprd.5b00331
Public URL https://durham-repository.worktribe.com/output/1397801

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Accepted Journal Article (740 Kb)
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Copyright Statement
This document is the Accepted Manuscript version of a Published Work that appeared in final form in Organic Process Research & Development, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://dx.doi.org/10.1021/acs.oprd.5b00331.





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