Kerry Strong k.a.strong@durham.ac.uk
Senior Technician (Biomarkers)
Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry
Strong, Kerry A.; Stokes, Peter; Parker, David; Buckley, Amy K.; Mosely, Jackie A.; Brodie, Claire N.; Dyer, Philip W.
Authors
Peter Stokes peter.stokes@durham.ac.uk
Mass Spectrometry Service Manager
David Parker david.parker@durham.ac.uk
Emeritus Professor
Amy K. Buckley
Jackie A. Mosely
Claire N. Brodie
Professor Philip Dyer p.w.dyer@durham.ac.uk
Professor
Abstract
A cheap, versatile, readily modified, and reusable glass probe system enabling delivery of solid air-/moisture-sensitive samples for mass spectrometric (MS) analysis using an Atmospheric pressure Solids Analysis Probe (ASAP) is described. The simplicity of the design allows quick and easy ASAP MS analyses of sensitive solid and liquid samples without the need for any modifications to commercially available vertically loaded ASAP mass spectrometers. A comparison of ASAP mass spectra obtained for metal complexes under air and an inert atmosphere is given.
Citation
Strong, K. A., Stokes, P., Parker, D., Buckley, A. K., Mosely, J. A., Brodie, C. N., & Dyer, P. W. (2022). Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry. Analytical Chemistry, 94(32), 11315-11320. https://doi.org/10.1021/acs.analchem.2c02039
Journal Article Type | Article |
---|---|
Acceptance Date | Jul 22, 2022 |
Online Publication Date | Aug 5, 2022 |
Publication Date | 2022 |
Deposit Date | Aug 19, 2022 |
Publicly Available Date | Aug 19, 2022 |
Journal | Analytical Chemistry |
Print ISSN | 0003-2700 |
Electronic ISSN | 1520-6882 |
Publisher | American Chemical Society |
Peer Reviewed | Peer Reviewed |
Volume | 94 |
Issue | 32 |
Pages | 11315-11320 |
DOI | https://doi.org/10.1021/acs.analchem.2c02039 |
Public URL | https://durham-repository.worktribe.com/output/1193917 |
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Publisher Licence URL
http://creativecommons.org/licenses/by/4.0/
Copyright Statement
© 2022 The Authors. Published by American Chemical Society. This is an open access article under the CC BY license (https://creativecommons.org/licenses/by/4.0/)
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