Improved heteronuclear decoupling schemes for solid-state magic angle spinning NMR by direct spectral optimization

De Paepe, G.; Hodgkinson, P.; Emsley, L.

Abstract

It is shown that a direct spectral optimization scheme can be implemented to obtain improved heteronuclear dipolar decoupling schemes for solid-state magic-angle-spinning NMR experiments. The resulting schemes, which turn out to have a particularly simple form, are shown to be applicable over the whole range of commercially available spinning speeds (from 5 to 35 kHz), and are shown to improve on the performance of the best existing sequences. (C) 2003 Elsevier Science B.V. All rights reserved.

Citation

De Paepe, G., Hodgkinson, P., & Emsley, L. (2003). Improved heteronuclear decoupling schemes for solid-state magic angle spinning NMR by direct spectral optimization. Chemical Physics Letters, 376(3-4), 259-267

• Journal Article Type: Article
• Publication Date: 2003-07
• Journal: Chemical Physics Letters
• Print ISSN: 0009-2614
• Publisher: Elsevier
• Peer Reviewed: Peer Reviewed
• Volume: 376
• Issue: 3-4
• Pages: 259-267