Photochemical Flow Oximation of Alkanes

Baxendale, Ian R.; Griffiths, Oliver M.; Ruggeri, Michele

Abstract

The nitrosation of several alkanes using tert-butyl nitrite has been performed in flow showing a remarkable reduction in the reaction time compared with batch processing. Due to the necessity for large excesses of the alkane component a continuous recycling process was devised for the preparation of larger quantities of material.

Citation

Baxendale, I. R., Griffiths, O. M., & Ruggeri, M. (2020). Photochemical Flow Oximation of Alkanes. Synlett: Accounts and Rapid Communications in Synthetic Organic Chemistry, 31(19), 1907-1912. https://doi.org/10.1055/s-0040-1707281

• Journal Article Type: Article
• Acceptance Date: Aug 19, 2020
• Online Publication Date: Sep 21, 2020
• Publication Date: 2020
• Deposit Date: Jan 6, 2022
• Publicly Available Date: Jan 6, 2022
• Journal: Synlett: Accounts and Rapid Communications in Synthetic Organic Chemistry
• Print ISSN: 0936-5214
• Electronic ISSN: 1437-2096
• Publisher: Thieme Gruppe
• Peer Reviewed: Peer Reviewed
• Volume: 31
• Issue: 19
• Pages: 1907-1912
• DOI: https://doi.org/10.1055/s-0040-1707281
• Public URL: https://durham-repository.worktribe.com/output/1221246