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Dr Juan Aguilar Malavia's Outputs (3)

Robust NMR water signal suppression for demanding analytical applications (2015)
Journal Article
Aguilar, J. A., & Kenwright, S. J. (2016). Robust NMR water signal suppression for demanding analytical applications. Analyst, 141(1), 236-242. https://doi.org/10.1039/c5an02121a

We describe the design and application of robust, general-purpose water signal suppression pulse sequences well suited to chemometric work. Such pulse sequences need to deal well with pulse mis-calibrations, radiation damping, chemical exchange, and... Read More about Robust NMR water signal suppression for demanding analytical applications.

Ultra-high dispersion NMR reveals new levels of detail (2015)
Journal Article
Aguilar, J., Kiraly, P., Adams, R., Bonneau, M., Grayson, E., Nilsson, M., Kenwright, A., & Morris, G. (2015). Ultra-high dispersion NMR reveals new levels of detail. RSC Advances, 5(65), 52902-52906. https://doi.org/10.1039/c5ra10192a

Pure shift NMR techniques can provide exquisite resolution, enabling chemists to analyse samples that would otherwise require unrealistically high magnetic fields. Although powerful, such techniques remain little used, in part because of the false pe... Read More about Ultra-high dispersion NMR reveals new levels of detail.

Real-time pure shift N-15 HSQC of proteins: a real improvement in resolution and sensitivity (2015)
Journal Article
Kiraly, P., Adams, R. W., Paudel, L., Foroozandeh, M., Aguilar, J. A., Timari, I., Cliff, M. J., Nilsson, M., Sandor, P., Batta, G., Waltho, J. P., Koever, K. E., & Morris, G. A. (2015). Real-time pure shift N-15 HSQC of proteins: a real improvement in resolution and sensitivity. Journal of Biomolecular NMR, 62(1), 43-52. https://doi.org/10.1007/s10858-015-9913-z

Spectral resolution in proton NMR spectroscopy is reduced by the splitting of resonances into multiplets due to the effect of homonuclear scalar couplings. Although these effects are often hidden in protein NMR spectroscopy by low digital resolution... Read More about Real-time pure shift N-15 HSQC of proteins: a real improvement in resolution and sensitivity.