M.R. Hampson
The nature of oxygen exchange in ZrW2O8 revealed by two-dimensional solid-state O-17 NMR
Hampson, M.R.; Hodgkinson, P.; Evans, J.S.O.; Harris, R.K.; King, I.J.; Allen, S.; Fayon, F.
Authors
Professor Paul Hodgkinson paul.hodgkinson@durham.ac.uk
Professor
Professor John Evans john.evans@durham.ac.uk
Professor
R.K. Harris
I.J. King
S. Allen
F. Fayon
Abstract
O-17 magic angle spinning (MAS) NMR has been used to determine the nature of oxygen exchange in ZrW2O8. A highly effective isotopic labelling technique has been developed and 1D NMR and 2D exchange spectroscopy (EXSY) experiments have revealed that mutual exchange occurs between all oxygen sites, even at temperatures considerably below the alpha to beta order-disorder phase transition.
Citation
Hampson, M., Hodgkinson, P., Evans, J., Harris, R., King, I., Allen, S., & Fayon, F. (online). The nature of oxygen exchange in ZrW2O8 revealed by two-dimensional solid-state O-17 NMR. Chemical Communications, 392-393
| Journal Article Type | Article |
|---|---|
| Journal | Chemical Communications |
| Print ISSN | 1359-7345 |
| Electronic ISSN | 1364-548X |
| Publisher | Royal Society of Chemistry |
| Peer Reviewed | Peer Reviewed |
| Issue | 4 |
| Pages | 392-393 |
| Public URL | https://durham-repository.worktribe.com/output/1602283 |
You might also like
Solid State Materials Chemistry
(2021)
Book
Solid State Materials Chemistry
(2020)
Book
Rietveld Refinement
(2018)
Book