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An Efficient Route To S-N-(9-Fluorenylmethoxycarbonyl)-4'-(1-Azi-2,2,2-Trifluoroethyl)phenylalanine (1994)
Journal Article
Fishwick, C., Sanderson, J., & Findlay, J. (1994). An Efficient Route To S-N-(9-Fluorenylmethoxycarbonyl)-4'-(1-Azi-2,2,2-Trifluoroethyl)phenylalanine. Tetrahedron Letters, 35(26), 4611-4614. https://doi.org/10.1016/s0040-4039%2800%2960743-8

An extremely efficient synthesis of optically pure photoactivatable phenylalanine derivative 1 is described. The key step involves a highly diastereoselective alkylation of a chiral glycine equivalent.

IMINOAMINOSULFINATES - SYNTHESIS, CRYSTAL-STRUCTURES, AND REARRANGEMENT MONITORED BY LI-7 SOLID-STATE NUCLEAR-MAGNETIC-RESONANCE SPECTROSCOPY (1993)
Journal Article
FREITAG, S., Kolodziejski, W., Pauer, F., & Stalke, D. (1993). IMINOAMINOSULFINATES - SYNTHESIS, CRYSTAL-STRUCTURES, AND REARRANGEMENT MONITORED BY LI-7 SOLID-STATE NUCLEAR-MAGNETIC-RESONANCE SPECTROSCOPY. Dalton Transactions, 3479-3488. https://doi.org/10.1039/dt9930003479

Alkali- and alkaline-earth-metal iminoaminosulfinates have been synthesised and characterized by X-ray diffraction and solid-state NMR investigations. The viability of metal-exchange reactions has been demonstrated resulting in a magnesium and a copp... Read More about IMINOAMINOSULFINATES - SYNTHESIS, CRYSTAL-STRUCTURES, AND REARRANGEMENT MONITORED BY LI-7 SOLID-STATE NUCLEAR-MAGNETIC-RESONANCE SPECTROSCOPY.

SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF A STANNAIMINE (1993)
Journal Article
Ossig, G., Meller, A., FREITAG, S., & Herbstirmer, R. (1993). SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF A STANNAIMINE. Journal of the Chemical Society. Chemical communications, 497-499. https://doi.org/10.1039/c39930000497

A stannaimine has been isolated for the first time; the tin atom is surrounded by three nitrogen atoms in a planar arrangement and the tin–nitrogen double bond is shortened by 10 pm compared with tin–nitrogen single bonds.

REACTIONS OF GERMYLENES WITH ACID AZIDES (1992)
Journal Article
Meller, A., Ossig, G., Maringgele, W., Noltemeyer, M., Stalke, D., Herbstirmer, R., …Sheldrick, G. (1992). REACTIONS OF GERMYLENES WITH ACID AZIDES

SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF GERMAIMINES (1991)
Journal Article
Meller, A., Ossig, G., Maringgele, W., Stalke, D., Herbstirmer, R., FREITAG, S., & Sheldrick, G. (1991). SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF GERMAIMINES. Journal of the Chemical Society. Chemical communications, 1123-1124. https://doi.org/10.1039/c39910001123

Three new germaimines have been synthesized and two of them characterized by X-ray diffraction; the Ge[double bond, length half m-dash]N bond lengths agree well with an ab initio prediction for H2Ge[double bond, length half m-dash]NH.

Formative Assessment: improving students' experience in the teaching labs
Journal Article
Milian, L. (online). Formative Assessment: improving students' experience in the teaching labs. Online educational research journal,

Formative assessment is recognised as one of the most effective ways to help and promote students’ learning. Students consider laboratory learning to be challenging, though sometimes it is not appreciated and not recognised as a valuable source of le... Read More about Formative Assessment: improving students' experience in the teaching labs.

Lanthanide Complexes Formed with the Tri- and Tetraacetate Derivatives of Bis(aminomethyl)phosphinic Acid: Equilibrium, Kinetic and NMR Spectroscopic Studies
Journal Article
Tircso, G., Kalman, F. K., Pal, R., Banyai, I., Varga, T. R., Kiraly, R., Lazar, I., Quebatte, L., Merbach, A. E., Toth, E., & Bruecher, E. (online). Lanthanide Complexes Formed with the Tri- and Tetraacetate Derivatives of Bis(aminomethyl)phosphinic Acid: Equilibrium, Kinetic and NMR Spectroscopic Studies. European Journal of Inorganic Chemistry, 2062-2073. https://doi.org/10.1002/ejic.201101299