# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2021
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_boran
_database_code_depnum_ccdc_archive 'CCDC 2034385'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-09-28 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-03-10
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.01.16 svn.ra754ea2f for OlexSys, GUI svn.r6014)
;
_chemical_formula_moiety '4.001(H2 N0.5), 0.5(B12 H12)'
_chemical_formula_sum 'B6.001 H14.002 N2'
_chemical_formula_weight 107.087
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_dispersion_source
H 0.00000 0.00000 Sasaki
B 0.00000 0.00000 Sasaki
N 0.00000 0.00000 Sasaki
_space_group_crystal_system cubic
_space_group_IT_number 225
_space_group_name_H-M_alt 'F m -3 m'
_space_group_name_Hall '-F 4 2 3'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x,-z,y
3 x,z,-y
4 z,y,-x
5 -z,y,x
6 -y,x,z
7 y,-x,z
8 z,x,y
9 y,z,x
10 -y,-z,x
11 z,-x,-y
12 -y,z,-x
13 -z,-x,y
14 -z,x,-y
15 y,-z,-x
16 x,-y,-z
17 -x,y,-z
18 -x,-y,z
19 y,x,-z
20 -y,-x,-z
21 z,-y,x
22 -z,-y,-x
23 -x,z,y
24 -x,-z,-y
25 -x,-y,-z
26 -x,z,-y
27 -x,-z,y
28 -z,-y,x
29 z,-y,-x
30 y,-x,-z
31 -y,x,-z
32 -z,-x,-y
33 -y,-z,-x
34 y,z,-x
35 -z,x,y
36 y,-z,x
37 z,x,-y
38 z,-x,y
39 -y,z,x
40 -x,y,z
41 x,-y,z
42 x,y,-z
43 -y,-x,z
44 y,x,z
45 -z,y,-x
46 z,y,x
47 x,-z,-y
48 x,z,y
49 x,y+1/2,z+1/2
50 x,-z+1/2,y+1/2
51 x,z+1/2,-y+1/2
52 z,y+1/2,-x+1/2
53 -z,y+1/2,x+1/2
54 -y,x+1/2,z+1/2
55 y,-x+1/2,z+1/2
56 z,x+1/2,y+1/2
57 y,z+1/2,x+1/2
58 -y,-z+1/2,x+1/2
59 z,-x+1/2,-y+1/2
60 -y,z+1/2,-x+1/2
61 -z,-x+1/2,y+1/2
62 -z,x+1/2,-y+1/2
63 y,-z+1/2,-x+1/2
64 x,-y+1/2,-z+1/2
65 -x,y+1/2,-z+1/2
66 -x,-y+1/2,z+1/2
67 y,x+1/2,-z+1/2
68 -y,-x+1/2,-z+1/2
69 z,-y+1/2,x+1/2
70 -z,-y+1/2,-x+1/2
71 -x,z+1/2,y+1/2
72 -x,-z+1/2,-y+1/2
73 -x,-y+1/2,-z+1/2
74 -x,z+1/2,-y+1/2
75 -x,-z+1/2,y+1/2
76 -z,-y+1/2,x+1/2
77 z,-y+1/2,-x+1/2
78 y,-x+1/2,-z+1/2
79 -y,x+1/2,-z+1/2
80 -z,-x+1/2,-y+1/2
81 -y,-z+1/2,-x+1/2
82 y,z+1/2,-x+1/2
83 -z,x+1/2,y+1/2
84 y,-z+1/2,x+1/2
85 z,x+1/2,-y+1/2
86 z,-x+1/2,y+1/2
87 -y,z+1/2,x+1/2
88 -x,y+1/2,z+1/2
89 x,-y+1/2,z+1/2
90 x,y+1/2,-z+1/2
91 -y,-x+1/2,z+1/2
92 y,x+1/2,z+1/2
93 -z,y+1/2,-x+1/2
94 z,y+1/2,x+1/2
95 x,-z+1/2,-y+1/2
96 x,z+1/2,y+1/2
97 x+1/2,y,z+1/2
98 x+1/2,-z,y+1/2
99 x+1/2,z,-y+1/2
100 z+1/2,y,-x+1/2
101 -z+1/2,y,x+1/2
102 -y+1/2,x,z+1/2
103 y+1/2,-x,z+1/2
104 z+1/2,x,y+1/2
105 y+1/2,z,x+1/2
106 -y+1/2,-z,x+1/2
107 z+1/2,-x,-y+1/2
108 -y+1/2,z,-x+1/2
109 -z+1/2,-x,y+1/2
110 -z+1/2,x,-y+1/2
111 y+1/2,-z,-x+1/2
112 x+1/2,-y,-z+1/2
113 -x+1/2,y,-z+1/2
114 -x+1/2,-y,z+1/2
115 y+1/2,x,-z+1/2
116 -y+1/2,-x,-z+1/2
117 z+1/2,-y,x+1/2
118 -z+1/2,-y,-x+1/2
119 -x+1/2,z,y+1/2
120 -x+1/2,-z,-y+1/2
121 -x+1/2,-y,-z+1/2
122 -x+1/2,z,-y+1/2
123 -x+1/2,-z,y+1/2
124 -z+1/2,-y,x+1/2
125 z+1/2,-y,-x+1/2
126 y+1/2,-x,-z+1/2
127 -y+1/2,x,-z+1/2
128 -z+1/2,-x,-y+1/2
129 -y+1/2,-z,-x+1/2
130 y+1/2,z,-x+1/2
131 -z+1/2,x,y+1/2
132 y+1/2,-z,x+1/2
133 z+1/2,x,-y+1/2
134 z+1/2,-x,y+1/2
135 -y+1/2,z,x+1/2
136 -x+1/2,y,z+1/2
137 x+1/2,-y,z+1/2
138 x+1/2,y,-z+1/2
139 -y+1/2,-x,z+1/2
140 y+1/2,x,z+1/2
141 -z+1/2,y,-x+1/2
142 z+1/2,y,x+1/2
143 x+1/2,-z,-y+1/2
144 x+1/2,z,y+1/2
145 x+1/2,y+1/2,z
146 x+1/2,-z+1/2,y
147 x+1/2,z+1/2,-y
148 z+1/2,y+1/2,-x
149 -z+1/2,y+1/2,x
150 -y+1/2,x+1/2,z
151 y+1/2,-x+1/2,z
152 z+1/2,x+1/2,y
153 y+1/2,z+1/2,x
154 -y+1/2,-z+1/2,x
155 z+1/2,-x+1/2,-y
156 -y+1/2,z+1/2,-x
157 -z+1/2,-x+1/2,y
158 -z+1/2,x+1/2,-y
159 y+1/2,-z+1/2,-x
160 x+1/2,-y+1/2,-z
161 -x+1/2,y+1/2,-z
162 -x+1/2,-y+1/2,z
163 y+1/2,x+1/2,-z
164 -y+1/2,-x+1/2,-z
165 z+1/2,-y+1/2,x
166 -z+1/2,-y+1/2,-x
167 -x+1/2,z+1/2,y
168 -x+1/2,-z+1/2,-y
169 -x+1/2,-y+1/2,-z
170 -x+1/2,z+1/2,-y
171 -x+1/2,-z+1/2,y
172 -z+1/2,-y+1/2,x
173 z+1/2,-y+1/2,-x
174 y+1/2,-x+1/2,-z
175 -y+1/2,x+1/2,-z
176 -z+1/2,-x+1/2,-y
177 -y+1/2,-z+1/2,-x
178 y+1/2,z+1/2,-x
179 -z+1/2,x+1/2,y
180 y+1/2,-z+1/2,x
181 z+1/2,x+1/2,-y
182 z+1/2,-x+1/2,y
183 -y+1/2,z+1/2,x
184 -x+1/2,y+1/2,z
185 x+1/2,-y+1/2,z
186 x+1/2,y+1/2,-z
187 -y+1/2,-x+1/2,z
188 y+1/2,x+1/2,z
189 -z+1/2,y+1/2,-x
190 z+1/2,y+1/2,x
191 x+1/2,-z+1/2,-y
192 x+1/2,z+1/2,y
_symmetry_Int_Tables_number 225
_cell_length_a 9.10295(12)
_cell_length_b 9.10295(12)
_cell_length_c 9.10295(12)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 754.304(17)
_cell_formula_units_Z 4
_cell_measurement_temperature 100.00(10)
_cell_measurement_reflns_used 2677
_cell_measurement_theta_min 3.8490
_cell_measurement_theta_max 75.7830
_cell_oxdiff_length_a 9.1026(3)
_cell_oxdiff_length_b 9.1026(2)
_cell_oxdiff_length_c 9.1036(3)
_cell_oxdiff_angle_alpha 90.021(3)
_cell_oxdiff_angle_beta 89.981(3)
_cell_oxdiff_angle_gamma 89.996(3)
_cell_oxdiff_volume 754.30(4)
_cell_oxdiff_measurement_reflns_used 2677
_exptl_absorpt_correction_T_min 0.71007
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_type multi-scan
_exptl_crystal_description block
_exptl_crystal_colour colorless
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.38b (Rigaku Oxford Diffraction, 2017)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_oxdiff_exptl_absorpt_empirical_full_min 0.917
_oxdiff_exptl_absorpt_empirical_full_max 1.207
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_exptl_absorpt_coefficient_mu 0.046
_exptl_crystal_density_diffrn 0.943
_exptl_crystal_F_000 232.0
_diffrn_reflns_av_R_equivalents 0.0243
_diffrn_reflns_av_unetI/netI 0.0117
_diffrn_reflns_Laue_measured_fraction_full 1.0000
_diffrn_reflns_Laue_measured_fraction_max 1.0000
_diffrn_reflns_limit_h_max 12
_diffrn_reflns_limit_h_min -23
_diffrn_reflns_limit_k_max 11
_diffrn_reflns_limit_k_min -24
_diffrn_reflns_limit_l_max 17
_diffrn_reflns_limit_l_min -23
_diffrn_reflns_number 4841
_diffrn_reflns_point_group_measured_fraction_full 1.0000
_diffrn_reflns_point_group_measured_fraction_max 1.0000
_diffrn_reflns_theta_full 25.2417
_diffrn_reflns_theta_max 62.47
_diffrn_reflns_theta_min 3.88
_diffrn_ambient_temperature 100.0
_diffrn_measured_fraction_theta_full 1.0000
_diffrn_measured_fraction_theta_max 1.0000
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.71073
_reflns_Friedel_coverage 0.0
_reflns_limit_h_max 13
_reflns_limit_h_min 0
_reflns_limit_k_max 22
_reflns_limit_k_min 1
_reflns_limit_l_max 16
_reflns_limit_l_min 0
_reflns_number_gt 341
_reflns_number_total 364
_reflns_threshold_expression I>=2u(I)
_computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_refine_diff_density_max 0.1093
_refine_diff_density_min -0.0662
_refine_diff_density_rms 0.0131
_refine_ls_d_res_high 0.4007
_refine_ls_d_res_low 5.2556
_refine_ls_goodness_of_fit_ref 0.9106
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 11
_refine_ls_number_reflns 364
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0105
_refine_ls_R_factor_gt 0.0095
_refine_ls_restrained_S_all 1.0180
_refine_ls_shift/su_max 0.0002
_refine_ls_shift/su_mean 0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0110P)^2^+0.0085P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0234
_refine_ls_wR_factor_ref 0.0236
_diffrn_ambient_environment N~2~
_diffrn_source 'micro-focus sealed X-ray tube'
_diffrn_source_type 'PhotonJet (Mo) X-ray Source'
_diffrn_radiation_probe x-ray
_diffrn_radiation_monochromator mirror
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 300K'
_diffrn_detector 'CCD plate'
_diffrn_detector_type 'Pilatus 300K'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11 0.0332405000
_diffrn_orient_matrix_UB_12 0.0675561000
_diffrn_orient_matrix_UB_13 -0.0200556000
_diffrn_orient_matrix_UB_21 0.0529070000
_diffrn_orient_matrix_UB_22 -0.0092625000
_diffrn_orient_matrix_UB_23 0.0564269000
_diffrn_orient_matrix_UB_31 0.0465604000
_diffrn_orient_matrix_UB_32 -0.0377135000
_diffrn_orient_matrix_UB_33 -0.0498435000
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):
# Type Start End Width t~exp~ \w \q \k \f Frames
#--------------------------------------------------------------------------
1 \w -5.00 73.00 0.25 20.00 -- 0.00 19.00-180.00 312
2 \w 19.00 77.00 0.25 55.00 -- 84.25 -83.00 -68.00 232
3 \w -49.00 8.00 0.25 20.00 -- 0.00 0.00-180.00 228
4 \w -74.00 -32.00 0.25 55.00 -- -105.75 19.00-120.00 168
5 \w -74.00 -32.00 0.25 55.00 -- -105.75 19.00 -90.00 168
6 \w -178.00-100.00 0.25 55.00 -- -105.75 -19.00 0.00 312
;
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be published - 2020
NoSpherA2 implementation of HAR makes use of
tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or DFT using selected funtionals
- for a fragment of the crystal.
This fregment can be embedded in an electrostatic crystal field by employing cluster charges.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
INT ACCURACY: High
METHOD: PBE
BASIS SET: def2-TZVPP
CHARGE: 6
MULTIPLICITY: 1
DATE: 2020-06-19_12-42-38
;
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
N1 N 0.25 0.25 0.25 0.01112(2) Uani 1.000080 24 S T P
B1 B 0.365268(13) 0.5 0.5 0.01009(2) Uani 1.000000 8 S T P
H1 H 0.2332(4) 0.5 0.5 0.0292(9) Uani 1.000000 8 S T P
H1a H 0.3146(2) 0.1854(2) 0.1854(2) 0.0351(9) Uani 1.000020 6 S T P
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
N1 0.01112(2) 0.01112(2) 0.01112(2) -0.000000 -0.000000 0.000000
B1 0.00831(3) 0.01099(3) 0.01099(3) -0.000000 -0.000000 0.000000
H1 0.0117(16) 0.0379(13) 0.0379(13) -0.000000 -0.000000 0.000000
H1a 0.0351(9) 0.0351(9) 0.0351(9) 0.0063(8) 0.0063(8) -0.0063(8)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
N1 H1a 1.019(3) . ?
N1 H1a 1.019(3) 64 ?
N1 H1a 1.019(3) 8 ?
N1 H1a 1.019(3) 9 ?
B1 B1 1.73447(16) 4_556 ?
B1 B1 1.73447(16) 6_655 ?
B1 B1 1.73447(16) 7_565 ?
B1 B1 1.73447(16) 5_655 ?
B1 H1 1.203(3) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
H1a N1 H1a 109.5 8 . ?
H1a N1 H1a 109.5 64 8 ?
H1a N1 H1a 109.47(11) 64 . ?
H1a N1 H1a 109.5 9 . ?
H1a N1 H1a 109.5 9 8 ?
H1a N1 H1a 109.5 64 9 ?
B1 B1 B1 60.0 6_655 5_655 ?
B1 B1 B1 60.0 7_565 5_655 ?
B1 B1 B1 90.0 7_565 6_655 ?
H1 B1 B1 135.0 . 5_655 ?
H1 B1 B1 135.0 . 7_565 ?
H1 B1 B1 135.0 . 6_655 ?
# start Validation Reply Form
_vrf_PLAT303_boran
;
PROBLEM: Full Occupancy Atom H1A with # Connections 9.00 Check
RESPONSE: Due to the high symmetry and correct bondlengths compared to spherical density descirption of X-ray data the authors are confident the geometry is correct
;
_vrf_PLAT927_boran
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0877 Check
RESPONSE: Non-Spherical refinement, therefore wR2 from CheckCIF is wrong
;
_vrf_PLAT928_boran
;
PROBLEM: Reported and Calculated S value Differ by . -3.586 Check
RESPONSE: Non-Spherical refinement, therefore S from CheckCIF is wrong
;
_vrf_PLAT049_boran
;
PROBLEM: Calculated Density Less Than 1.0 gcm-3 ......... 0.9422 Check
RESPONSE: This structure consists of many light atoms
;
_vrf_PLAT926_boran
;
PROBLEM: Reported and Calculated R1 Differ by ......... -0.0247 Check
RESPONSE: Non-Spherical refinement, therefore R1 from CheckCIF is wrong
;
# end Validation Reply Form
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
_diffrn_refln_scale_group_code
-1 1 -1 8702.13 178.886 1
-1 -1 -1 8705.88 178.847 3
0 0 2 36.222 0.99818 1
2 0 0 34.0091 1.06597 3
-2 0 0 32.9767 1.07136 3
0 2 0 33.1917 1.15125 1
0 0 -2 42.2192 1.03608 1
-2 0 -2 8753.52 176.59 3
2 -2 0 8263.07 176.421 1
-2 2 0 8700.83 176.442 1
0 2 -2 8304.42 176.533 1
0 -2 -2 8797.38 176.29 3
-2 2 2 8562.3 171.987 1
-2 -2 -2 8102.89 172.495 3
2 2 2 8695.05 172.558 3
-2 2 -2 8709.41 172.58 1
1 -3 -1 238.124 5.08027 1
3 -1 -1 211.966 4.89247 3
1 1 3 227.068 5.19037 3
1 1 -3 222.865 5.07728 1
-1 1 -3 220.667 5.19352 1
-3 -1 -1 221.499 5.26174 3
-1 3 1 233.74 5.09483 1
-1 3 -1 234.972 5.31115 1
-3 1 1 234.096 4.91068 3
1 -1 3 212.207 5.19043 1
-1 1 3 229.742 4.8757 3
-3 1 -1 235.251 5.23378 3
-1 -1 3 215.057 5.07309 1
3 -1 1 192.443 5.23884 3
-1 -1 -3 180.573 5.07729 3
-3 -3 -1 369.926 8.42807 3
-1 -3 -3 368.482 8.1754 3
-3 1 -3 348.873 8.39184 1
1 -3 -3 375.584 7.79943 3
-3 -1 -3 330.817 8.34665 3
-3 3 -1 368.272 8.34439 1
1 -3 -3 377.416 7.73515 1
-1 -3 3 312.01 8.33846 1
3 -3 -1 360.829 8.06032 1
-1 3 -3 352.07 8.44212 1
1 3 -3 349.106 8.44442 1
-3 3 1 360.241 8.0748 1
-3 -3 3 3561.91 13.6273 1
-3 3 -3 3763.76 14.1786 1
-3 -3 -3 3732.99 13.6837 3
0 4 0 8962.77 184.095 1
0 0 -4 9074.08 183.73 1
4 0 0 9054.72 183.941 3
-4 0 0 8721.31 183.902 3
0 0 4 8851.08 183.714 1
-4 2 0 1688.42 36.0268 1
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-22 -8 2 32.7791 1.38916 6
-8 -22 2 31.4293 1.42092 6
-2 -22 8 33.8108 1.582 6
2 -22 8 28.7119 1.46303 6
-8 -22 4 0.37974 0.67542 6
-4 -22 8 0.41453 0.71854 6
-8 -22 -4 0.70942 0.70351 5
-8 -22 -4 -0.1402 0.679 4
-8 -22 4 0.15138 0.76592 4
-4 -22 8 0.95132 0.74331 4
-8 -22 -6 29.8936 1.30341 5
-8 -22 -6 30.1817 1.21994 4
-8 -22 6 31.4184 1.36801 6
-6 -22 8 31.1022 1.41811 6
-8 -22 8 3.09786 0.54246 6
-10 -22 0 21.2736 1.15482 4
-10 -22 0 18.6022 0.87688 6
0 -22 10 20.4957 1.12261 6
-22 -10 2 2.15864 0.47921 6
-10 -22 2 1.12099 0.48739 6
-2 -22 10 1.13093 0.61134 6
-10 -22 -2 2.56885 0.67415 5
-10 -22 -2 2.16079 0.6766 4
-10 -22 2 1.43467 0.64782 4
-22 -10 -2 2.9931 0.60878 6
-10 -22 4 2.99991 0.57783 6
-4 -22 10 3.9372 0.63103 6
-10 -22 -4 3.00975 0.59636 5
-10 -22 -4 2.81353 0.58109 4
-22 -10 -4 2.7537 0.55295 6
-10 -22 6 0.5887 0.43769 6
-6 -22 10 0.28953 0.43309 6
-10 -22 -6 0.40195 0.38545 5
-22 -10 -6 0.73598 0.39155 6
1 -1 -23 15.4858 1.16216 2
1 1 -23 15.1622 1.15747 2
-1 -1 -23 17.7636 1.19628 2
-1 1 -23 17.2607 1.18637 2
-1 -23 -1 16.723 1.16965 4
-1 -23 1 15.8646 1.22487 4
1 -23 -1 15.0847 1.0262 4
1 -23 1 17.0169 1.17379 4
3 -1 -23 1.66037 0.7316 2
3 1 -23 2.44368 0.70312 2
1 -3 -23 2.3795 0.67115 2
1 3 -23 1.79553 0.67175 2
-1 -3 -23 2.87114 0.7233 2
-1 3 -23 2.14243 0.69577 2
-3 -1 -23 2.12108 0.72294 2
-3 1 -23 2.57483 0.71079 2
-3 -23 -1 2.95347 0.79509 4
-3 -23 1 2.71536 0.87958 4
-1 -23 -3 2.6693 0.61966 4
-1 -23 3 2.20508 0.86331 4
1 -23 3 3.32324 0.89325 4
-23 -3 1 2.79394 0.58931 6
3 -3 -23 1.35712 0.64896 2
3 3 -23 0.77541 0.58744 2
-3 -23 3 0.37859 0.53729 6
-3 -3 -23 0.79104 0.60432 2
-3 3 -23 0.21792 0.56605 2
-3 -23 3 0.05548 0.84357 4
3 -23 3 1.35604 0.69218 4
5 -1 -23 3.49995 0.72127 2
5 1 -23 4.26972 0.70139 2
1 -23 5 3.85796 0.5991 6
-5 -1 -23 2.89419 0.69466 2
-5 1 -23 3.99288 0.69001 2
-5 -23 -1 4.03527 0.80684 4
-5 -23 1 4.03078 0.86837 4
-1 -23 5 3.55774 0.88654 4
1 -23 5 3.5021 0.85984 4
-23 -5 1 2.5034 0.57265 6
-3 -23 5 0.21676 0.57623 6
-5 -23 -3 -0.85613 0.63958 4
-5 -23 3 0.30706 0.75783 4
-3 -23 5 0.563 0.79158 4
-5 -23 5 0.68044 0.56109 6
-5 -23 -5 0.44829 0.39167 4
-5 -23 5 -0.09209 0.65312 4
-7 -23 -1 12.6023 0.95766 4
-7 -23 1 12.0543 0.97329 4
-1 -23 7 12.6349 0.99057 4
-23 -7 -1 12.8871 0.8701 6
-23 -7 1 12.0323 0.72658 6
-1 -23 7 12.4284 0.86053 6
-3 -23 7 2.80084 0.60085 6
-7 -23 -3 3.16943 0.62738 4
-7 -23 3 2.42269 0.66896 4
-3 -23 7 2.8455 0.6837 4
-7 -23 5 3.09012 0.53314 6
-5 -23 7 3.63332 0.55533 6
-7 -23 5 2.89451 0.58438 4
-5 -23 7 4.41288 0.61225 4
-9 -23 -1 5.50727 0.61648 4
-9 -23 1 5.96523 0.63977 4
-23 -9 -1 4.44218 0.48241 6
-3 -23 9 0.44101 0.39484 6
-9 -23 -3 0.8874 0.4151 4
-9 -23 3 0.27341 0.42167 4
-23 -9 -3 0.294 0.3563 6
-2 -24 0 1.29655 0.54794 4
0 -24 2 0.41927 0.53021 4
-2 -24 -2 4.16102 0.4651 4
-2 -24 2 3.64454 0.6436 4
-4 -24 0 4.70843 0.64725 4
0 -24 4 4.87674 0.65277 4
-4 -24 2 8.95574 0.76377 4
-2 -24 4 10.9091 0.81131 4
-4 -24 4 0.41684 0.48317 4
-6 -24 0 -0.03121 0.42845 4
-6 -24 2 6.09141 0.58775 4
-2 -24 6 4.25622 0.55259 4
_iucr_refine_fcf_details
;
data_boran_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x,-z,y
3 x,z,-y
4 z,y,-x
5 -z,y,x
6 -y,x,z
7 y,-x,z
8 z,x,y
9 y,z,x
10 -y,-z,x
11 z,-x,-y
12 -y,z,-x
13 -z,-x,y
14 -z,x,-y
15 y,-z,-x
16 x,-y,-z
17 -x,y,-z
18 -x,-y,z
19 y,x,-z
20 -y,-x,-z
21 z,-y,x
22 -z,-y,-x
23 -x,z,y
24 -x,-z,-y
25 -x,-y,-z
26 -x,z,-y
27 -x,-z,y
28 -z,-y,x
29 z,-y,-x
30 y,-x,-z
31 -y,x,-z
32 -z,-x,-y
33 -y,-z,-x
34 y,z,-x
35 -z,x,y
36 y,-z,x
37 z,x,-y
38 z,-x,y
39 -y,z,x
40 -x,y,z
41 x,-y,z
42 x,y,-z
43 -y,-x,z
44 y,x,z
45 -z,y,-x
46 z,y,x
47 x,-z,-y
48 x,z,y
49 x,y+1/2,z+1/2
50 x,-z+1/2,y+1/2
51 x,z+1/2,-y+1/2
52 z,y+1/2,-x+1/2
53 -z,y+1/2,x+1/2
54 -y,x+1/2,z+1/2
55 y,-x+1/2,z+1/2
56 z,x+1/2,y+1/2
57 y,z+1/2,x+1/2
58 -y,-z+1/2,x+1/2
59 z,-x+1/2,-y+1/2
60 -y,z+1/2,-x+1/2
61 -z,-x+1/2,y+1/2
62 -z,x+1/2,-y+1/2
63 y,-z+1/2,-x+1/2
64 x,-y+1/2,-z+1/2
65 -x,y+1/2,-z+1/2
66 -x,-y+1/2,z+1/2
67 y,x+1/2,-z+1/2
68 -y,-x+1/2,-z+1/2
69 z,-y+1/2,x+1/2
70 -z,-y+1/2,-x+1/2
71 -x,z+1/2,y+1/2
72 -x,-z+1/2,-y+1/2
73 -x,-y+1/2,-z+1/2
74 -x,z+1/2,-y+1/2
75 -x,-z+1/2,y+1/2
76 -z,-y+1/2,x+1/2
77 z,-y+1/2,-x+1/2
78 y,-x+1/2,-z+1/2
79 -y,x+1/2,-z+1/2
80 -z,-x+1/2,-y+1/2
81 -y,-z+1/2,-x+1/2
82 y,z+1/2,-x+1/2
83 -z,x+1/2,y+1/2
84 y,-z+1/2,x+1/2
85 z,x+1/2,-y+1/2
86 z,-x+1/2,y+1/2
87 -y,z+1/2,x+1/2
88 -x,y+1/2,z+1/2
89 x,-y+1/2,z+1/2
90 x,y+1/2,-z+1/2
91 -y,-x+1/2,z+1/2
92 y,x+1/2,z+1/2
93 -z,y+1/2,-x+1/2
94 z,y+1/2,x+1/2
95 x,-z+1/2,-y+1/2
96 x,z+1/2,y+1/2
97 x+1/2,y,z+1/2
98 x+1/2,-z,y+1/2
99 x+1/2,z,-y+1/2
100 z+1/2,y,-x+1/2
101 -z+1/2,y,x+1/2
102 -y+1/2,x,z+1/2
103 y+1/2,-x,z+1/2
104 z+1/2,x,y+1/2
105 y+1/2,z,x+1/2
106 -y+1/2,-z,x+1/2
107 z+1/2,-x,-y+1/2
108 -y+1/2,z,-x+1/2
109 -z+1/2,-x,y+1/2
110 -z+1/2,x,-y+1/2
111 y+1/2,-z,-x+1/2
112 x+1/2,-y,-z+1/2
113 -x+1/2,y,-z+1/2
114 -x+1/2,-y,z+1/2
115 y+1/2,x,-z+1/2
116 -y+1/2,-x,-z+1/2
117 z+1/2,-y,x+1/2
118 -z+1/2,-y,-x+1/2
119 -x+1/2,z,y+1/2
120 -x+1/2,-z,-y+1/2
121 -x+1/2,-y,-z+1/2
122 -x+1/2,z,-y+1/2
123 -x+1/2,-z,y+1/2
124 -z+1/2,-y,x+1/2
125 z+1/2,-y,-x+1/2
126 y+1/2,-x,-z+1/2
127 -y+1/2,x,-z+1/2
128 -z+1/2,-x,-y+1/2
129 -y+1/2,-z,-x+1/2
130 y+1/2,z,-x+1/2
131 -z+1/2,x,y+1/2
132 y+1/2,-z,x+1/2
133 z+1/2,x,-y+1/2
134 z+1/2,-x,y+1/2
135 -y+1/2,z,x+1/2
136 -x+1/2,y,z+1/2
137 x+1/2,-y,z+1/2
138 x+1/2,y,-z+1/2
139 -y+1/2,-x,z+1/2
140 y+1/2,x,z+1/2
141 -z+1/2,y,-x+1/2
142 z+1/2,y,x+1/2
143 x+1/2,-z,-y+1/2
144 x+1/2,z,y+1/2
145 x+1/2,y+1/2,z
146 x+1/2,-z+1/2,y
147 x+1/2,z+1/2,-y
148 z+1/2,y+1/2,-x
149 -z+1/2,y+1/2,x
150 -y+1/2,x+1/2,z
151 y+1/2,-x+1/2,z
152 z+1/2,x+1/2,y
153 y+1/2,z+1/2,x
154 -y+1/2,-z+1/2,x
155 z+1/2,-x+1/2,-y
156 -y+1/2,z+1/2,-x
157 -z+1/2,-x+1/2,y
158 -z+1/2,x+1/2,-y
159 y+1/2,-z+1/2,-x
160 x+1/2,-y+1/2,-z
161 -x+1/2,y+1/2,-z
162 -x+1/2,-y+1/2,z
163 y+1/2,x+1/2,-z
164 -y+1/2,-x+1/2,-z
165 z+1/2,-y+1/2,x
166 -z+1/2,-y+1/2,-x
167 -x+1/2,z+1/2,y
168 -x+1/2,-z+1/2,-y
169 -x+1/2,-y+1/2,-z
170 -x+1/2,z+1/2,-y
171 -x+1/2,-z+1/2,y
172 -z+1/2,-y+1/2,x
173 z+1/2,-y+1/2,-x
174 y+1/2,-x+1/2,-z
175 -y+1/2,x+1/2,-z
176 -z+1/2,-x+1/2,-y
177 -y+1/2,-z+1/2,-x
178 y+1/2,z+1/2,-x
179 -z+1/2,x+1/2,y
180 y+1/2,-z+1/2,x
181 z+1/2,x+1/2,-y
182 z+1/2,-x+1/2,y
183 -y+1/2,z+1/2,x
184 -x+1/2,y+1/2,z
185 x+1/2,-y+1/2,z
186 x+1/2,y+1/2,-z
187 -y+1/2,-x+1/2,z
188 y+1/2,x+1/2,z
189 -z+1/2,y+1/2,-x
190 z+1/2,y+1/2,x
191 x+1/2,-z+1/2,-y
192 x+1/2,z+1/2,y
_space_group_crystal_system cubic
_space_group_IT_number 225
_space_group_name_H-M_alt 'F m -3 m'
_space_group_name_Hall '-F 4 2 3'
_symmetry_space_group_name_H-M 'F m -3 m'
_symmetry_space_group_name_Hall '-F 4 2 3'
_symmetry_Int_Tables_number 225
_cell_length_a 9.10295(12)
_cell_length_b 9.10295(12)
_cell_length_c 9.10295(12)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 754.304(17)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
0 2 0 18.553 19.222 0.769 11.615 o
0 2 2 4527.570 4547.440 59.116 0.002 o
0 4 0 4661.780 4740.910 43.633 0.002 o
0 4 2 897.748 911.674 7.423 0.057 o
0 4 4 260.440 267.626 3.377 0.419 o
0 6 0 211.574 206.887 2.403 0.714 o
0 6 2 998.463 1012.860 5.543 0.057 o
0 6 4 126.979 126.008 0.516 2.802 o
0 6 6 1031.830 1047.250 7.907 0.046 o
0 8 0 2126.310 2114.350 31.239 0.006 o
0 8 2 52.205 53.350 0.467 9.213 o
0 8 4 542.774 539.420 2.910 0.189 o
0 8 6 84.365 83.954 0.529 4.965 o
0 8 8 1066.480 1053.750 6.524 0.049 o
0 10 0 9.644 10.437 0.377 38.684 o
0 10 2 150.259 148.407 1.001 1.847 o
0 10 4 212.307 211.845 1.505 0.967 o
0 10 6 225.894 225.921 1.512 0.886 o
0 10 8 0.121 0.024 0.086 1132.040 o
0 10 10 33.448 32.946 0.551 12.800 o
0 12 0 302.575 305.629 3.614 0.344 o
0 12 2 62.045 62.071 0.477 7.545 o
0 12 4 9.170 9.441 0.192 73.288 o
0 12 6 16.904 16.364 0.225 40.678 o
0 12 8 160.453 159.807 1.266 1.516 o
0 12 10 59.564 59.337 0.721 6.334 o
0 12 12 7.202 7.314 0.727 15.455 o
0 14 0 80.698 80.698 1.386 2.714 o
0 14 2 267.815 270.538 1.829 0.640 o
0 14 4 4.075 4.105 0.175 136.709 o
0 14 6 272.844 270.915 1.853 0.625 o
0 14 8 36.197 36.112 0.471 13.393 o
0 14 10 82.916 83.746 0.896 3.924 o
0 14 12 1.191 1.605 0.363 64.287 o
0 14 14 90.110 92.001 2.045 1.548 o
0 16 0 282.483 287.877 9.712 0.087 o
0 16 2 0.739 0.750 0.167 268.917 o
0 16 4 62.204 63.482 0.913 5.005 o
0 16 6 5.678 5.487 0.246 82.298 o
0 16 8 154.129 154.991 1.917 1.170 o
0 16 10 1.083 1.247 0.192 197.666 o
0 16 12 25.931 26.867 0.709 11.395 o
0 16 14 2.762 2.872 0.340 65.664 o
0 16 16 27.887 25.081 0.766 10.198 o
0 18 0 2.257 2.581 0.385 54.522 o
0 18 2 12.963 13.391 0.265 45.555 o
0 18 4 50.297 51.910 1.061 4.926 o
0 18 6 19.996 20.823 0.375 25.394 o
0 18 8 2.190 2.341 0.202 152.990 o
0 18 10 2.526 2.550 0.224 127.586 o
0 18 12 15.936 16.105 0.401 28.108 o
0 20 0 43.958 44.197 1.188 4.560 o
0 20 2 5.137 5.443 0.298 67.487 o
0 20 4 4.822 5.035 0.311 65.403 o
0 20 6 1.263 1.402 0.163 242.518 o
0 20 8 24.911 24.837 0.452 18.788 o
0 20 10 5.390 5.558 0.252 81.421 o
0 22 0 6.968 7.333 0.495 29.644 o
0 22 2 31.476 31.131 0.478 15.002 o
0 22 4 0.122 0.034 0.156 366.676 o
1 1 1 4579.210 4618.480 67.111 0.001 o
1 3 1 121.298 117.723 1.698 1.631 o
1 3 3 196.872 189.792 2.300 0.799 o
1 5 1 166.504 156.251 7.098 0.168 o
1 5 3 138.885 141.285 0.598 2.356 o
1 5 5 3.268 3.450 0.097 236.705 o
1 7 1 696.884 696.131 3.860 0.116 o
1 7 3 92.093 89.500 0.412 4.715 o
1 7 5 128.274 129.880 0.593 2.664 o
1 7 7 575.253 571.466 2.764 0.176 o
1 9 1 234.558 236.897 1.666 0.802 o
1 9 3 0.199 0.359 0.059 1651.920 o
1 9 5 14.215 14.205 0.141 55.837 o
1 9 7 205.147 206.782 0.816 1.221 o
1 9 9 56.194 55.254 0.476 8.536 o
1 11 1 5.497 5.525 0.165 118.555 o
1 11 3 88.339 88.753 0.474 4.785 o
1 11 5 36.557 34.990 0.292 16.799 o
1 11 7 13.447 13.132 0.163 57.021 o
1 11 9 0.829 0.861 0.108 488.234 o
1 11 11 42.757 42.946 0.761 7.911 o
1 13 1 68.231 67.848 0.554 6.363 o
1 13 3 1.084 1.060 0.092 519.196 o
1 13 5 1.018 1.056 0.102 476.054 o
1 13 7 66.831 66.540 0.580 6.385 o
1 13 9 15.374 15.392 0.237 42.765 o
1 13 11 2.115 2.012 0.189 171.216 o
1 13 13 3.786 3.593 0.347 60.009 o
1 15 1 143.691 142.388 1.194 1.795 o
1 15 3 21.032 20.765 0.238 32.058 o
1 15 5 33.698 33.870 0.336 17.137 o
1 15 7 114.919 113.994 0.970 2.627 o
1 15 9 46.400 46.801 0.910 6.200 o
1 15 11 4.211 4.518 0.253 89.660 o
1 15 13 16.317 17.121 0.385 28.556 o
1 15 15 26.455 27.954 0.594 13.763 o
1 17 1 13.206 13.222 0.264 45.436 o
1 17 3 2.689 2.722 0.166 179.489 o
1 17 5 0.130 0.157 0.137 464.335 o
1 17 7 14.360 14.265 0.302 38.751 o
1 17 9 2.240 2.272 0.175 182.955 o
1 17 11 2.192 2.088 0.254 110.488 o
1 17 13 0.383 0.336 0.179 262.418 o
1 17 15 3.925 3.860 0.182 135.291 o
1 19 1 0.180 0.080 0.164 327.001 o
1 19 3 10.793 10.862 0.248 54.946 o
1 19 5 5.015 5.015 0.205 105.295 o
1 19 7 0.940 0.719 0.164 267.858 o
1 19 9 0.215 0.267 0.139 434.222 o
1 19 11 5.695 6.069 0.277 70.717 o
1 21 1 12.336 12.174 0.285 45.252 o
1 21 3 0.633 0.896 0.123 431.208 o
1 21 5 1.768 1.816 0.131 282.865 o
1 21 7 10.867 10.764 0.197 63.605 o
2 2 2 4390.050 4523.230 62.409 0.001 o
2 4 2 27.395 28.289 0.341 20.744 o
2 4 4 2356.570 2367.270 12.159 0.011 o
2 6 2 450.800 459.482 2.813 0.251 o
2 6 4 40.831 38.768 0.410 13.085 o
2 6 6 82.245 80.398 0.601 4.946 o
2 8 2 343.412 338.665 1.947 0.441 o
2 8 4 191.297 191.182 0.832 1.364 o
2 8 6 452.742 450.314 1.754 0.291 o
2 8 8 12.196 12.331 0.235 52.014 o
2 10 2 325.806 328.009 2.142 0.454 o
2 10 4 18.315 17.988 0.188 40.015 o
2 10 6 146.363 144.195 0.890 2.002 o
2 10 8 84.493 81.983 0.593 4.820 o
2 10 10 202.607 201.126 1.684 0.969 o
2 12 2 0.717 0.766 0.094 607.588 o
2 12 4 418.945 415.656 1.698 0.334 o
2 12 6 15.836 16.119 0.203 44.447 o
2 12 8 44.758 45.282 0.403 11.677 o
2 12 10 1.062 1.028 0.118 401.965 o
2 12 12 122.786 126.416 1.589 1.693 o
2 14 2 13.151 14.065 0.277 43.257 o
2 14 4 26.608 26.393 0.277 23.797 o
2 14 6 0.903 0.985 0.121 408.946 o
2 14 8 145.342 144.422 1.005 1.922 o
2 14 10 18.608 18.472 0.323 30.350 o
2 14 12 14.221 14.946 0.276 41.073 o
2 14 14 0.040 0.039 0.438 47.879 o
2 16 2 49.697 50.973 0.909 5.922 o
2 16 4 46.855 46.374 0.358 11.678 o
2 16 6 62.394 62.081 0.540 7.138 o
2 16 8 0.030 0.172 0.122 594.047 o
2 16 10 12.668 12.522 0.253 48.329 o
2 16 12 14.443 14.550 0.335 35.377 o
2 16 14 25.082 25.752 0.387 20.844 o
2 16 16 0.316 0.235 0.184 253.820 o
2 18 2 66.144 68.347 0.698 5.767 o
2 18 4 4.652 4.752 0.153 140.258 o
2 18 6 34.480 34.230 0.353 16.452 o
2 18 8 7.154 7.185 0.218 80.388 o
2 18 10 41.489 41.343 0.589 10.162 o
2 18 12 0.527 0.364 0.215 183.643 o
2 20 2 2.881 2.726 0.269 94.710 o
2 20 4 37.130 37.795 0.315 15.735 o
2 20 6 5.925 6.185 0.174 107.552 o
2 20 8 3.818 3.856 0.159 154.580 o
2 20 10 0.348 0.389 0.148 369.865 o
2 22 2 0.545 0.554 0.153 327.686 o
2 22 4 6.371 6.010 0.158 111.320 o
3 3 3 1972.970 1955.960 31.095 0.006 o
3 5 3 523.182 539.525 3.491 0.182 o
3 5 5 554.288 552.553 4.548 0.147 o
3 7 3 87.796 87.762 0.602 4.509 o
3 7 5 3.135 3.481 0.076 266.368 o
3 7 7 83.068 84.053 0.666 4.619 o
3 9 3 163.560 165.398 1.035 1.606 o
3 9 5 83.841 81.347 0.535 5.043 o
3 9 7 8.915 8.410 0.160 84.495 o
3 9 9 5.804 5.660 0.190 103.387 o
3 11 3 395.461 394.015 2.412 0.328 o
3 11 5 261.303 262.700 1.251 0.761 o
3 11 7 31.375 30.248 0.334 18.755 o
3 11 9 72.655 73.892 0.565 5.807 o
3 11 11 165.207 164.876 2.158 0.984 o
3 13 3 97.236 97.726 0.790 3.542 o
3 13 5 49.161 47.750 0.425 10.453 o
3 13 7 0.473 0.584 0.139 390.935 o
3 13 9 6.171 5.849 0.184 102.691 o
3 13 11 41.909 42.680 0.546 10.572 o
3 13 13 5.184 5.755 0.427 39.836 o
3 15 3 5.005 5.353 0.220 96.859 o
3 15 5 0.372 0.357 0.126 487.897 o
3 15 7 22.753 22.771 0.325 25.471 o
3 15 9 3.326 3.310 0.163 164.737 o
3 15 11 4.074 4.429 0.205 115.695 o
3 15 13 0.501 0.344 0.258 130.796 o
3 15 15 6.010 5.997 0.356 50.569 o
3 17 3 42.446 42.679 0.480 11.370 o
3 17 5 24.649 24.733 0.301 24.642 o
3 17 7 0.206 0.328 0.156 349.499 o
3 17 9 4.552 4.709 0.242 91.933 o
3 17 11 19.408 19.954 0.393 25.074 o
3 17 13 3.308 3.254 0.194 138.016 o
3 19 3 45.606 48.479 0.650 8.529 o
3 19 5 29.944 30.725 0.337 19.169 o
3 19 7 4.236 4.366 0.195 120.616 o
3 19 9 9.243 9.234 0.215 68.283 o
3 19 11 20.152 21.388 0.439 22.014 o
3 21 3 2.998 2.902 0.192 145.899 o
3 21 5 1.116 1.199 0.140 313.386 o
3 21 7 1.167 1.188 0.116 390.502 o
4 4 4 196.500 206.972 3.038 0.584 o
4 6 4 943.850 937.803 5.158 0.065 o
4 6 6 94.965 94.858 0.652 3.965 o
4 8 4 7.519 7.610 0.146 99.785 o
4 8 6 55.445 55.221 0.504 8.410 o
4 8 8 234.914 234.224 1.810 0.771 o
4 10 4 829.984 825.924 4.524 0.083 o
4 10 6 0.002 0.016 0.075 1630.970 o
4 10 8 133.664 133.622 0.731 2.401 o
4 10 10 22.308 22.165 0.365 24.096 o
4 12 4 87.786 87.612 0.841 3.862 o
4 12 6 224.167 221.896 1.526 0.896 o
4 12 8 4.306 4.314 0.147 152.237 o
4 12 10 237.670 237.506 1.426 0.845 o
4 12 12 16.861 15.796 0.529 20.325 o
4 14 4 131.856 131.828 1.104 2.072 o
4 14 6 45.783 45.709 0.530 9.983 o
4 14 8 4.461 4.406 0.183 125.477 o
4 14 10 4.466 4.511 0.239 94.489 o
4 14 12 39.914 40.611 0.531 11.255 o
4 14 14 21.995 22.536 0.596 15.291 o
4 16 4 0.045 0.231 0.174 297.258 o
4 16 6 19.531 18.976 0.314 29.893 o
4 16 8 34.314 34.412 0.404 15.418 o
4 16 10 34.962 35.329 0.458 14.021 o
4 16 12 0.579 0.553 0.221 172.210 o
4 16 14 2.784 3.312 0.236 112.534 o
4 18 4 141.746 142.671 1.209 1.802 o
4 18 6 0.345 0.423 0.144 387.090 o
4 18 8 32.075 30.473 0.922 7.441 o
4 18 10 4.425 4.230 0.231 99.375 o
4 18 12 45.379 46.103 0.805 7.157 o
4 20 4 2.757 2.980 0.222 123.828 o
4 20 6 20.317 20.809 0.254 31.829 o
4 20 8 2.703 2.870 0.139 211.317 o
4 20 10 22.938 21.632 0.386 22.974 o
4 22 4 8.697 8.252 0.246 65.004 o
5 5 5 134.279 136.538 1.808 1.390 o
5 7 5 0.596 0.456 0.066 1017.260 o
5 7 7 158.119 155.757 0.987 1.734 o
5 9 5 26.661 26.658 0.364 20.703 o
5 9 7 23.195 24.395 0.240 28.302 o
5 9 9 0.040 -0.072 0.116 678.819 o
5 11 5 159.004 158.799 2.119 1.035 o
5 11 7 9.439 10.022 0.222 64.651 o
5 11 9 40.559 39.354 0.388 13.408 o
5 11 11 106.547 107.406 1.256 2.382 o
5 13 5 22.539 22.993 0.469 19.389 o
5 13 7 4.835 4.737 0.212 104.367 o
5 13 9 0.648 0.641 0.146 343.617 o
5 13 11 24.526 23.363 0.392 21.467 o
5 13 13 1.324 1.196 0.279 103.519 o
5 15 5 0.646 0.698 0.188 225.254 o
5 15 7 32.490 32.314 0.441 15.426 o
5 15 9 7.378 7.390 0.260 67.418 o
5 15 11 0.929 1.363 0.232 145.836 o
5 15 13 1.852 2.146 0.191 172.164 o
5 15 15 8.137 7.715 0.272 61.700 o
5 17 5 12.648 13.388 0.380 33.627 o
5 17 7 0.234 0.324 0.151 366.565 o
5 17 9 1.374 1.126 0.206 172.542 o
5 17 11 11.918 11.731 0.296 44.861 o
5 17 13 1.328 1.276 0.171 226.975 o
5 19 5 19.078 20.225 0.856 9.769 o
5 19 7 1.542 1.691 0.166 222.798 o
5 19 9 5.087 4.772 0.183 116.947 o
5 19 11 13.672 12.994 0.246 46.815 o
5 21 5 0.207 0.297 0.154 358.185 o
5 21 7 2.198 2.057 0.113 291.423 o
6 6 6 2.055 2.141 0.271 100.878 o
6 8 6 457.642 459.116 2.591 0.255 o
6 8 8 43.593 44.278 0.466 11.211 o
6 10 6 49.638 49.029 0.536 9.187 o
6 10 8 111.180 108.812 0.621 3.289 o
6 10 10 99.978 99.187 0.909 3.200 o
6 12 6 36.826 36.389 0.545 11.946 o
6 12 8 13.719 13.150 0.222 49.402 o
6 12 10 1.218 1.238 0.139 309.179 o
6 12 12 66.943 68.697 1.017 4.265 o
6 14 6 0.931 1.025 0.241 139.294 o
6 14 8 150.608 150.066 0.966 1.859 o
6 14 10 5.751 5.699 0.294 66.343 o
6 14 12 20.603 21.227 0.527 18.174 o
6 14 14 1.129 1.091 0.231 146.220 o
6 16 6 71.180 71.626 0.811 4.898 o
6 16 8 1.772 1.891 0.161 220.544 o
6 16 10 18.299 18.133 0.334 30.064 o
6 16 12 6.004 6.269 0.267 72.140 o
6 16 14 26.310 25.982 0.494 16.753 o
6 18 6 16.744 17.250 0.334 31.764 o
6 18 8 11.235 10.950 0.246 54.088 o
6 18 10 23.335 23.149 0.378 22.690 o
6 18 12 0.007 -0.001 0.146 430.516 o
6 20 6 8.710 8.721 0.363 42.942 o
6 20 8 1.123 0.999 0.130 351.758 o
7 7 7 416.190 422.939 4.216 0.216 o
7 9 7 181.820 179.361 1.452 1.209 o
7 9 9 54.576 55.256 0.573 7.955 o
7 11 7 18.410 18.402 0.499 20.672 o
7 11 9 0.511 0.416 0.133 423.302 o
7 11 11 17.975 17.740 0.446 23.637 o
7 13 7 60.962 60.226 0.721 6.215 o
7 13 9 17.148 17.995 0.313 32.592 o
7 13 11 0.061 0.042 0.245 152.002 o
7 13 13 5.089 4.844 0.333 58.943 o
7 15 7 89.921 91.462 0.924 3.525 o
7 15 9 39.773 39.385 0.456 12.539 o
7 15 11 5.339 5.423 0.482 32.790 o
7 15 13 14.658 13.861 0.385 31.206 o
7 15 15 21.143 22.069 0.720 12.185 o
7 17 7 14.165 13.856 0.523 22.135 o
7 17 9 3.304 3.502 0.184 144.083 o
7 17 11 0.461 0.545 0.189 232.036 o
7 17 13 0.841 0.992 0.155 290.761 o
7 19 7 1.666 1.161 0.166 226.937 o
7 19 9 0.004 0.005 0.137 486.999 o
8 8 8 522.492 514.063 5.028 0.148 o
8 10 8 0.054 0.033 0.176 294.549 o
8 10 10 17.148 16.058 0.413 26.526 o
8 12 8 85.975 85.049 0.899 3.800 o
8 12 10 39.045 38.751 0.530 11.578 o
8 12 12 3.917 3.768 0.277 82.740 o
8 14 8 15.555 15.694 0.327 34.258 o
8 14 10 46.247 46.307 0.527 9.911 o
8 14 12 1.305 0.955 0.243 133.414 o
8 14 14 50.575 49.087 1.659 2.649 o
8 16 8 86.242 85.445 1.553 2.283 o
8 16 10 1.187 1.112 0.182 213.946 o
8 16 12 14.553 14.528 0.370 32.210 o
8 16 14 1.161 1.004 0.137 326.155 o
8 18 8 1.938 2.019 0.209 152.023 o
8 18 10 1.392 1.516 0.167 229.186 o
9 9 9 11.162 11.722 0.859 10.853 o
9 11 9 4.958 4.633 0.256 84.042 o
9 11 11 33.886 33.070 0.819 8.437 o
9 13 9 2.223 2.087 0.276 96.656 o
9 13 11 4.182 4.092 0.222 106.256 o
9 13 13 0.280 0.479 0.403 55.828 o
9 15 9 14.148 14.102 0.515 22.537 o
9 15 11 0.385 0.315 0.158 329.816 o
9 15 13 4.769 4.852 0.251 86.643 o
9 17 9 0.105 0.118 0.202 220.789 o
9 17 11 2.747 2.673 0.161 184.689 o
10 10 10 121.452 118.744 3.289 0.678 o
10 12 10 2.922 3.223 0.296 80.621 o
10 12 12 72.871 72.614 1.962 1.805 o
10 14 10 16.929 16.333 0.590 17.602 o
10 14 12 3.072 3.418 0.213 124.950 o
10 14 14 0.509 0.691 0.286 106.426 o
10 16 10 2.807 2.835 0.309 76.681 o
10 16 12 11.048 11.038 0.599 19.748 o
11 11 11 68.345 64.712 2.100 1.668 o
11 13 11 19.550 18.131 0.556 17.890 o
11 13 13 3.158 2.446 0.358 59.824 o
11 15 11 2.638 2.295 0.445 41.908 o
11 15 13 0.013 -0.066 0.176 298.625 o
12 12 12 3.003 3.137 0.527 30.238 o
12 14 12 12.546 11.039 0.976 8.598 o
13 13 13 0.002 0.234 0.282 114.857 o
;
_iucr_refine_instructions_details
;
TITL 2017S027_NH4B6H6_a.res in Fm-3m
CELL 0.71073 9.102951 9.102951 9.102951 90 90 90
ZERR 3.99936 0.000116 0.000116 0.000116 0 0 0
LATT 4
SYMM -X,-Y,+Z
SYMM -X,+Y,-Z
SYMM +X,-Y,-Z
SYMM +Z,+X,+Y
SYMM +Z,-X,-Y
SYMM -Z,-X,+Y
SYMM -Z,+X,-Y
SYMM +Y,+Z,+X
SYMM -Y,+Z,-X
SYMM +Y,-Z,-X
SYMM -Y,-Z,+X
SYMM +Y,+X,-Z
SYMM -Y,-X,-Z
SYMM +Y,-X,+Z
SYMM -Y,+X,+Z
SYMM +X,+Z,-Y
SYMM -X,+Z,+Y
SYMM -X,-Z,-Y
SYMM +X,-Z,+Y
SYMM +Z,+Y,-X
SYMM +Z,-Y,+X
SYMM -Z,+Y,+X
SYMM -Z,-Y,-X
SFAC B H N
DISP B 0.0006 0.0007 6.6181
DISP H 0 0 0.624
DISP N 0.0041 0.0033 19.5955
UNIT 24 56 8
L.S. 50
PLAN 1
TEMP -173.15
CONF
BOND $H
fmap 2
acta
MORE -1
LIST -3
SHEL 99 0.4
WGHT 0.01102 0.008495
FVAR 1.372809
REM
REM
REM
N1 3 0.25000 0.25000 0.25000 10.04167 0.01112 0.01112 0.01112 =
0.00000 -0.00000 -0.00000
B1 1 0.36527 0.50000 0.50000 10.12500 0.00831 0.01099 0.01099 =
0.00000 0.00000 0.00000
H1 2 0.23316 0.50000 0.50000 10.12500 0.01171 0.03794 0.03794 =
0.00000 0.00000 0.00000
H1a 2 0.31462 0.18538 0.18538 10.16667 0.03513 0.03513 0.03513 =
-0.00631 0.00631 0.00631
HKLF 4
END
Q1 1 0.266667 0.5 0.5 11 0.05 0.08
Q2 1 0 0.5 0.5 11 0.05 0.05
Q3 1 0.416667 0.5 0.5 11 0.05 0.05
Q4 1 0.388889 0.111111 0.111111 11 0.05 0.04
Q5 1 0.15 0.5 0.65 11 0.05 0.03
REM The information below was added by Olex2.
REM
REM R1 = 0.0095 for 341 Fo > 4sig(Fo) and 0.0105 for all 364 data
REM 11 parameters refined using 0 restraints
REM Highest difference peak 0.1093, deepest hole -0.0662
REM Mean Shift 0.0001, Max Shift 0.0008.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0105
REM R1_gt = 0.0095
REM wR_ref = 0.0226
REM GOOF = 0.9106
REM Shift_max = 0.0008
REM Shift_mean = 0.0001
REM Reflections_all = 364
REM Reflections_gt = 341
REM Parameters = 11
REM Hole = -0.0662
REM Peak = 0.1093
REM Flack = n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_CaF2
_database_code_depnum_ccdc_archive 'CCDC 2034386'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-09-28 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-03-13
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.03.04 svn.rc2590c38 for OlexSys, GUI svn.r6014)
;
_chemical_formula_moiety 'Ca1 F2'
_chemical_formula_sum 'Ca F2'
_chemical_formula_weight 78.075
_chemical_oxdiff_formula 'Ca F'
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_dispersion_source
Ca 0.13779 0.19369 Sasaki
F 0.00604 0.00613 Sasaki
_vrf_PLAT974_CaF2
;
PROBLEM: Check Calcd Negative Resid. Density on Ca01 -2.41 eA-3
RESPONSE: Residual densities calculated by CheckCIF are based on spherical densities
;
_vrf_PLAT112_CaF2
;
PROBLEM: ADDSYM Detects New (Pseudo) Symm. Elem 4 100 %Fit
RESPONSE: The high symmetry in SG number 225 contains all recommended symmetry elements
;
_vrf_PLAT927_CaF2
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0241 Check
RESPONSE: Statistics calculated by CheckCIF cannot account for non-spherical refinements
;
_vrf_PLAT928_CaF2
;
PROBLEM: Reported and Calculated S value Differ by . -0.949 Check
RESPONSE: Statistics calculated by CheckCIF cannot account for non-spherical refinements
;
_space_group_crystal_system cubic
_space_group_IT_number 225
_space_group_name_H-M_alt 'F m -3 m'
_space_group_name_Hall '-F 4 2 3'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x,-z,y
3 x,z,-y
4 z,y,-x
5 -z,y,x
6 -y,x,z
7 y,-x,z
8 z,x,y
9 y,z,x
10 -y,-z,x
11 z,-x,-y
12 -y,z,-x
13 -z,-x,y
14 -z,x,-y
15 y,-z,-x
16 x,-y,-z
17 -x,y,-z
18 -x,-y,z
19 y,x,-z
20 -y,-x,-z
21 z,-y,x
22 -z,-y,-x
23 -x,z,y
24 -x,-z,-y
25 -x,-y,-z
26 -x,z,-y
27 -x,-z,y
28 -z,-y,x
29 z,-y,-x
30 y,-x,-z
31 -y,x,-z
32 -z,-x,-y
33 -y,-z,-x
34 y,z,-x
35 -z,x,y
36 y,-z,x
37 z,x,-y
38 z,-x,y
39 -y,z,x
40 -x,y,z
41 x,-y,z
42 x,y,-z
43 -y,-x,z
44 y,x,z
45 -z,y,-x
46 z,y,x
47 x,-z,-y
48 x,z,y
49 x,y+1/2,z+1/2
50 x,-z+1/2,y+1/2
51 x,z+1/2,-y+1/2
52 z,y+1/2,-x+1/2
53 -z,y+1/2,x+1/2
54 -y,x+1/2,z+1/2
55 y,-x+1/2,z+1/2
56 z,x+1/2,y+1/2
57 y,z+1/2,x+1/2
58 -y,-z+1/2,x+1/2
59 z,-x+1/2,-y+1/2
60 -y,z+1/2,-x+1/2
61 -z,-x+1/2,y+1/2
62 -z,x+1/2,-y+1/2
63 y,-z+1/2,-x+1/2
64 x,-y+1/2,-z+1/2
65 -x,y+1/2,-z+1/2
66 -x,-y+1/2,z+1/2
67 y,x+1/2,-z+1/2
68 -y,-x+1/2,-z+1/2
69 z,-y+1/2,x+1/2
70 -z,-y+1/2,-x+1/2
71 -x,z+1/2,y+1/2
72 -x,-z+1/2,-y+1/2
73 -x,-y+1/2,-z+1/2
74 -x,z+1/2,-y+1/2
75 -x,-z+1/2,y+1/2
76 -z,-y+1/2,x+1/2
77 z,-y+1/2,-x+1/2
78 y,-x+1/2,-z+1/2
79 -y,x+1/2,-z+1/2
80 -z,-x+1/2,-y+1/2
81 -y,-z+1/2,-x+1/2
82 y,z+1/2,-x+1/2
83 -z,x+1/2,y+1/2
84 y,-z+1/2,x+1/2
85 z,x+1/2,-y+1/2
86 z,-x+1/2,y+1/2
87 -y,z+1/2,x+1/2
88 -x,y+1/2,z+1/2
89 x,-y+1/2,z+1/2
90 x,y+1/2,-z+1/2
91 -y,-x+1/2,z+1/2
92 y,x+1/2,z+1/2
93 -z,y+1/2,-x+1/2
94 z,y+1/2,x+1/2
95 x,-z+1/2,-y+1/2
96 x,z+1/2,y+1/2
97 x+1/2,y,z+1/2
98 x+1/2,-z,y+1/2
99 x+1/2,z,-y+1/2
100 z+1/2,y,-x+1/2
101 -z+1/2,y,x+1/2
102 -y+1/2,x,z+1/2
103 y+1/2,-x,z+1/2
104 z+1/2,x,y+1/2
105 y+1/2,z,x+1/2
106 -y+1/2,-z,x+1/2
107 z+1/2,-x,-y+1/2
108 -y+1/2,z,-x+1/2
109 -z+1/2,-x,y+1/2
110 -z+1/2,x,-y+1/2
111 y+1/2,-z,-x+1/2
112 x+1/2,-y,-z+1/2
113 -x+1/2,y,-z+1/2
114 -x+1/2,-y,z+1/2
115 y+1/2,x,-z+1/2
116 -y+1/2,-x,-z+1/2
117 z+1/2,-y,x+1/2
118 -z+1/2,-y,-x+1/2
119 -x+1/2,z,y+1/2
120 -x+1/2,-z,-y+1/2
121 -x+1/2,-y,-z+1/2
122 -x+1/2,z,-y+1/2
123 -x+1/2,-z,y+1/2
124 -z+1/2,-y,x+1/2
125 z+1/2,-y,-x+1/2
126 y+1/2,-x,-z+1/2
127 -y+1/2,x,-z+1/2
128 -z+1/2,-x,-y+1/2
129 -y+1/2,-z,-x+1/2
130 y+1/2,z,-x+1/2
131 -z+1/2,x,y+1/2
132 y+1/2,-z,x+1/2
133 z+1/2,x,-y+1/2
134 z+1/2,-x,y+1/2
135 -y+1/2,z,x+1/2
136 -x+1/2,y,z+1/2
137 x+1/2,-y,z+1/2
138 x+1/2,y,-z+1/2
139 -y+1/2,-x,z+1/2
140 y+1/2,x,z+1/2
141 -z+1/2,y,-x+1/2
142 z+1/2,y,x+1/2
143 x+1/2,-z,-y+1/2
144 x+1/2,z,y+1/2
145 x+1/2,y+1/2,z
146 x+1/2,-z+1/2,y
147 x+1/2,z+1/2,-y
148 z+1/2,y+1/2,-x
149 -z+1/2,y+1/2,x
150 -y+1/2,x+1/2,z
151 y+1/2,-x+1/2,z
152 z+1/2,x+1/2,y
153 y+1/2,z+1/2,x
154 -y+1/2,-z+1/2,x
155 z+1/2,-x+1/2,-y
156 -y+1/2,z+1/2,-x
157 -z+1/2,-x+1/2,y
158 -z+1/2,x+1/2,-y
159 y+1/2,-z+1/2,-x
160 x+1/2,-y+1/2,-z
161 -x+1/2,y+1/2,-z
162 -x+1/2,-y+1/2,z
163 y+1/2,x+1/2,-z
164 -y+1/2,-x+1/2,-z
165 z+1/2,-y+1/2,x
166 -z+1/2,-y+1/2,-x
167 -x+1/2,z+1/2,y
168 -x+1/2,-z+1/2,-y
169 -x+1/2,-y+1/2,-z
170 -x+1/2,z+1/2,-y
171 -x+1/2,-z+1/2,y
172 -z+1/2,-y+1/2,x
173 z+1/2,-y+1/2,-x
174 y+1/2,-x+1/2,-z
175 -y+1/2,x+1/2,-z
176 -z+1/2,-x+1/2,-y
177 -y+1/2,-z+1/2,-x
178 y+1/2,z+1/2,-x
179 -z+1/2,x+1/2,y
180 y+1/2,-z+1/2,x
181 z+1/2,x+1/2,-y
182 z+1/2,-x+1/2,y
183 -y+1/2,z+1/2,x
184 -x+1/2,y+1/2,z
185 x+1/2,-y+1/2,z
186 x+1/2,y+1/2,-z
187 -y+1/2,-x+1/2,z
188 y+1/2,x+1/2,z
189 -z+1/2,y+1/2,-x
190 z+1/2,y+1/2,x
191 x+1/2,-z+1/2,-y
192 x+1/2,z+1/2,y
_symmetry_Int_Tables_number 225
_cell_length_a 5.45095(5)
_cell_length_b 5.45095(5)
_cell_length_c 5.45095(5)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 161.963(3)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 6248
_cell_measurement_temperature 100.0(10)
_cell_measurement_theta_max 65.6870
_cell_measurement_theta_min 5.0900
_exptl_crystal_description block
_exptl_absorpt_coefficient_mu 1.747
_exptl_absorpt_correction_T_max 0.895
_exptl_absorpt_correction_T_min 0.776
_exptl_absorpt_correction_type analytical
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019)
Analytical numeric absorption correction using a multifaceted crystal
model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_density_diffrn 3.202
_exptl_crystal_F_000 152.597
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
2 -1 1 0.1314
0 -1 0 0.1160
-1 -2 2 0.0676
1 0 1 0.1219
1 0 2 0.1147
0 2 1 0.1446
1 2 -1 0.0891
1 2 2 0.1164
0 0 -1 0.1362
2 1 2 0.1044
-2 1 -2 0.0900
-1 -2 -2 0.1498
1 1 -1 0.0643
-1 1 -1 0.0693
1 2 -2 0.0676
0 0 1 0.0947
-2 -1 2 0.0573
1 -2 -1 0.1285
1 -2 0 0.1096
1 -2 1 0.1020
-2 1 -1 0.0731
-1 -2 1 0.0617
1 1 1 0.0946
-2 -1 1 0.0470
-1 2 -2 0.0640
-1 -1 1 0.0403
2 1 -1 0.0576
1 1 2 0.0989
_exptl_crystal_size_max 0.304
_exptl_crystal_size_mid 0.205
_exptl_crystal_size_min 0.105
loop_
_exptl_oxdiff_crystal_face_indexfrac_h
_exptl_oxdiff_crystal_face_indexfrac_k
_exptl_oxdiff_crystal_face_indexfrac_l
_exptl_oxdiff_crystal_face_x
_exptl_oxdiff_crystal_face_y
_exptl_oxdiff_crystal_face_z
1.9980 -0.9956 1.0082 0.2453 0.0521 -0.0151
0.0005 -0.9990 0.0055 0.0382 0.0457 0.0833
-1.0010 -1.9945 2.0089 0.0276 0.2969 0.0768
0.9981 0.0027 1.0013 0.1145 0.0449 -0.0771
0.9969 0.0048 2.0010 0.1364 0.1283 -0.1327
-0.0022 2.0001 0.9889 -0.0546 -0.0080 -0.2224
0.9998 1.9966 -1.0092 -0.0057 -0.2134 -0.1324
0.9960 2.0028 1.9901 0.0599 0.0369 -0.2994
0.0013 -0.0021 -0.9998 -0.0219 -0.0834 0.0557
1.9958 1.0044 1.9971 0.1908 0.0440 -0.2375
-1.9967 0.9935 -2.0080 -0.2672 -0.1355 0.0708
-0.9960 -2.0028 -1.9901 -0.0599 -0.0369 0.2994
1.0002 0.9976 -1.0037 0.0325 -0.1677 -0.0491
-0.9986 0.9963 -1.0067 -0.1527 -0.0906 -0.0063
1.0010 1.9945 -2.0089 -0.0276 -0.2969 -0.0768
-0.0013 0.0021 0.9998 0.0219 0.0834 -0.0557
-2.0009 -0.9962 2.0020 -0.1032 0.2897 0.0148
1.0016 -1.9994 -0.9874 0.1472 -0.0305 0.2010
1.0003 -1.9973 0.0124 0.1691 0.0529 0.1453
0.9990 -1.9953 1.0122 0.1910 0.1363 0.0896
-1.9980 0.9956 -1.0082 -0.2453 -0.0521 0.0151
-0.9998 -1.9966 1.0092 0.0057 0.2134 0.1324
0.9977 1.0017 0.9958 0.0763 -0.0008 -0.1604
-1.9996 -0.9982 1.0022 -0.1251 0.2063 0.0705
-0.9978 1.9932 -2.0119 -0.2128 -0.2198 -0.0340
-1.0002 -0.9976 1.0037 -0.0325 0.1677 0.0491
1.9996 0.9982 -1.0022 0.1251 -0.2063 -0.0705
0.9964 1.0038 1.9956 0.0981 0.0826 -0.2161
_diffrn_reflns_av_R_equivalents 0.0673
_diffrn_reflns_av_unetI/netI 0.0117
_diffrn_reflns_Laue_measured_fraction_full 1.0000
_diffrn_reflns_Laue_measured_fraction_max 1.0000
_diffrn_reflns_limit_h_max 13
_diffrn_reflns_limit_h_min -13
_diffrn_reflns_limit_k_max 13
_diffrn_reflns_limit_k_min -13
_diffrn_reflns_limit_l_max 13
_diffrn_reflns_limit_l_min -13
_diffrn_reflns_number 5299
_diffrn_reflns_point_group_measured_fraction_full 1.0000
_diffrn_reflns_point_group_measured_fraction_max 1.0000
_diffrn_reflns_theta_full 19.6651
_diffrn_reflns_theta_max 44.26
_diffrn_reflns_theta_min 5.11
_diffrn_ambient_environment N~2~
_diffrn_ambient_temperature 99.97(10)
_diffrn_detector 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type HyPix
_diffrn_measured_fraction_theta_full 1.0000
_diffrn_measured_fraction_theta_max 1.0000
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):
# Type Start End Width t~exp~ \w \q \k \f Frames
#--------------------------------------------------------------------------
1 \w -18.00 73.00 1.00 5.00 -- 0.00 65.00-147.00 91
2 \w 74.00 149.00 1.00 20.00 -- 86.25 47.00 -55.00 75
3 \w 82.00 149.00 1.00 20.00 -- 86.25 110.00 24.00 67
4 \w 74.00 149.00 1.00 20.00 -- 86.25 19.00 150.00 75
5 \w 74.00 149.00 1.00 20.00 -- 86.25 19.00 30.00 75
6 \w 72.00 149.00 1.00 20.00 -- 86.25 57.00-120.00 77
7 \w 74.00 149.00 1.00 20.00 -- 86.25 37.00-150.00 75
8 \w 72.00 149.00 1.00 20.00 -- 86.25 57.00 -30.00 77
9 \w 72.00 149.00 1.00 20.00 -- 86.25 57.00 60.00 77
10 \w 72.00 149.00 1.00 20.00 -- 86.25 57.00 150.00 77
11 \w 14.00 53.00 1.00 20.00 -- 86.25 -65.00 76.00 39
12 \w 14.00 81.00 1.00 20.00 -- 86.25 -99.00 0.00 67
13 \w 14.00 81.00 1.00 20.00 -- 86.25 -77.00 12.00 67
14 \w 14.00 41.00 1.00 20.00 -- 86.25 -57.00 150.00 27
15 \w 14.00 115.00 1.00 20.00 -- 86.25 -88.00 136.03 101
16 \w 14.00 41.00 1.00 20.00 -- 86.25 -57.00 -90.00 27
17 \w 14.00 41.00 1.00 20.00 -- 86.25 -57.00-150.00 27
18 \w 14.00 41.00 1.00 20.00 -- 86.25 -57.00-180.00 27
19 \w 14.00 114.00 1.00 20.00 -- 86.25 -87.00-107.96 100
20 \w -12.00 76.00 1.00 5.00 -- 0.00 19.00 150.00 88
21 \w -12.00 60.00 1.00 5.00 -- 0.00 19.00 90.00 72
22 \w -22.00 34.00 1.00 5.00 -- 0.00 -99.00 60.00 56
23 \w -22.00 34.00 1.00 5.00 -- 0.00 -99.00 120.00 56
24 \w -42.00 -12.00 1.00 20.00 -- -40.25 -88.00 160.39 30
25 \w -41.00 -10.00 1.00 20.00 -- -40.25 -92.00 78.08 31
26 \w -75.00 -50.00 1.00 40.00 -- -40.25 110.00 24.00 25
27 \w 91.00 116.00 1.00 40.00 -- 86.25 110.00 24.00 25
;
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_measurement_method '\w scans'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11 0.0926552000
_diffrn_orient_matrix_UB_12 -0.0381070000
_diffrn_orient_matrix_UB_13 0.0220841000
_diffrn_orient_matrix_UB_21 -0.0386687000
_diffrn_orient_matrix_UB_22 -0.0453312000
_diffrn_orient_matrix_UB_23 0.0834962000
_diffrn_orient_matrix_UB_31 -0.0212714000
_diffrn_orient_matrix_UB_32 -0.0837436000
_diffrn_orient_matrix_UB_33 -0.0555333000
_diffrn_radiation_monochromator mirror
_diffrn_radiation_probe x-ray
_diffrn_radiation_type 'Ag K\a'
_diffrn_radiation_wavelength 0.56087
_diffrn_source 'micro-focus sealed X-ray tube'
_diffrn_source_type 'PhotonJet (Ag) X-ray Source'
_reflns_Friedel_coverage 0.0
_reflns_limit_h_max 7
_reflns_limit_h_min 0
_reflns_limit_k_max 13
_reflns_limit_k_min 1
_reflns_limit_l_max 9
_reflns_limit_l_min 0
_reflns_number_gt 96
_reflns_number_total 96
_reflns_odcompleteness_completeness 95.02
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta 44.37
_reflns_threshold_expression I>=2u(I)
_computing_cell_refinement 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_collection 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_reduction 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_refine_diff_density_max 0.6860
_refine_diff_density_min -0.4146
_refine_diff_density_rms 0.0898
_refine_ls_d_res_high 0.4018
_refine_ls_d_res_low 3.1471
_refine_ls_goodness_of_fit_ref 1.0864
_refine_ls_hydrogen_treatment undef
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 3
_refine_ls_number_reflns 96
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0114
_refine_ls_R_factor_gt 0.0114
_refine_ls_restrained_S_all 1.0864
_refine_ls_shift/su_max 0.0000
_refine_ls_shift/su_mean 0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0175P)^2^+0.0607P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0279
_refine_ls_wR_factor_ref 0.0279
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be published - 2020
NoSpherA2 implementation of HAR makes use of
tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or DFT using selected funtionals
- for a fragment of the crystal.
This fregment can be embedded in an electrostatic crystal field by employing cluster charges.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
INT ACCURACY: High
METHOD: PBE
BASIS SET: def2-TZVPP
CHARGE: 18
MULTIPLICITY: 1
DATE: 2020-06-17_15-21-20
;
_olex2_refinement_description
;
;
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Ca01 Ca 0.5 0.5 0.5 0.00334(4) Uani 0.999840 48 S T P
F002 F 0.25 0.75 0.75 0.00505(6) Uani 1.000080 24 S T P
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Ca01 0.00334(4) 0.00334(4) 0.00334(4) -0.000000 -0.000000 0.000000
F002 0.00505(6) 0.00505(6) 0.00505(6) -0.000000 -0.000000 0.000000
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ca01 Ca01 3.85440(3) 49_554 ?
Ca01 F002 2.360331(12) 1_555 ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F002 Ca01 Ca01 144.7356(3) 49_544 97 ?
F002 Ca01 Ca01 35.2644(3) 57_545 97 ?
F002 Ca01 F002 70.5288(6) 56_554 52_545 ?
F002 Ca01 F002 109.4712(6) 57_545 56_554 ?
Ca01 F002 Ca01 109.4712(6) 59_566 11_566 ?
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
_diffrn_refln_scale_group_code
1 1 -1 131655 752.309 22
-1 -1 1 130983 431.837 26
1 -1 -1 143571 1048.63 1
1 -1 1 135525 1088.91 20
-1 1 -1 127516 768.201 22
1 1 1 130537 974.744 1
1 -1 -1 143833 1058.53 21
0 0 -2 152.191 26.9979 23
0 0 2 198.079 29.5982 23
0 0 -2 213.969 39.3622 1
0 2 0 167.911 37.5769 1
2 0 0 149.465 30.0849 20
2 0 0 203.993 37.0365 21
-2 0 0 197.235 42.0694 22
2 0 0 154.438 36.199 23
0 2 0 182.594 31.1441 20
-2 2 0 298353 1794.77 22
2 2 0 300498 1902.63 22
2 0 -2 320514 2284.26 21
0 -2 -2 291860 1739.17 21
2 0 2 260222 1898.13 20
2 2 0 275170 1556.2 1
-2 0 2 320778 1647.06 1
2 0 -2 305286 1610.65 1
0 2 2 310922 2081.54 1
2 -2 0 282089 1970.54 20
0 2 2 337773 1900.59 21
2 0 2 310272 1116.86 24
-2 0 -2 297957 1928.29 20
-2 0 -2 284992 1891.04 23
0 2 -2 302210 2107.35 20
2 -2 2 1984.21 183.451 20
-2 -2 2 1902.74 51.7518 26
2 -2 2 1883.61 63.5295 25
-2 -2 -2 1579.52 102.963 20
-2 -2 2 1846.91 113.551 22
-2 -2 -2 1926.82 52.8002 26
2 2 -2 1987.52 39.5822 25
2 -2 -2 2026.58 174.407 1
2 -2 2 1861.38 115.971 22
2 2 -2 1761.16 153.741 20
-2 2 2 2255.52 178.729 21
2 2 2 1860.02 162.431 1
1 -3 1 78764.9 942.837 1
-1 1 3 76043.6 961.094 1
1 -3 -1 76187.7 1021.4 21
-1 -3 1 50706.5 824.716 20
3 -1 -1 76876.6 1056.41 21
-1 -1 3 72506.8 699.651 1
-3 -1 -1 58852.9 565.508 21
1 3 -1 71372.9 665.521 22
1 -3 -1 71628.4 889.601 20
-3 1 -1 77891.3 1031.45 21
3 1 -1 64680.6 403.972 25
-1 1 3 71243 414.169 24
-3 1 1 74261.6 974.253 22
3 -1 -1 67031 457.081 25
-1 3 1 74846.9 1065.38 1
-1 -3 -1 77898.3 631.251 20
3 1 1 69485 712.864 20
-1 3 1 73494.5 978.445 21
-1 -3 -1 67796.5 915.447 1
3 1 -1 74373.1 910.19 21
1 1 -3 68815.3 1089.17 20
-1 1 -3 69640.9 820.559 23
-1 -1 -3 65787 946.181 20
3 1 1 71268.8 933.046 23
1 3 1 71842 947.368 1
3 1 -1 71085.8 909.826 22
1 3 1 75474.6 749.235 21
-3 1 -1 67430.1 894.217 22
1 1 3 74367.6 899.402 23
3 -1 1 77633.6 1029.25 20
-3 1 1 63150.3 737.976 23
1 -1 -3 72030.7 948.973 1
-1 3 -1 73525.6 623.142 22
-1 -3 1 68967.1 707.845 1
1 3 -1 68363.6 812.904 20
3 1 -1 68926.1 749.028 23
1 1 -3 66318.8 529.739 23
-1 3 -1 73012 1003.7 20
3 -1 -1 72923.1 930.514 1
1 -1 3 67440.4 1085.37 20
-1 3 -3 47072.8 986.347 20
-3 1 3 39945.2 433.991 23
3 3 1 43323.5 770.627 1
-3 1 3 55761.8 826.822 1
3 1 3 43458.1 882.241 1
3 -1 -3 51550.5 1001.89 21
-1 -3 -3 47907.5 688.684 21
3 1 3 39981.7 769.965 20
-3 -1 3 53122.5 827.67 22
3 3 -1 46543.7 755.894 22
-3 3 1 50226.7 856.526 22
3 3 -1 47934.6 536.282 1
-3 1 -3 46281.9 856.011 23
3 1 -3 57189.8 1069.8 21
3 3 -1 35852.4 592.482 20
3 -3 -1 51426.1 959.925 1
3 3 1 52182.4 940.223 22
-3 -1 -3 42907 862.054 23
1 3 -3 45387.9 908.479 20
1 -3 -3 47750.1 958.089 1
-3 -3 1 46292.3 335.436 26
3 -3 -1 45364 967.062 21
1 -3 -3 46357 872.743 21
-1 3 3 52252.7 944.866 21
3 1 3 49118.2 457.595 24
3 1 -3 37272.2 507.643 1
3 -3 1 48083.1 971.637 20
1 3 3 46907.8 921.335 1
3 -1 3 45719.7 953.357 20
3 -1 -3 46162.4 808.055 1
-3 3 -1 43697.8 715.463 22
-3 -1 -3 46409.9 817.712 20
3 3 -3 29821.1 797.247 20
-3 3 3 38310.9 926.06 21
3 -3 3 33910.1 352.001 25
-3 3 3 37185.8 853.511 1
3 -3 3 36077.5 610.835 22
3 -3 -3 34592.6 847.744 1
-3 3 3 30800.6 225.271 24
3 3 3 35419.1 859.009 1
-3 -3 3 32755.7 576.06 22
3 -3 3 36406.7 980.413 20
-3 -3 -3 30640.1 516.046 20
-3 3 -3 32308.9 800.72 23
4 0 0 156207 1429.57 23
0 -4 0 175400 1591.34 20
0 0 4 174137 1194.15 23
0 4 0 172032 1629.01 21
0 0 -4 167442 1257.11 23
-4 0 0 151917 1484.53 23
-4 0 0 154648 1419.56 21
0 4 0 153309 1544.71 1
4 0 0 165301 1534.18 21
0 -4 0 172863 1621.45 1
-4 0 0 159329 1579.46 22
0 0 4 170222 1547.64 1
4 0 0 157172 835.238 25
4 0 0 174846 1475.41 20
0 -4 2 2841.64 234.582 20
0 -4 2 3197.45 198.605 1
4 -2 0 3177.36 231.588 20
0 -2 -4 3354.23 238.141 1
-4 2 0 2794.1 227.351 21
2 4 0 3118.19 191.039 1
4 0 2 2823.9 206.857 20
2 0 -4 3859.2 284.932 21
0 2 4 3312.29 204.625 23
4 0 -2 3336.13 103.486 25
-4 2 0 3330.07 223.416 22
2 -4 0 3405.77 246.365 20
4 0 -2 3079.9 187.629 1
0 4 2 3542.46 251.451 1
-2 0 4 3225.69 197.607 1
-4 0 -2 3009.24 192.13 21
0 -2 4 3132.84 187.884 1
2 0 4 3060.16 113.253 24
4 2 0 3256.5 166.41 21
-4 2 0 2657.32 199.995 23
-2 4 0 3377.58 259.105 21
0 4 -2 3033.65 221.213 20
4 0 2 3104.96 222.394 23
-2 0 -4 2898.72 208.535 23
4 0 2 2920.27 97.0341 24
4 2 0 3332.92 140.559 20
-4 0 2 2726.97 146.968 23
4 2 0 3119.84 228.178 22
2 0 -4 3128.36 191.16 1
4 0 -2 3460.69 248.433 21
0 2 -4 2945.94 174.535 23
0 2 -4 3158.85 259.823 20
4 -2 0 2829.3 242.26 21
4 2 0 3003.92 214.603 23
-2 -4 0 2798.08 178.678 1
4 2 0 2507.3 172.68 1
-4 0 -2 2978.96 207.256 20
0 4 2 3002.51 196.082 21
0 -2 -4 3254.83 217.253 21
0 -4 -2 2843.36 213.493 21
4 2 2 120442 1556.17 22
2 -2 4 124411 1143.26 22
-2 -4 -2 107084 727.861 20
-2 -4 2 67931.5 663.166 1
4 2 -2 124037 1513.26 21
4 -2 -2 118021 1451.74 1
2 2 4 113231 1474.67 23
4 -2 -2 115755 1591.08 21
-2 2 4 129957 1501.52 1
-4 2 -2 105523 1467.38 21
4 2 2 94361.2 1365.7 1
-2 -2 4 123007 1116.2 22
4 -2 2 104389 703.627 25
2 2 -4 108883 1589.04 20
2 4 -2 98184.6 1168.62 20
-2 -2 4 126089 824.816 1
2 -4 -2 117524 1590.75 1
2 -4 -2 108617 1487.74 21
4 -2 2 109674 1532.87 20
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-1 -13 -1 4900.51 308.91 19
1 -13 1 5272.93 291.496 19
1 -1 -13 5152.2 279.215 8
1 -13 -1 4858.33 302.387 19
-1 1 -13 5436.72 259.882 8
1 1 -13 5312.1 276.854 8
-1 1 13 4837.82 304.482 4
-1 -13 -1 4551.03 293.668 17
1 -13 -1 4884.22 293.136 17
1 1 13 4440.44 278.477 4
1 1 -13 4911.02 290.216 2
-1 -1 13 4886.84 322.82 4
1 -1 13 4723.05 310.593 4
-13 1 -1 3773.95 254.62 13
-13 1 1 3735.77 252.692 13
-13 1 1 3387.85 214.546 12
-13 -1 1 3879.99 246.363 12
-1 -13 1 5209.75 317.983 3
-1 13 -1 4881.68 259.184 6
1 13 -1 5140.68 238.041 6
-13 -1 -1 1300.18 110.685 11
-1 13 1 5093.24 272.648 6
-13 -1 1 4891.35 194.979 26
-13 -1 -1 4895.42 193.642 26
1 13 1 5466.98 261.237 6
-13 1 -1 4319.54 234.761 11
-13 1 1 1450.19 120.878 11
1 -13 1 5126.24 317.416 3
-1 1 13 4648.28 303.543 10
1 1 13 4942.22 311.961 10
-1 -13 1 4562.02 268.541 9
1 -13 1 4761.9 286.213 9
1 -13 -1 4517.87 247.292 9
-1 -1 -13 4916.15 222.898 5
1 -1 -13 4988.21 258.104 5
-3 -1 -13 4144.46 257.42 2
3 -1 -13 4581.87 277.697 2
-1 -3 -13 4740.12 272.019 8
-3 -1 -13 5329.09 243.893 8
-1 -13 3 4724.24 267.121 19
-3 -13 1 4600.01 303.609 19
1 -3 -13 4785.28 289.623 8
-1 3 13 4354.26 270.892 4
-3 -13 -1 4476.64 311.942 19
1 -13 3 4940.92 257.712 19
-3 1 13 4469.64 301.427 4
-3 1 -13 4963.31 217.028 8
1 3 13 4176.77 245.971 4
3 -13 1 4806.31 266.791 19
1 -13 -3 4515.58 307.223 19
3 -13 -1 4717.43 292.176 19
-3 -1 13 4425.74 305.01 4
-3 1 -13 4824.92 273.403 2
3 1 -13 4882.28 282.734 2
-1 3 -13 4628.75 234.695 8
1 3 -13 4725.82 260.133 8
3 -13 -1 4347.79 265.654 17
1 -13 -3 4076.06 277.196 17
3 1 13 3979.95 249.193 4
-1 -3 13 4618.85 325.027 4
-3 -13 -1 4177.64 226.645 16
-3 -13 1 4365.02 273.106 16
-3 -13 -1 2721.26 273.308 15
-1 -13 -3 2456.8 268.63 15
3 -1 13 4250.97 285.312 4
1 3 -13 4672.67 284.748 2
-3 13 1 4048.24 197.476 7
1 -3 13 4679.68 323.598 4
-3 -1 -13 4599.58 251.488 15
-3 1 -13 4675.28 255.233 15
-1 3 -13 4943.86 234.878 15
1 -3 -13 4451.74 271.804 14
-13 1 -3 3400.72 247.871 13
-13 3 -1 3279.94 232.607 13
-13 -3 -1 3461.43 239.797 13
-13 3 1 3162.82 228.788 13
-13 -3 1 3514.1 242.815 13
-13 1 3 3641.97 250.263 13
-13 -3 -1 3201.55 245.254 12
-13 1 3 3112.17 197.682 12
-13 -3 1 3693.73 253.864 12
-13 -1 3 3409.35 225.13 12
-3 -13 1 4572.66 303.835 3
-1 13 -3 4217.69 229.586 6
-1 -13 3 4666.12 290.49 3
-1 -13 -3 4584.1 284.712 3
-3 13 -1 4334.3 265.701 6
-3 13 1 4708.58 278.54 6
3 -13 1 4312.3 200.656 27
-13 -1 -3 3568.29 213.796 11
-13 1 -3 4246.98 254.043 11
3 13 1 4550.94 213.662 6
-13 -1 3 4540.76 180.51 26
-13 -1 -3 4544.92 172.252 26
1 -13 3 4648.13 290.575 3
1 -13 -3 4481.16 282.978 3
-13 -3 1 4414 179.435 26
-13 -3 -1 4451.93 178.527 26
-1 13 3 4497.03 269.272 6
-13 3 -1 4240.95 259.719 11
1 13 3 4330.94 253.011 6
13 1 3 4035.35 236.914 25
13 3 1 3742.41 212.198 25
3 -13 1 4328.27 288.129 3
-3 1 13 4608.05 302.064 10
-1 3 13 4469.65 287.723 10
-1 -3 13 4712.96 308.212 10
1 3 13 4403.8 280.895 10
1 -3 13 4586.96 306.983 10
3 1 13 4478.97 306.346 10
3 -1 13 4512.37 314.155 10
1 -13 3 4517.8 301.481 9
3 -13 1 4452.33 283.866 9
3 -13 -1 4098.56 250.811 9
1 -3 -13 4515.63 240.502 5
-13 -3 -1 5077.84 233.08 19
-13 -3 1 4879.82 257.711 19
3 -1 -13 4676.43 275.535 5
13 -3 1 4235.41 275.05 9
_iucr_refine_fcf_details
;
data_CaF2_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x,-z,y
3 x,z,-y
4 z,y,-x
5 -z,y,x
6 -y,x,z
7 y,-x,z
8 z,x,y
9 y,z,x
10 -y,-z,x
11 z,-x,-y
12 -y,z,-x
13 -z,-x,y
14 -z,x,-y
15 y,-z,-x
16 x,-y,-z
17 -x,y,-z
18 -x,-y,z
19 y,x,-z
20 -y,-x,-z
21 z,-y,x
22 -z,-y,-x
23 -x,z,y
24 -x,-z,-y
25 -x,-y,-z
26 -x,z,-y
27 -x,-z,y
28 -z,-y,x
29 z,-y,-x
30 y,-x,-z
31 -y,x,-z
32 -z,-x,-y
33 -y,-z,-x
34 y,z,-x
35 -z,x,y
36 y,-z,x
37 z,x,-y
38 z,-x,y
39 -y,z,x
40 -x,y,z
41 x,-y,z
42 x,y,-z
43 -y,-x,z
44 y,x,z
45 -z,y,-x
46 z,y,x
47 x,-z,-y
48 x,z,y
49 x,y+1/2,z+1/2
50 x,-z+1/2,y+1/2
51 x,z+1/2,-y+1/2
52 z,y+1/2,-x+1/2
53 -z,y+1/2,x+1/2
54 -y,x+1/2,z+1/2
55 y,-x+1/2,z+1/2
56 z,x+1/2,y+1/2
57 y,z+1/2,x+1/2
58 -y,-z+1/2,x+1/2
59 z,-x+1/2,-y+1/2
60 -y,z+1/2,-x+1/2
61 -z,-x+1/2,y+1/2
62 -z,x+1/2,-y+1/2
63 y,-z+1/2,-x+1/2
64 x,-y+1/2,-z+1/2
65 -x,y+1/2,-z+1/2
66 -x,-y+1/2,z+1/2
67 y,x+1/2,-z+1/2
68 -y,-x+1/2,-z+1/2
69 z,-y+1/2,x+1/2
70 -z,-y+1/2,-x+1/2
71 -x,z+1/2,y+1/2
72 -x,-z+1/2,-y+1/2
73 -x,-y+1/2,-z+1/2
74 -x,z+1/2,-y+1/2
75 -x,-z+1/2,y+1/2
76 -z,-y+1/2,x+1/2
77 z,-y+1/2,-x+1/2
78 y,-x+1/2,-z+1/2
79 -y,x+1/2,-z+1/2
80 -z,-x+1/2,-y+1/2
81 -y,-z+1/2,-x+1/2
82 y,z+1/2,-x+1/2
83 -z,x+1/2,y+1/2
84 y,-z+1/2,x+1/2
85 z,x+1/2,-y+1/2
86 z,-x+1/2,y+1/2
87 -y,z+1/2,x+1/2
88 -x,y+1/2,z+1/2
89 x,-y+1/2,z+1/2
90 x,y+1/2,-z+1/2
91 -y,-x+1/2,z+1/2
92 y,x+1/2,z+1/2
93 -z,y+1/2,-x+1/2
94 z,y+1/2,x+1/2
95 x,-z+1/2,-y+1/2
96 x,z+1/2,y+1/2
97 x+1/2,y,z+1/2
98 x+1/2,-z,y+1/2
99 x+1/2,z,-y+1/2
100 z+1/2,y,-x+1/2
101 -z+1/2,y,x+1/2
102 -y+1/2,x,z+1/2
103 y+1/2,-x,z+1/2
104 z+1/2,x,y+1/2
105 y+1/2,z,x+1/2
106 -y+1/2,-z,x+1/2
107 z+1/2,-x,-y+1/2
108 -y+1/2,z,-x+1/2
109 -z+1/2,-x,y+1/2
110 -z+1/2,x,-y+1/2
111 y+1/2,-z,-x+1/2
112 x+1/2,-y,-z+1/2
113 -x+1/2,y,-z+1/2
114 -x+1/2,-y,z+1/2
115 y+1/2,x,-z+1/2
116 -y+1/2,-x,-z+1/2
117 z+1/2,-y,x+1/2
118 -z+1/2,-y,-x+1/2
119 -x+1/2,z,y+1/2
120 -x+1/2,-z,-y+1/2
121 -x+1/2,-y,-z+1/2
122 -x+1/2,z,-y+1/2
123 -x+1/2,-z,y+1/2
124 -z+1/2,-y,x+1/2
125 z+1/2,-y,-x+1/2
126 y+1/2,-x,-z+1/2
127 -y+1/2,x,-z+1/2
128 -z+1/2,-x,-y+1/2
129 -y+1/2,-z,-x+1/2
130 y+1/2,z,-x+1/2
131 -z+1/2,x,y+1/2
132 y+1/2,-z,x+1/2
133 z+1/2,x,-y+1/2
134 z+1/2,-x,y+1/2
135 -y+1/2,z,x+1/2
136 -x+1/2,y,z+1/2
137 x+1/2,-y,z+1/2
138 x+1/2,y,-z+1/2
139 -y+1/2,-x,z+1/2
140 y+1/2,x,z+1/2
141 -z+1/2,y,-x+1/2
142 z+1/2,y,x+1/2
143 x+1/2,-z,-y+1/2
144 x+1/2,z,y+1/2
145 x+1/2,y+1/2,z
146 x+1/2,-z+1/2,y
147 x+1/2,z+1/2,-y
148 z+1/2,y+1/2,-x
149 -z+1/2,y+1/2,x
150 -y+1/2,x+1/2,z
151 y+1/2,-x+1/2,z
152 z+1/2,x+1/2,y
153 y+1/2,z+1/2,x
154 -y+1/2,-z+1/2,x
155 z+1/2,-x+1/2,-y
156 -y+1/2,z+1/2,-x
157 -z+1/2,-x+1/2,y
158 -z+1/2,x+1/2,-y
159 y+1/2,-z+1/2,-x
160 x+1/2,-y+1/2,-z
161 -x+1/2,y+1/2,-z
162 -x+1/2,-y+1/2,z
163 y+1/2,x+1/2,-z
164 -y+1/2,-x+1/2,-z
165 z+1/2,-y+1/2,x
166 -z+1/2,-y+1/2,-x
167 -x+1/2,z+1/2,y
168 -x+1/2,-z+1/2,-y
169 -x+1/2,-y+1/2,-z
170 -x+1/2,z+1/2,-y
171 -x+1/2,-z+1/2,y
172 -z+1/2,-y+1/2,x
173 z+1/2,-y+1/2,-x
174 y+1/2,-x+1/2,-z
175 -y+1/2,x+1/2,-z
176 -z+1/2,-x+1/2,-y
177 -y+1/2,-z+1/2,-x
178 y+1/2,z+1/2,-x
179 -z+1/2,x+1/2,y
180 y+1/2,-z+1/2,x
181 z+1/2,x+1/2,-y
182 z+1/2,-x+1/2,y
183 -y+1/2,z+1/2,x
184 -x+1/2,y+1/2,z
185 x+1/2,-y+1/2,z
186 x+1/2,y+1/2,-z
187 -y+1/2,-x+1/2,z
188 y+1/2,x+1/2,z
189 -z+1/2,y+1/2,-x
190 z+1/2,y+1/2,x
191 x+1/2,-z+1/2,-y
192 x+1/2,z+1/2,y
_space_group_crystal_system cubic
_space_group_IT_number 225
_space_group_name_H-M_alt 'F m -3 m'
_space_group_name_Hall '-F 4 2 3'
_symmetry_space_group_name_H-M 'F m -3 m'
_symmetry_space_group_name_Hall '-F 4 2 3'
_symmetry_Int_Tables_number 225
_cell_length_a 5.45095(5)
_cell_length_b 5.45095(5)
_cell_length_c 5.45095(5)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 161.963(3)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
0 2 0 5.265 5.566 0.316 2769.580 o
0 2 2 9186.320 9364.950 128.109 0.028 o
0 4 0 5092.310 5134.860 67.439 0.094 o
0 4 2 88.484 96.162 0.999 132.758 o
0 4 4 2528.640 2595.450 32.130 0.378 o
0 6 0 120.209 116.319 2.748 62.988 o
0 6 2 2012.960 1956.620 28.032 0.566 o
0 6 4 128.956 128.767 1.375 81.281 o
0 6 6 1112.060 1067.520 9.658 2.277 o
0 8 0 1245.200 1264.500 30.461 0.811 o
0 8 2 119.228 119.667 1.563 85.611 o
0 8 4 977.298 975.355 5.251 3.175 o
0 8 6 85.921 87.797 0.726 149.026 o
0 8 8 546.323 522.519 6.766 7.195 o
0 10 0 87.724 90.633 1.292 127.144 o
0 10 2 713.820 732.933 4.080 5.490 o
0 10 4 73.611 73.728 0.763 179.231 o
0 10 6 486.037 483.374 4.195 10.101 o
0 10 8 34.719 35.821 0.777 386.858 o
0 12 0 440.373 442.919 9.386 6.893 o
0 12 2 48.592 48.944 0.659 292.202 o
0 12 4 360.031 377.398 3.783 15.526 o
0 12 6 30.025 22.398 1.478 294.579 o
1 1 1 3919.510 4118.570 67.241 0.125 o
1 3 1 2099.420 2189.730 17.306 0.662 o
1 3 3 1405.750 1443.530 18.617 1.147 o
1 5 1 1061.770 1031.380 11.976 2.204 o
1 5 3 867.927 879.289 7.456 3.527 o
1 5 5 651.871 641.182 7.205 5.470 o
1 7 1 649.537 655.079 6.671 5.623 o
1 7 3 579.321 567.025 3.993 7.907 o
1 7 5 467.548 458.898 2.424 12.009 o
1 7 7 342.872 337.657 1.796 20.201 o
1 9 1 419.461 426.004 4.403 12.102 o
1 9 3 378.638 383.344 1.736 17.103 o
1 9 5 305.014 310.543 1.245 24.553 o
1 9 7 230.105 226.617 1.647 36.841 o
1 9 9 157.651 154.710 2.348 53.379 o
1 11 1 251.852 261.177 1.952 30.701 o
1 11 3 228.723 235.718 1.473 36.974 o
1 11 5 189.844 193.206 1.409 48.628 o
1 11 7 143.917 140.683 1.699 67.576 o
1 13 1 139.773 140.324 3.088 50.063 o
1 13 3 129.471 134.555 1.297 80.691 o
2 2 2 55.515 60.351 0.909 227.312 o
2 4 2 3402.180 3331.140 45.820 0.207 o
2 4 4 120.579 117.858 1.969 77.491 o
2 6 2 126.827 124.999 1.703 77.930 o
2 6 4 1434.750 1401.760 8.131 1.556 o
2 6 6 113.454 111.725 1.064 101.239 o
2 8 2 1104.750 1099.650 10.906 2.154 o
2 8 4 105.943 105.356 0.585 118.142 o
2 8 6 712.317 702.383 3.176 5.812 o
2 8 8 58.395 59.198 0.742 232.958 o
2 10 2 80.803 82.620 0.772 159.004 o
2 10 4 582.290 588.542 2.479 8.231 o
2 10 6 51.867 52.795 0.466 285.301 o
2 10 8 333.460 323.747 3.095 19.095 o
2 12 2 399.255 413.668 3.537 13.825 o
2 12 4 37.612 39.556 0.431 407.005 o
2 12 6 276.547 279.764 3.264 23.543 o
3 3 3 1058.750 1015.450 22.464 1.334 o
3 5 3 744.051 730.519 8.238 4.293 o
3 5 5 577.306 565.610 4.694 7.638 o
3 7 3 516.978 511.331 4.343 9.158 o
3 7 5 420.466 418.852 1.933 14.459 o
3 7 7 310.225 311.668 1.549 23.677 o
3 9 3 346.049 343.284 2.001 19.589 o
3 9 5 281.360 282.407 1.317 27.896 o
3 9 7 206.887 207.561 1.355 43.689 o
3 9 9 142.184 137.346 2.646 55.733 o
3 11 3 210.698 216.105 2.004 39.140 o
3 11 5 169.534 176.005 1.303 56.904 o
3 11 7 128.618 122.426 1.977 72.947 o
4 4 4 1675.060 1565.030 20.876 0.886 o
4 6 4 119.912 119.453 1.183 92.131 o
4 6 6 879.421 862.593 5.367 3.812 o
4 8 4 790.170 794.623 5.222 4.503 o
4 8 6 72.832 73.930 0.510 189.670 o
4 8 8 436.942 442.412 4.269 11.591 o
4 10 4 59.850 60.658 0.664 231.506 o
4 10 6 398.537 405.161 3.156 14.416 o
4 10 8 30.993 28.481 0.417 527.080 o
4 12 4 306.530 307.881 3.167 20.917 o
5 5 5 466.121 463.500 4.317 10.633 o
5 7 5 341.598 342.537 2.065 19.786 o
5 7 7 254.497 250.420 2.357 29.677 o
5 9 5 230.191 235.921 2.431 32.968 o
5 9 7 172.226 174.245 1.401 55.678 o
5 11 5 142.330 144.691 1.573 69.018 o
6 6 6 80.307 79.164 1.300 141.576 o
6 8 6 481.289 480.862 3.662 10.601 o
6 8 8 38.875 37.842 0.836 344.507 o
6 10 6 34.634 34.227 0.563 433.418 o
7 7 7 190.116 187.837 4.034 31.048 o
7 9 7 129.374 118.415 2.999 56.042 o
;
_iucr_refine_instructions_details
;
TITL caf_ag3_a.res in Fm-3m
REM Old TITL CaF_Ag3 in Fm-3m
REM SHELXT solution in Fm-3m
REM R1 0.012, Rweak 0.001, Alpha 0.002, Orientation as input
REM Formula found by SHELXT: F2 Ca
CELL 0.56087 5.450952 5.450952 5.450952 90 90 90
ZERR 4 0.000052 0.000052 0.000052 0 0 0
LATT 4
SYMM -X,-Y,+Z
SYMM -X,+Y,-Z
SYMM +X,-Y,-Z
SYMM +Z,+X,+Y
SYMM +Z,-X,-Y
SYMM -Z,-X,+Y
SYMM -Z,+X,-Y
SYMM +Y,+Z,+X
SYMM -Y,+Z,-X
SYMM +Y,-Z,-X
SYMM -Y,-Z,+X
SYMM +Y,+X,-Z
SYMM -Y,-X,-Z
SYMM +Y,-X,+Z
SYMM -Y,+X,+Z
SYMM +X,+Z,-Y
SYMM -X,+Z,+Y
SYMM -X,-Z,-Y
SYMM +X,-Z,+Y
SYMM +Z,+Y,-X
SYMM +Z,-Y,+X
SYMM -Z,+Y,+X
SYMM -Z,-Y,-X
SFAC Ca F
DISP Ca 0.1378 0.1937 651.9347
DISP F 0.006 0.0061 27.6988
UNIT 4 8
L.S. 10
PLAN 10
CONF
MORE -1
fmap 2
acta
LIST -6
WGHT 0.017492 0.060656
FVAR 0.977822
REM
REM
REM
Ca01 1 0.50000 0.50000 0.50000 10.02083 0.00334 0.00334 0.00334 =
0.00000 0.00000 0.00000
F002 2 0.25000 0.75000 0.75000 10.04167 0.00505 0.00505 0.00505 =
0.00000 -0.00000 -0.00000
HKLF 4
END
Q1 1 0.388889 0.611111 0.611111 11 0.05 0.25
Q2 1 0.5 0.722222 0.5 11 0.05 0.19
Q3 1 0 0.75 0.75 11 0.05 0.19
Q4 1 0.138889 0.861111 0.861111 11 0.05 0.08
Q5 1 0 1 1 11 0.05 -0.04
REM The information below was added by Olex2.
REM
REM R1 = 0.0114 for 96 Fo > 4sig(Fo) and 0.0114 for all 96 data
REM 3 parameters refined using 0 restraints
REM Highest difference peak 0.6860, deepest hole -0.4146
REM Mean Shift 0.0000, Max Shift 0.0000.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0114
REM R1_gt = 0.0114
REM wR_ref = 0.0279
REM GOOF = 1.0864
REM Shift_max = 0.0000
REM Shift_mean = 0.0000
REM Reflections_all = 96
REM Reflections_gt = 96
REM Parameters = 3
REM Hole = -0.4146
REM Peak = 0.6860
REM Flack = n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.970
_oxdiff_exptl_absorpt_empirical_full_min 0.709
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2
_database_code_depnum_ccdc_archive 'CCDC 2035147'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-10-02 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-17-11
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.01.16 svn.ra754ea2f for OlexSys, GUI svn.r6014)
;
#----------------------------------------------------------------------------#
# CHEMICAL INFORMATION #
#----------------------------------------------------------------------------#
_chemical_formula_moiety 'C3 H7 N O2'
_chemical_formula_sum 'C3 H7 N O2'
_chemical_formula_weight 89.0947
_chemical_absolute_configuration syn
#----------------------------------------------------------------------------#
# UNIT CELL INFORMATION #
#----------------------------------------------------------------------------#
_symmetry_cell_setting Orthorhombic
_symmetry_space_group_name_H-M 'p 21 21 21'
_symmetry_space_group_name_Hall 'p 2ac 2ab'
_symmetry_Int_Tables_number 19
loop_
_symmetry_equiv_pos_as_xyz
'+x, +y, +z'
'-x+1/2, -y, +z+1/2'
'+x+1/2, -y+1/2, -z'
'-x, +y+1/2, -z+1/2'
_cell_length_a 5.9279(10)
_cell_length_b 12.2597(17)
_cell_length_c 5.7939(9)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 421.07(11)
_cell_formula_units_Z 4
_cell_measurement_temperature 23
_cell_measurement_wavelength 0.71073
_cell_measurement_theta_min 15.00
_cell_measurement_theta_max 22.50
_cell_measurement_reflns_used 1524
#----------------------------------------------------------------------------#
# CRYSTAL INFORMATION #
#----------------------------------------------------------------------------#
_exptl_crystal_description sphere
_exptl_crystal_colour colorless
_exptl_crystal_size_rad 0.18
_exptl_crystal_density_diffrn 1.406
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 192
#----------------------------------------------------------------------------#
# ABSORPTION CORRECTION #
#----------------------------------------------------------------------------#
_exptl_absorpt_coefficient_mu 0.117
_exptl_absorpt_correction_type none
#----------------------------------------------------------------------------#
# DATA COLLECTION #
#----------------------------------------------------------------------------#
_diffrn_ambient_temperature 23
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_type MoK\a
_diffrn_radiation_probe x-ray
_diffrn_measurement_method 'area detector'
_diffrn_measurement_device_type 'P-1 four circle diffractometer'
_diffrn_standards_number 0
_diffrn_reflns_av_unetI/netI 0.0243
_diffrn_reflns_number 2387
_diffrn_reflns_limit_h_min 0
_diffrn_reflns_limit_h_max 12
_diffrn_reflns_limit_k_min 0
_diffrn_reflns_limit_k_max 26
_diffrn_reflns_limit_l_min 0
_diffrn_reflns_limit_l_max 12
_diffrn_reflns_theta_full 25.2417
_diffrn_reflns_theta_max 50.14
_diffrn_reflns_theta_min 3.32
_diffrn_measured_fraction_theta_full 0.9641
_diffrn_measured_fraction_theta_max 0.9412
_diffrn_reflns_point_group_measured_fraction_full 0.9641
_diffrn_reflns_point_group_measured_fraction_max 0.9412
_reflns_Friedel_fraction_full 0
_reflns_Friedel_fraction_max 0
_reflns_Friedel_coverage 0.0
_reflns_number_gt 2387
_reflns_number_total 2387
_reflns_threshold_expression I/u(I)>2.1
#----------------------------------------------------------------------------#
# COMPUTER PROGRAMS USED #
#----------------------------------------------------------------------------#
_computing_structure_solution 'SHELXS-2013 (Sheldrick, 2008)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
#----------------------------------------------------------------------------#
# STRUCTURE SOLUTION #
#----------------------------------------------------------------------------#
_atom_sites_solution_hydrogens difmap
#----------------------------------------------------------------------------#
# REFINEMENT INFORMATION #
#----------------------------------------------------------------------------#
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
_atom_type_scat_dispersion_source
H 0.00000 0.00000 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
C 0.00347 0.00161 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
O 0.01158 0.00611 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
N 0.00653 0.00323 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
_refine_diff_density_max 0.1628
_refine_diff_density_min -0.1652
_refine_diff_density_rms 0.0419
_refine_ls_d_res_high 0.4630
_refine_ls_d_res_low 6.1299
_refine_ls_goodness_of_fit_ref 1.2147
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 118
_refine_ls_number_reflns 2387
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0196
_refine_ls_R_factor_gt 0.0196
_refine_ls_restrained_S_all 1.2147
_refine_ls_shift/su_max 0.0005
_refine_ls_shift/su_mean 0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details w=1/[\s^2^(Fo^2^)]
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0332
_refine_ls_wR_factor_ref 0.0332
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be publsihed - 2020
NoSpherA2 makes use of tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or B3LYP
- for a fragment of the crystal embedded in
an electrostatic crystal field.
The following options were used:
SOFTWARE: ORCA
METHOD: rhf
BASIS SET: 6-311G(d,p)
CHARGE: 0
MULTIPLICITY: 1
DATE: 2020-01-29_13-41-33
;
#----------------------------------------------------------------------------#
# VALIDATION REPLY FORM #
#----------------------------------------------------------------------------#
_vrf_PLAT881_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2
;
PROBLEM: No Datum for _diffrn_reflns_av_R_equivalents ... Please Do !
RESPONSE: The dataset used corresponds to the CCDC number 1203202 (CSD code
LALNIN03), which is merged. No information on Rmerge was provided by the
previous authors.
;
_vrf_PLAT926_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2
;
PROBLEM: Reported and Calculated R1 Differ by ......... -0.0111 Check
RESPONSE: Because CheckCIF is unable to treat aspherical refinements.
;
_vrf_PLAT927_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0452 Check
RESPONSE: Because CheckCIF is unable to treat aspherical refinements.
;
_vrf_PLAT928_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2
;
PROBLEM: Reported and Calculated S value Differ by . -1.657 Check
RESPONSE: Because CheckCIF is unable to treat aspherical refinements.
;
# end Validation Reply Form
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_refinement_flags_posn
N1 N 0.64723(5) 0.13752(2) 0.18292(5) 0.00536(4) Uani 1.000000 .
H1a H 0.7039(13) 0.0593(6) 0.2015(15) 0.026(2) Uani 1.000000 .
H1b H 0.7774(12) 0.1900(5) 0.2116(15) 0.0230(19) Uani 1.000000 .
H1c H 0.5805(12) 0.1495(5) 0.0182(14) 0.0239(19) Uani 1.000000 .
C1 C 0.46639(5) 0.16112(2) 0.35429(5) 0.00464(4) Uani 1.000000 .
H1 H 0.4267(10) 0.2481(4) 0.3426(12) 0.0218(17) Uani 1.000000 .
C2 C 0.25992(5) 0.09066(3) 0.30333(6) 0.00710(4) Uani 1.000000 .
H2a H 0.1911(11) 0.1102(5) 0.1333(13) 0.030(2) Uani 1.000000 .
H2b H 0.1259(12) 0.1046(6) 0.4304(14) 0.030(2) Uani 1.000000 .
H2c H 0.3031(10) 0.0052(5) 0.3083(14) 0.030(2) Uani 1.000000 .
C3 C 0.55406(5) 0.14079(2) 0.59985(5) 0.00440(4) Uani 1.000000 .
O1 O 0.72667(4) 0.083801(18) 0.62429(4) 0.00651(4) Uani 1.000000 .
O2 O 0.44091(4) 0.184009(18) 0.76109(4) 0.00632(3) Uani 1.000000 .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
N1 0.00557(8) 0.00616(7) 0.00434(9) 0.00012(7) 0.00070(7) -0.00012(7)
H1a 0.029(5) 0.034(4) 0.015(5) -0.005(4) 0.009(4) -0.003(4)
H1b 0.022(4) 0.025(4) 0.022(5) 0.004(4) 0.002(4) -0.002(4)
H1c 0.023(4) 0.015(4) 0.033(5) -0.002(4) 0.021(4) -0.008(4)
C1 0.00535(9) 0.00488(8) 0.00368(10) 0.00039(7) -0.00054(7) 0.00009(7)
H1 0.027(4) 0.015(3) 0.023(4) 0.005(3) -0.007(4) 0.002(3)
C2 0.00604(9) 0.00898(9) 0.00628(11) -0.00137(8) -0.00057(8) -0.00042(8)
H2a 0.024(4) 0.046(5) 0.020(5) -0.012(4) -0.004(4) 0.004(4)
H2b 0.022(4) 0.039(5) 0.029(5) -0.007(4) 0.004(4) 0.002(4)
H2c 0.028(5) 0.025(3) 0.036(6) -0.007(4) 0.002(4) 0.000(4)
C3 0.00498(8) 0.00458(7) 0.00363(9) 0.00047(7) -0.00013(7) -0.00006(7)
O1 0.00683(7) 0.00711(7) 0.00561(9) 0.00234(6) -0.00062(7) 0.00047(6)
O2 0.00746(7) 0.00754(7) 0.00397(8) 0.00210(6) 0.00043(7) -0.00043(6)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
N1 H1a 1.022(7) . ?
N1 H1b 1.018(7) . ?
N1 H1c 1.044(8) . ?
N1 C1 1.4895(4) . ?
C1 H1 1.094(5) . ?
C1 C2 1.5269(4) . ?
C1 C3 1.5351(5) . ?
C2 H2a 1.093(7) . ?
C2 H2b 1.096(7) . ?
C2 H2c 1.079(6) . ?
C3 O1 1.2471(4) . ?
C3 O2 1.2662(4) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
H1b N1 H1a 109.1(5) . . ?
H1c N1 H1a 110.7(6) . . ?
H1c N1 H1b 110.3(6) . . ?
C1 N1 H1a 110.4(5) . . ?
C1 N1 H1b 108.3(4) . . ?
C1 N1 H1c 108.0(4) . . ?
H1 C1 N1 107.6(3) . . ?
C2 C1 N1 109.76(3) . . ?
C2 C1 H1 111.5(3) . . ?
C3 C1 N1 110.04(2) . . ?
C3 C1 H1 106.8(4) . . ?
C3 C1 C2 111.02(2) . . ?
H2a C2 C1 110.5(3) . . ?
H2b C2 C1 111.3(4) . . ?
H2b C2 H2a 107.5(5) . . ?
H2c C2 C1 110.7(3) . . ?
H2c C2 H2a 109.0(5) . . ?
H2c C2 H2b 107.8(5) . . ?
O1 C3 C1 118.30(3) . . ?
O2 C3 C1 115.88(3) . . ?
O2 C3 O1 125.82(3) . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1 C1 C3 O1 -18.15(3) . . . . ?
N1 C1 C3 O2 162.19(2) . . . . ?
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
0 2 0 179.82 1.72
0 4 0 5073.71 43.49
0 6 0 87.76 1.02
0 8 0 44.37 0.7
0 10 0 0.78 0.34
0 12 0 227.75 2.6
0 14 0 57.3 1.1
0 16 0 24.7 0.84
0 18 0 222.73 2.91
0 22 0 132.62 2.31
0 26 0 6.31 0.6
0 1 1 708.79 7.17
0 2 1 116.96 1.19
0 3 1 693.29 6.26
0 4 1 96.15 1.04
0 6 1 464.73 4.48
0 7 1 36.13 0.6
0 8 1 43.4 0.71
0 9 1 31.39 0.65
0 10 1 134.35 1.66
0 11 1 65.28 1.08
0 12 1 74.7 1.2
0 13 1 18.43 0.68
0 14 1 37.09 0.92
0 15 1 89.01 1.52
0 17 1 1.11 0.34
0 18 1 58.59 1.34
0 19 1 15.81 0.87
0 20 1 26.85 1.02
0 21 1 2.63 0.41
0 23 1 1.69 0.41
0 25 1 2.92 0.55
0 26 1 19.36 1.21
0 0 2 2781.11 32.59
0 1 2 521.67 6.41
0 2 2 177.65 2.03
0 3 2 54.98 0.78
0 4 2 167.52 1.75
0 5 2 554.6 5.21
0 6 2 94.63 1.14
0 7 2 5.3 0.33
0 8 2 109.31 1.37
0 9 2 23.18 0.58
0 10 2 45.26 0.84
0 11 2 81.97 1.23
0 12 2 27.64 0.73
0 13 2 21.03 0.68
0 14 2 20.83 0.74
0 15 2 177.41 2.34
0 16 2 4.35 0.4
0 17 2 59.75 1.35
0 18 2 19.96 0.89
0 19 2 117.29 2.05
0 20 2 0.96 0.4
0 21 2 44.95 1.33
0 22 2 36.02 1.26
0 23 2 17.63 1.01
0 24 2 2.44 0.45
0 25 2 21.98 1.23
0 26 2 2.5 0.49
0 1 3 82.18 1.71
0 2 3 154.36 2.86
0 3 3 201 2.4
0 4 3 723.07 7.61
0 5 3 79.56 1.17
0 6 3 266.47 2.78
0 7 3 21.92 0.56
0 8 3 60.32 0.97
0 9 3 139.65 1.74
0 10 3 38.76 0.81
0 11 3 68.85 1.16
0 12 3 116.35 1.66
0 13 3 142.37 1.96
0 14 3 27.22 0.84
0 15 3 88.51 1.55
0 16 3 151.45 2.21
0 17 3 46.19 1.21
0 18 3 26.42 0.97
0 19 3 2.45 0.4
0 20 3 43.48 1.31
0 21 3 0.85 0.38
0 22 3 1.13 0.4
0 23 3 27.55 1.14
0 24 3 12.44 0.89
0 25 3 4.87 0.56
0 0 4 205.15 3.82
0 1 4 38.96 1.18
0 2 4 91.05 2.01
0 3 4 7.83 0.44
0 4 4 224.51 2.78
0 6 4 69.4 1.2
0 7 4 28.59 0.76
0 8 4 63.09 1.05
0 9 4 7.04 0.45
0 10 4 88.39 1.35
0 11 4 95.86 1.48
0 12 4 38.16 0.94
0 13 4 11.24 0.64
0 14 4 139.35 2.04
0 15 4 44.29 1.16
0 16 4 92.63 1.7
0 17 4 5.58 0.45
0 18 4 9.43 0.73
0 19 4 3.29 0.43
0 20 4 1.79 0.4
0 22 4 4.26 0.48
0 24 4 26 1.11
0 25 4 2.84 0.5
0 1 5 231.01 4.42
0 2 5 134.31 2.89
0 3 5 48.15 1.5
0 4 5 380.68 4.49
0 5 5 173.89 2.38
0 7 5 6.48 0.52
0 8 5 142.09 2.13
0 9 5 67.86 1.39
0 10 5 7.78 0.54
0 11 5 20.3 0.76
0 12 5 1.46 0.32
0 13 5 77.47 1.47
0 14 5 3.44 0.4
0 15 5 13.79 0.77
0 16 5 12.99 0.78
0 17 5 75.36 1.62
0 18 5 2.28 0.41
0 19 5 13.33 0.88
0 21 5 19.21 1.02
0 22 5 5.38 0.51
0 23 5 12.25 0.94
0 1 6 91.72 2.4
0 2 6 15.85 1
0 3 6 1.46 0.63
0 4 6 15.64 1.06
0 5 6 84.39 1.54
0 6 6 10.94 0.64
0 7 6 138.98 2.19
0 8 6 29.35 0.96
0 9 6 14.04 0.76
0 10 6 15.27 0.8
0 11 6 114.68 1.86
0 12 6 6.17 0.55
0 13 6 4.67 0.47
0 14 6 11.44 0.72
0 16 6 40.64 1.25
0 17 6 28.49 1.08
0 18 6 7.63 0.67
0 19 6 43.26 1.36
0 20 6 1.8 0.42
0 21 6 20.84 1.06
0 22 6 10.35 0.76
0 23 6 16.64 0.97
0 1 7 57.51 2.01
0 2 7 529.52 9.52
0 4 7 11.53 1.08
0 5 7 23.56 1.4
0 6 7 42.24 1.19
0 7 7 45.64 1.25
0 8 7 1.91 0.42
0 9 7 4.83 0.51
0 10 7 9.02 0.79
0 11 7 30.72 1.16
0 12 7 5.71 0.63
0 13 7 11.39 0.78
0 14 7 1.45 0.38
0 16 7 79.93 1.77
0 17 7 1.03 0.39
0 18 7 2.26 0.43
0 19 7 6.71 0.54
0 20 7 132.31 2.4
0 21 7 0.89 0.39
0 0 8 23.95 1.48
0 1 8 3.51 0.93
0 2 8 8.52 1.12
0 3 8 15.38 1.32
0 6 8 10.05 0.8
0 7 8 58.35 1.53
0 8 8 85.61 1.89
0 9 8 12 0.85
0 10 8 6.4 0.68
0 11 8 39.23 1.37
0 12 8 39.36 1.41
0 13 8 31.46 1.32
0 14 8 12.27 0.96
0 16 8 0.98 0.39
0 17 8 6.43 0.54
0 19 8 9.03 0.75
0 20 8 6.03 0.52
0 1 9 8.34 1.14
0 2 9 45.38 2.15
0 3 9 61.98 2.48
0 4 9 21.74 1.59
0 7 9 45.52 1.49
0 8 9 77.94 1.9
0 9 9 16.12 1.05
0 10 9 13.55 1
0 11 9 2.19 0.51
0 12 9 34.14 1.37
0 13 9 28.52 1.31
0 15 9 46.28 1.61
0 16 9 14.15 1.07
0 17 9 15.19 0.96
0 18 9 8.4 0.63
0 0 10 4.71 1.2
0 2 10 20.26 1.7
0 3 10 47.91 2.36
0 4 10 27.73 1.9
0 5 10 32 2.01
0 6 10 40.72 2.28
0 7 10 53.18 2.55
0 8 10 58.9 1.76
0 9 10 6.59 0.64
0 10 10 1.82 0.51
0 11 10 16.03 1.12
0 12 10 13.13 0.91
0 13 10 12.27 1.03
0 14 10 42.63 1.59
0 15 10 5.73 0.63
0 2 11 2.64 1.21
0 3 11 6.65 1.45
0 6 11 7.55 1.5
0 7 11 3.03 1.32
0 8 11 8.21 1.5
0 9 11 7.83 0.75
0 10 11 1.54 0.52
0 11 11 8.17 0.82
0 12 11 29.51 1.37
0 1 12 26.43 2.2
0 2 12 19.77 1.92
0 3 12 113.72 3.87
0 5 12 9.57 1.68
0 6 12 54.58 2.7
0 7 12 63.43 2.98
1 1 0 246.12 2.31
1 2 0 5369.63 56.86
1 3 0 57.84 0.67
1 4 0 1642.66 14.45
1 5 0 331.16 3.22
1 6 0 60.55 0.78
1 7 0 18.84 0.43
1 8 0 393.56 3.92
1 9 0 3.19 0.34
1 10 0 42.14 0.79
1 11 0 94.82 1.33
1 12 0 26.34 0.69
1 13 0 56.1 1.06
1 15 0 84.47 1.45
1 16 0 23.94 0.83
1 17 0 28.91 0.94
1 18 0 0.91 0.37
1 19 0 33.01 1.08
1 20 0 39.41 1.22
1 21 0 1.4 0.42
1 22 0 3.91 0.46
1 23 0 6.86 0.59
1 24 0 9.58 0.77
1 26 0 7.17 0.62
1 0 1 75.15 0.81
1 1 1 130.72 1.33
1 2 1 101.9 1.08
1 3 1 1064.41 9.47
1 4 1 153.69 1.6
1 5 1 428.55 4.14
1 6 1 21.42 0.43
1 7 1 332.12 3.34
1 8 1 229.59 2.43
1 9 1 227.34 2.48
1 10 1 128.42 1.64
1 11 1 16.78 0.55
1 13 1 124.92 1.73
1 14 1 28.95 0.81
1 15 1 85.76 1.48
1 16 1 60.47 1.26
1 17 1 24.89 0.88
1 18 1 23.28 0.91
1 19 1 14.98 0.81
1 20 1 5.7 0.47
1 21 1 2.02 0.4
1 22 1 34.03 1.18
1 23 1 10.43 0.87
1 24 1 20.49 1.05
1 25 1 9.29 0.8
1 26 1 1.96 0.47
1 0 2 3039.32 35.37
1 1 2 70.14 0.92
1 2 2 560.27 5.99
1 3 2 189.97 1.98
1 4 2 1041.63 9.43
1 5 2 18.21 0.4
1 6 2 214.83 2.26
1 7 2 158.6 1.78
1 8 2 10.03 0.42
1 9 2 60.49 0.96
1 10 2 58.21 0.98
1 11 2 115.45 1.56
1 12 2 112.96 1.59
1 13 2 107.88 1.6
1 14 2 53.55 1.11
1 15 2 30.97 0.9
1 16 2 27.04 0.92
1 17 2 74.12 1.49
1 18 2 107.76 1.89
1 19 2 40.34 1.18
1 20 2 9.5 0.69
1 21 2 22.39 1
1 22 2 35.81 1.25
1 23 2 42.49 1.39
1 24 2 10.43 0.78
1 26 2 4.4 0.55
1 0 3 31.36 0.9
1 1 3 296.14 5.12
1 2 3 220 2.58
1 3 3 89.79 1.25
1 4 3 93.64 1.31
1 5 3 22.55 0.51
1 6 3 135.19 1.6
1 7 3 5.07 0.37
1 8 3 252.19 2.75
1 9 3 28.4 0.69
1 10 3 78 1.21
1 11 3 16.31 0.58
1 12 3 31.61 0.82
1 13 3 33.09 0.89
1 14 3 112.42 1.74
1 15 3 32.78 0.96
1 16 3 9.1 0.6
1 17 3 24.5 0.92
1 18 3 25.96 0.98
1 19 3 26.64 1.03
1 20 3 7.6 0.65
1 21 3 23.09 1.03
1 22 3 7.04 0.6
1 23 3 2.69 0.45
1 24 3 7.96 0.63
1 25 3 17.53 1.14
1 0 4 321.45 5.71
1 1 4 254.55 4.63
1 2 4 28.14 1.02
1 3 4 22.92 0.63
1 4 4 107.36 1.53
1 5 4 81.92 1.31
1 6 4 127.61 1.83
1 7 4 81.95 1.2
1 8 4 44.22 0.87
1 9 4 2.13 0.38
1 10 4 22.23 0.69
1 11 4 61.03 1.15
1 12 4 137.9 1.95
1 13 4 26.56 0.84
1 14 4 38.58 1.04
1 15 4 2.92 0.39
1 16 4 23.08 0.89
1 17 4 27.5 1
1 18 4 57.35 1.43
1 19 4 39.95 1.22
1 20 4 9.05 0.78
1 21 4 10.57 0.77
1 22 4 21.31 1.02
1 23 4 14.76 0.94
1 24 4 2.09 0.42
1 0 5 278.56 5.19
1 1 5 119.84 2.65
1 2 5 453.96 7.95
1 3 5 172.59 3.56
1 4 5 105.84 1.65
1 5 5 8.38 0.52
1 6 5 224.91 2.95
1 7 5 71.42 1.36
1 8 5 67.87 1.35
1 9 5 88.15 1.43
1 10 5 9.32 0.57
1 11 5 35.1 0.93
1 12 5 24.55 0.84
1 13 5 43.79 1.13
1 14 5 39.36 1.1
1 15 5 29.22 1
1 16 5 76.96 1.6
1 17 5 11.22 0.78
1 18 5 6.81 0.63
1 19 5 18.29 0.95
1 20 5 63.31 1.61
1 21 5 24.58 1.09
1 22 5 1.69 0.42
1 23 5 4.48 0.49
1 24 5 17.07 0.98
1 2 6 7.39 0.81
1 3 6 12.16 0.97
1 4 6 15.66 1.06
1 5 6 13.01 0.65
1 6 6 21.43 0.8
1 7 6 7.62 0.61
1 8 6 8.9 0.67
1 9 6 10.84 0.75
1 10 6 2.38 0.43
1 11 6 9.63 0.66
1 12 6 28.39 0.94
1 13 6 7.38 0.59
1 14 6 27.43 0.98
1 15 6 10.78 0.8
1 16 6 2.92 0.42
1 17 6 21.07 0.98
1 18 6 13.57 0.88
1 19 6 11.56 0.84
1 20 6 30.94 1.22
1 21 6 9.21 0.76
1 22 6 8.45 0.74
1 23 6 11.78 0.87
1 0 7 242.74 5.04
1 1 7 26.29 1.42
1 2 7 60.08 2.07
1 3 7 79.75 2.44
1 4 7 138.36 3.44
1 5 7 29.94 1.02
1 6 7 60.44 1.44
1 7 7 9.31 0.75
1 8 7 55.17 1.42
1 9 7 65.97 1.58
1 10 7 18.37 0.94
1 11 7 21.39 0.89
1 12 7 1.87 0.45
1 13 7 41.47 1.22
1 14 7 24.11 1.03
1 15 7 31.65 1.15
1 16 7 25.32 1.05
1 17 7 20.08 0.99
1 18 7 42.16 1.36
1 19 7 6.61 0.6
1 20 7 15.13 0.97
1 21 7 9.12 0.65
1 0 8 10.23 1.18
1 1 8 34.61 1.75
1 2 8 19.45 1.41
1 3 8 31.46 1.67
1 4 8 32.11 1.72
1 5 8 100.16 3.05
1 6 8 14.74 0.9
1 7 8 89.49 1.92
1 8 8 3.18 0.48
1 9 8 50.19 1.49
1 10 8 38.92 1.35
1 11 8 93.59 2.08
1 12 8 11.53 0.95
1 13 8 27.74 1.24
1 14 8 1.18 0.5
1 15 8 45.34 1.35
1 16 8 5.47 0.51
1 17 8 26.28 1.16
1 18 8 5.35 0.51
1 19 8 2.22 0.43
1 1 9 2.19 0.98
1 2 9 50.49 2.22
1 4 9 3.19 1.11
1 5 9 28.01 1.8
1 6 9 9.85 1.27
1 7 9 15.55 0.99
1 8 9 8.18 0.73
1 9 9 19.43 1.09
1 10 9 28.98 1.29
1 11 9 45.17 1.54
1 12 9 8.76 0.81
1 13 9 15.77 1.11
1 14 9 7.76 0.81
1 15 9 21.79 1.21
1 16 9 42.07 1.55
1 17 9 17.93 1.03
1 18 9 11.34 0.88
1 0 10 3.41 1.15
1 1 10 25.21 1.84
1 3 10 19.75 1.68
1 4 10 21.27 1.78
1 5 10 32.03 2.05
1 6 10 40.76 2.26
1 7 10 31.06 2.06
1 8 10 24.03 1.23
1 9 10 7.23 0.79
1 10 10 54.84 1.76
1 11 10 15.97 1.12
1 12 10 44.65 1.61
1 14 10 6.44 0.65
1 15 10 10.32 0.86
1 1 11 11.76 1.58
1 2 11 33.14 2.21
1 3 11 22.93 1.91
1 4 11 11.66 1.59
1 5 11 6.02 1.42
1 6 11 3.87 1.32
1 7 11 8.44 1.55
1 8 11 15.31 1.16
1 9 11 23.05 1.28
1 10 11 18.35 1.2
1 11 11 3.53 0.58
1 12 11 1.58 0.52
1 0 12 17.52 1.89
1 1 12 74.46 3.12
1 2 12 8.13 1.7
1 4 12 28.46 2.17
1 5 12 67.23 3.05
1 7 12 22.4 2.04
2 0 0 41.03 0.52
2 1 0 30.45 0.43
2 2 0 1642.63 14.47
2 3 0 769.66 7.02
2 4 0 35.08 0.52
2 5 0 89.17 1.06
2 6 0 2036.41 18.08
2 7 0 287.43 2.94
2 8 0 0.75 0.3
2 9 0 229.89 2.53
2 10 0 248.88 2.73
2 11 0 2.36 0.35
2 12 0 42.46 0.89
2 13 0 164.35 2.1
2 14 0 10.7 0.59
2 15 0 68.44 1.3
2 16 0 36.2 1
2 17 0 34.91 1.02
2 18 0 42.77 1.17
2 19 0 36.95 1.14
2 20 0 0.9 0.36
2 21 0 7.57 0.63
2 22 0 14.8 0.91
2 23 0 10.92 0.86
2 24 0 31.69 1.21
2 25 0 4.03 0.56
2 26 0 1.05 0.44
2 0 1 1.6 0.16
2 1 1 76.33 0.86
2 2 1 271.45 2.67
2 3 1 524.91 4.94
2 4 1 154.41 1.63
2 5 1 417.6 4.06
2 6 1 22.42 0.47
2 7 1 95.87 1.2
2 8 1 4.74 0.35
2 9 1 267.32 2.88
2 10 1 8.52 0.45
2 11 1 4.65 0.42
2 12 1 39.82 0.87
2 13 1 78.11 1.32
2 14 1 43.77 1
2 15 1 23.24 0.79
2 16 1 3.49 0.39
2 17 1 9.86 0.68
2 18 1 9.74 0.71
2 19 1 28.61 1.04
2 20 1 70.12 1.6
2 21 1 28.25 1.1
2 22 1 22.83 1.05
2 23 1 2.51 0.44
2 24 1 40.26 1.31
2 25 1 22.5 1.29
2 26 1 29.82 1.42
2 0 2 4.11 0.22
2 1 2 302 2.99
2 2 2 1061.19 9.6
2 3 2 104.8 1.23
2 4 2 87.16 1.07
2 5 2 8.21 0.34
2 6 2 285.84 2.95
2 7 2 137.38 1.63
2 8 2 141 1.72
2 9 2 125.4 1.58
2 10 2 2.59 0.36
2 11 2 62.74 1.1
2 12 2 56.09 1.06
2 13 2 71.93 1.28
2 14 2 33.1 0.89
2 15 2 31.14 0.92
2 16 2 71.67 1.43
2 18 2 10.59 0.72
2 19 2 1.11 0.36
2 20 2 31.17 1.1
2 21 2 29.6 1.14
2 22 2 3.49 0.46
2 23 2 2.48 0.44
2 24 2 8.53 0.74
2 25 2 39.07 1.63
2 0 3 129.28 1.5
2 1 3 137.4 1.55
2 2 3 375.51 3.72
2 3 3 438.71 4.34
2 4 3 64.45 0.92
2 5 3 244.11 2.61
2 6 3 89.09 1.2
2 7 3 106.32 1.38
2 8 3 117.12 1.52
2 9 3 283.34 3.12
2 10 3 251.54 2.86
2 11 3 11.76 0.57
2 12 3 82.7 1.38
2 13 3 42.94 1.01
2 14 3 47.17 1.11
2 15 3 16.62 0.78
2 16 3 2.73 0.39
2 17 3 12.49 0.74
2 18 3 2.06 0.38
2 19 3 38.04 1.19
2 20 3 9.67 0.65
2 21 3 42.42 1.34
2 22 3 7.64 0.7
2 23 3 5.1 0.56
2 25 3 12.78 1.05
2 0 4 55.58 1.5
2 1 4 104.64 1.51
2 2 4 128.39 1.79
2 3 4 130.56 1.81
2 4 4 12.73 0.56
2 5 4 58.57 0.96
2 6 4 105.93 1.42
2 7 4 100.33 1.4
2 8 4 114.04 1.56
2 9 4 47.61 0.96
2 10 4 135.41 1.84
2 11 4 48.77 1.05
2 12 4 12.41 0.64
2 14 4 11.45 0.69
2 15 4 12.56 0.73
2 16 4 24.67 0.9
2 17 4 37.94 1.16
2 18 4 24.84 1.02
2 19 4 8.53 0.69
2 20 4 26.09 1.07
2 21 4 19.85 1.02
2 22 4 16.43 1.01
2 23 4 22.95 1.05
2 24 4 3.27 0.46
2 0 5 141.46 3.04
2 1 5 33.25 1.28
2 2 5 157.95 2.2
2 3 5 30.97 0.83
2 4 5 145.24 2.08
2 5 5 62.41 1.22
2 6 5 12.22 0.62
2 7 5 13.86 0.69
2 8 5 61.42 1.15
2 9 5 25.65 0.79
2 10 5 135.72 1.93
2 11 5 59.07 1.23
2 12 5 14.01 0.73
2 13 5 2.21 0.37
2 14 5 90.5 1.68
2 15 5 12.44 0.75
2 16 5 1.11 0.35
2 17 5 5.22 0.47
2 18 5 43.39 1.34
2 19 5 10.89 0.82
2 20 5 1.38 0.41
2 21 5 0.93 0.4
2 22 5 20.53 1.02
2 23 5 16.1 1
2 0 6 74.87 2.16
2 1 6 92 2.45
2 2 6 2.26 0.7
2 3 6 2.21 0.56
2 4 6 22.16 0.8
2 5 6 96.53 1.72
2 7 6 75.53 1.53
2 9 6 4.82 0.47
2 10 6 11.86 0.68
2 11 6 102.3 1.75
2 12 6 7.72 0.53
2 13 6 61.02 1.39
2 14 6 11.03 0.73
2 15 6 55.59 1.41
2 16 6 15.05 0.88
2 17 6 45.94 1.34
2 18 6 48.61 1.43
2 19 6 2.3 0.43
2 20 6 3.73 0.47
2 21 6 13.46 0.94
2 22 6 44.76 1.39
2 0 7 7.26 0.96
2 1 7 43.02 1.78
2 2 7 12.3 1.1
2 3 7 14.18 1.17
2 4 7 127.64 2.62
2 5 7 69.53 1.54
2 6 7 28.72 1.04
2 7 7 81.94 1.74
2 8 7 80.67 1.73
2 9 7 4.88 0.52
2 10 7 9.3 0.78
2 11 7 95.59 2.02
2 12 7 2.13 0.38
2 13 7 47.91 1.33
2 14 7 39.42 1.22
2 15 7 32.09 1.17
2 16 7 4.2 0.47
2 17 7 49.77 1.45
2 18 7 9.69 0.75
2 19 7 6.86 0.62
2 20 7 0.96 0.4
2 21 7 10.18 0.78
2 0 8 52.96 2.15
2 1 8 57.6 2.25
2 2 8 23.09 1.55
2 3 8 28.43 1.64
2 4 8 15.6 1.35
2 5 8 55.36 1.49
2 6 8 46.08 1.41
2 7 8 40.96 1.34
2 9 8 11.52 0.78
2 10 8 1.38 0.48
2 11 8 8.35 0.76
2 13 8 30.77 1.34
2 14 8 9.77 0.79
2 15 8 6.87 0.68
2 16 8 3.18 0.46
2 17 8 23.02 1.11
2 18 8 1.88 0.42
2 19 8 6.58 0.53
2 0 9 74.14 2.71
2 1 9 17.12 1.47
2 2 9 107.12 3.36
2 3 9 5.25 1.08
2 4 9 47.77 2.25
2 5 9 11.23 1.36
2 6 9 48.83 1.54
2 7 9 10.35 0.9
2 8 9 3.29 0.53
2 9 9 37.57 1.4
2 10 9 13.83 1
2 11 9 15.31 1.05
2 12 9 17.01 1.11
2 13 9 34.41 1.43
2 14 9 70.81 1.94
2 16 9 15.21 0.99
2 17 9 4.24 0.51
2 0 10 48.67 2.4
2 1 10 65.8 2.77
2 2 10 2.8 1.16
2 3 10 6.43 1.31
2 4 10 4.59 1.23
2 5 10 45.71 2.36
2 6 10 16.62 1.63
2 7 10 25.68 1.29
2 8 10 29.77 1.37
2 9 10 11.97 0.9
2 10 10 32.81 1.42
2 11 10 43.41 1.55
2 12 10 47.33 1.65
2 13 10 6.95 0.67
2 14 10 16.74 1.13
2 15 10 2.89 0.56
2 0 11 12.33 1.64
2 1 11 9.71 1.56
2 2 11 3.24 1.34
2 3 11 7.11 1.43
2 6 11 13.36 1.64
2 8 11 5.54 0.64
2 10 11 6.17 0.77
2 11 11 4.49 0.6
2 0 12 45.71 2.59
2 1 12 20.15 2.05
2 2 12 6.09 1.59
2 3 12 41.73 2.48
2 4 12 10.95 1.74
2 6 12 28.73 2.17
3 1 0 30.34 0.5
3 3 0 67.69 0.86
3 4 0 404.59 3.95
3 5 0 204.07 2.17
3 6 0 38.58 0.68
3 7 0 237.81 2.55
3 8 0 79.01 1.13
3 9 0 105.43 1.41
3 10 0 29.39 0.71
3 11 0 245.95 2.8
3 12 0 8.01 0.52
3 13 0 2.68 0.44
3 14 0 3.67 0.48
3 15 0 23.51 0.83
3 16 0 41.99 1.11
3 17 0 41.38 1.14
3 18 0 2.09 0.37
3 19 0 2.88 0.41
3 20 0 27.32 1.05
3 21 0 29.72 1.12
3 22 0 3.99 0.47
3 24 0 7.88 0.64
3 25 0 28.93 1.4
3 0 1 171.86 1.82
3 1 1 361 3.56
3 2 1 57.69 0.77
3 3 1 424.89 4.16
3 4 1 80.11 1.02
3 5 1 23.77 0.52
3 6 1 67.46 0.96
3 7 1 155.76 1.82
3 8 1 41.78 0.79
3 9 1 373.82 3.93
3 10 1 36.11 0.8
3 11 1 52.42 1.01
3 12 1 53.23 1.06
3 13 1 87.61 1.48
3 14 1 26.48 0.84
3 15 1 1.95 0.36
3 16 1 38.52 1.07
3 17 1 29.53 0.99
3 18 1 49.97 1.3
3 19 1 19.3 0.9
3 20 1 3.62 0.44
3 21 1 66.21 1.6
3 22 1 60.64 1.6
3 23 1 15.13 0.93
3 24 1 29.18 1.18
3 25 1 7.63 0.75
3 1 2 175.83 1.92
3 2 2 265.92 2.73
3 3 2 261.03 2.71
3 4 2 53.88 0.84
3 5 2 308.07 3.19
3 6 2 624.21 6.12
3 7 2 7.14 0.41
3 8 2 87.06 1.24
3 9 2 60.88 1.03
3 10 2 248.4 2.82
3 11 2 33.86 0.83
3 12 2 104.13 1.59
3 13 2 25.65 0.8
3 14 2 6.5 0.58
3 15 2 12.62 0.7
3 16 2 35.91 1.04
3 17 2 27.91 0.98
3 18 2 8.85 0.7
3 19 2 5.41 0.53
3 20 2 11.31 0.82
3 22 2 2.75 0.44
3 23 2 9.6 0.85
3 24 2 26.97 1.15
3 25 2 4.44 0.55
3 0 3 179.41 2
3 1 3 245.98 2.61
3 2 3 17.02 0.5
3 3 3 163.58 1.88
3 4 3 12.34 0.47
3 5 3 209.38 2.32
3 6 3 3.32 0.37
3 7 3 248.81 2.76
3 8 3 42.14 0.85
3 9 3 25.59 0.71
3 10 3 11.31 0.55
3 11 3 74.25 1.29
3 12 3 39.29 0.95
3 13 3 12.15 0.65
3 14 3 8.87 0.58
3 15 3 11.77 0.71
3 16 3 2 0.38
3 17 3 8 0.62
3 19 3 10.06 0.8
3 20 3 5.98 0.51
3 21 3 1.58 0.41
3 22 3 6.25 0.53
3 23 3 38.94 1.35
3 24 3 8.32 0.71
3 0 4 11.33 0.46
3 1 4 110.86 1.44
3 2 4 30.29 0.68
3 3 4 78.35 1.16
3 4 4 24.45 0.63
3 5 4 264.65 2.92
3 6 4 78.24 1.22
3 7 4 58.23 1.05
3 8 4 52.71 1.03
3 9 4 65.91 1.19
3 10 4 20.53 0.71
3 11 4 28.38 0.86
3 12 4 29.32 0.88
3 13 4 102.39 1.71
3 14 4 9.83 0.67
3 15 4 36.76 1.09
3 16 4 16.91 0.82
3 17 4 31.48 1.09
3 18 4 24.92 1.03
3 19 4 16.5 0.92
3 20 4 20.39 0.99
3 21 4 25.18 1.09
3 22 4 6.82 0.61
3 23 4 9.83 0.84
3 24 4 1.07 0.4
3 0 5 48.86 0.95
3 1 5 43.74 0.9
3 2 5 34.69 0.81
3 3 5 71.65 1.19
3 4 5 70.08 1.19
3 5 5 70.81 1.21
3 6 5 43.04 0.94
3 7 5 119.9 1.72
3 8 5 183.08 2.34
3 9 5 1.78 0.46
3 10 5 130.62 1.94
3 11 5 7.14 0.52
3 12 5 120.79 1.92
3 13 5 10.05 0.7
3 14 5 62.54 1.43
3 15 5 43.26 1.22
3 16 5 9.79 0.76
3 17 5 3.07 0.43
3 18 5 6.26 0.52
3 19 5 10.37 0.76
3 20 5 2.77 0.45
3 21 5 3.5 0.47
3 22 5 14.8 0.97
3 23 5 3.69 0.47
3 1 6 3.7 0.5
3 2 6 40.79 1.07
3 3 6 4.72 0.55
3 4 6 9.35 0.66
3 5 6 20.57 0.84
3 6 6 18.23 0.84
3 7 6 38.48 1.12
3 8 6 18.36 0.78
3 9 6 31.7 0.95
3 10 6 23.47 0.87
3 11 6 66.39 1.42
3 12 6 3.53 0.42
3 13 6 55.29 1.37
3 14 6 25.18 1
3 15 6 7.03 0.57
3 16 6 40.78 1.28
3 17 6 23.45 1.04
3 18 6 9.96 0.75
3 19 6 21.34 1.06
3 20 6 62.07 1.62
3 21 6 5.65 0.52
3 22 6 5.04 0.5
3 0 7 5.79 0.98
3 2 7 148.09 3.65
3 3 7 28.37 1.05
3 4 7 9.43 0.77
3 5 7 31.38 1.1
3 6 7 11.75 0.83
3 7 7 35.22 1.18
3 8 7 10.91 0.84
3 9 7 106.55 2.09
3 10 7 49.53 1.28
3 11 7 6.03 0.47
3 12 7 2.34 0.39
3 13 7 37.28 1.2
3 14 7 47.99 1.35
3 15 7 36.39 1.24
3 16 7 2.72 0.44
3 17 7 2.77 0.44
3 18 7 7.66 0.62
3 19 7 20.39 1.06
3 20 7 8.97 0.73
3 21 7 5.09 0.5
3 0 8 2.09 0.98
3 1 8 111.35 3.25
3 2 8 58.2 2.3
3 3 8 44.86 2.05
3 4 8 38.15 1.28
3 5 8 37.73 1.28
3 6 8 25.65 1.11
3 7 8 29.61 1.18
3 8 8 32.68 1.26
3 9 8 21.7 1.1
3 10 8 4.31 0.55
3 11 8 97.81 2.17
3 12 8 16.9 1.05
3 13 8 6.18 0.57
3 14 8 4.49 0.48
3 15 8 17.63 0.97
3 16 8 15.02 0.97
3 17 8 10.97 0.88
3 18 8 8.14 0.63
3 19 8 22.59 1.09
3 0 9 67.53 2.65
3 1 9 11.69 1.38
3 2 9 18.97 1.58
3 3 9 13.65 1.46
3 4 9 99.77 3.3
3 6 9 7.92 0.65
3 7 9 8.83 0.73
3 8 9 42.32 1.5
3 9 9 6.16 0.63
3 10 9 27.35 1.27
3 11 9 4.16 0.58
3 12 9 4.83 0.6
3 13 9 1.51 0.52
3 14 9 30.49 1.33
3 15 9 6.28 0.6
3 16 9 8.83 0.65
3 17 9 21.32 1.06
3 1 10 56.16 2.55
3 2 10 27.17 1.96
3 3 10 80.71 3.11
3 4 10 11.69 1.54
3 5 10 7 1.38
3 6 10 22.84 1.22
3 7 10 11.45 0.87
3 8 10 7.1 0.67
3 9 10 32.66 1.42
3 10 10 7.43 0.82
3 11 10 4.48 0.6
3 12 10 1.1 0.5
3 13 10 18.65 1.19
3 14 10 16.61 1.11
3 1 11 10.74 1.64
3 2 11 14.83 1.69
3 3 11 34.1 2.23
3 4 11 16.58 1.83
3 5 11 15.32 1.71
3 6 11 11.88 1.66
3 7 11 22.08 1.26
3 8 11 6.38 0.79
3 9 11 10.53 0.82
3 10 11 8.79 0.85
3 11 11 9.2 2.88
3 0 12 5.4 1.63
3 1 12 7.16 1.64
3 2 12 3.2 1.5
4 0 0 384.16 3.81
4 1 0 378.42 3.8
4 2 0 39.43 0.69
4 3 0 1.72 0.3
4 4 0 36.22 0.69
4 5 0 15.1 0.5
4 6 0 128.92 1.6
4 7 0 86.25 1.24
4 8 0 129.68 1.67
4 9 0 127.5 1.69
4 10 0 67.67 1.17
4 11 0 12.4 0.6
4 12 0 235.38 2.91
4 13 0 67.76 1.28
4 14 0 2.76 0.36
4 15 0 12.38 0.7
4 16 0 88.64 1.66
4 17 0 1.16 0.34
4 18 0 2 0.38
4 19 0 7.1 0.65
4 21 0 7.82 0.61
4 23 0 4.69 0.5
4 24 0 21.39 1.06
4 0 1 1.43 0.29
4 1 1 145.48 1.67
4 2 1 33.89 0.65
4 3 1 147.5 1.71
4 4 1 11.88 0.45
4 5 1 58.76 0.93
4 6 1 42.58 0.8
4 7 1 240.3 2.67
4 8 1 42.06 0.85
4 9 1 4.16 0.4
4 10 1 33.52 0.81
4 11 1 260.81 3.03
4 12 1 66.34 1.25
4 13 1 42.06 1.03
4 14 1 45.19 1.1
4 15 1 44.07 1.14
4 16 1 51.36 1.26
4 17 1 16.69 0.85
4 18 1 30.36 1.05
4 19 1 41.72 1.25
4 20 1 31.99 1.16
4 21 1 7.56 0.68
4 22 1 13.99 0.94
4 23 1 2.14 0.44
4 24 1 19.2 1.03
4 25 1 5.12 0.57
4 0 2 10.51 0.43
4 1 2 258.72 2.77
4 2 2 9.48 0.44
4 3 2 73.56 1.06
4 4 2 195.76 2.2
4 5 2 132.93 1.67
4 6 2 31.66 0.71
4 7 2 173.34 2.1
4 8 2 158.05 1.97
4 9 2 5.52 0.44
4 10 2 40.35 0.91
4 11 2 18.31 0.68
4 12 2 45.34 1.04
4 14 2 14.12 0.72
4 15 2 14.74 0.76
4 16 2 16.2 0.82
4 17 2 18.95 0.89
4 18 2 5.99 0.53
4 19 2 10.97 0.81
4 20 2 8.26 0.6
4 21 2 9.31 0.81
4 22 2 9.51 0.65
4 23 2 17.35 1.01
4 24 2 1.58 0.41
4 0 3 4.58 0.38
4 1 3 219.85 2.43
4 2 3 37.62 0.77
4 3 3 454.09 4.59
4 4 3 93.09 1.31
4 5 3 106.16 1.46
4 6 3 5.31 0.42
4 7 3 59.19 1.06
4 8 3 85.28 1.36
4 9 3 31.31 0.81
4 10 3 16.57 0.66
4 11 3 29.07 0.85
4 12 3 41.17 1.04
4 13 3 12.06 0.69
4 14 3 22.04 0.87
4 15 3 72.11 1.49
4 16 3 26.77 0.99
4 17 3 0.94 0.35
4 18 3 21.16 0.97
4 19 3 34.31 1.17
4 20 3 12.93 0.86
4 21 3 33.06 1.23
4 22 3 24.91 1.14
4 23 3 0.97 0.4
4 24 3 13.66 0.95
4 0 4 75.67 1.17
4 1 4 121.41 1.6
4 2 4 33.4 0.77
4 3 4 94.7 1.37
4 4 4 34.37 0.79
4 5 4 85.48 1.33
4 6 4 54.9 1.05
4 7 4 42.07 0.94
4 8 4 8.74 0.53
4 9 4 1.41 0.44
4 10 4 35.34 0.94
4 11 4 24.04 0.82
4 12 4 67.54 1.37
4 13 4 25.55 0.91
4 14 4 9 0.62
4 15 4 39.2 1.17
4 16 4 52.8 1.37
4 17 4 58.32 1.48
4 18 4 1.55 0.4
4 19 4 8.32 0.62
4 20 4 22.06 1.07
4 21 4 19.7 1.02
4 22 4 2.04 0.46
4 23 4 62.64 1.62
4 0 5 27.34 0.76
4 1 5 22.54 0.7
4 2 5 6.07 0.48
4 3 5 160.45 2.07
4 4 5 28 0.78
4 5 5 82.91 1.38
4 6 5 13.49 0.61
4 7 5 34.48 0.92
4 8 5 47.22 1.07
4 9 5 43.99 1.09
4 10 5 26.59 0.87
4 11 5 9.68 0.65
4 12 5 18.92 0.85
4 13 5 6.59 0.58
4 14 5 8.33 0.63
4 15 5 1.92 0.39
4 16 5 20.76 0.97
4 17 5 10.15 0.79
4 18 5 2.26 0.43
4 19 5 5.34 0.51
4 20 5 28.45 1.17
4 21 5 2.18 0.43
4 22 5 1.06 0.4
4 1 6 86.63 1.47
4 2 6 15 0.67
4 3 6 25.2 0.82
4 4 6 11.62 0.65
4 5 6 135.18 1.98
4 6 6 40.44 1.05
4 7 6 39.58 1.06
4 8 6 53.1 1.25
4 9 6 132.94 2.08
4 10 6 25.88 0.96
4 11 6 35.79 1.07
4 12 6 61.9 1.44
4 13 6 48.31 1.3
4 14 6 12.24 0.81
4 15 6 53.53 1.44
4 16 6 17.9 0.95
4 17 6 41.48 1.33
4 18 6 26.05 1.11
4 19 6 36.31 1.27
4 20 6 1.82 0.42
4 21 6 22.03 1.08
4 0 7 135.47 2.06
4 1 7 9.24 0.7
4 2 7 12.58 0.82
4 3 7 11.87 0.8
4 4 7 63.9 1.55
4 5 7 16.07 0.89
4 6 7 19.74 0.84
4 7 7 25.63 0.95
4 8 7 50.6 1.29
4 9 7 6.11 0.58
4 10 7 43.04 1.21
4 11 7 51.07 1.36
4 12 7 39.23 1.21
4 13 7 10.31 0.72
4 14 7 30 1.15
4 15 7 2.08 0.42
4 16 7 3.3 0.46
4 17 7 9.22 0.76
4 18 7 5.59 0.52
4 19 7 12.67 0.89
4 20 7 1.91 0.42
4 0 8 43.42 2.05
4 1 8 19.25 1.22
4 2 8 13.46 0.89
4 3 8 11.58 0.87
4 4 8 28.61 1.16
4 5 8 4.32 0.53
4 6 8 8.86 0.75
4 7 8 31.95 1.27
4 8 8 3.66 0.53
4 9 8 87.39 2.07
4 10 8 18.79 0.97
4 11 8 8.67 0.72
4 12 8 0.83 0.39
4 13 8 51.52 1.48
4 14 8 33.45 1.24
4 15 8 2.2 0.44
4 16 8 9.62 0.77
4 18 8 15.94 0.97
4 0 9 18.87 1.62
4 1 9 13.44 1.46
4 2 9 13.05 1.43
4 3 9 23.71 1.18
4 4 9 58.17 1.68
4 5 9 13.62 0.99
4 6 9 35.5 1.42
4 7 9 5.49 0.61
4 8 9 83.6 2.08
4 9 9 16.7 1.08
4 10 9 19.53 1.13
4 12 9 23.36 1.27
4 13 9 9.12 0.75
4 14 9 11.54 0.88
4 15 9 26.02 1.13
4 16 9 2.41 0.44
4 1 10 81.44 3.16
4 2 10 13.93 1.61
4 3 10 3.04 1.26
4 4 10 29.68 1.34
4 5 10 56.65 1.79
4 6 10 27.59 1.34
4 7 10 15.29 1.09
4 8 10 15.2 1.09
4 10 10 14.79 1.09
4 11 10 6.93 0.67
4 12 10 1.59 0.53
4 13 10 8.52 0.7
4 0 11 27.34 2.09
4 2 11 3.11 1.32
4 3 11 8.85 1.54
4 4 11 32.38 2.21
4 5 11 12.88 1.32
4 7 11 6.63 0.66
4 8 11 20.2 1.25
4 9 11 9.65 0.84
5 1 0 39.38 0.76
5 2 0 42.79 0.81
5 3 0 226.54 2.52
5 4 0 59.83 1
5 5 0 71.65 1.12
5 7 0 11.56 0.53
5 8 0 16.03 0.6
5 9 0 25.07 0.73
5 10 0 37.82 0.91
5 11 0 36.19 0.94
5 12 0 1.59 0.47
5 13 0 11.99 0.69
5 14 0 51.61 1.23
5 15 0 15.11 0.81
5 16 0 4.5 0.42
5 17 0 10.31 0.68
5 18 0 6.17 0.63
5 21 0 0.9 0.39
5 22 0 7.79 0.62
5 24 0 2.02 0.43
5 0 1 5.85 0.4
5 1 1 131.1 1.63
5 2 1 89.18 1.26
5 3 1 374.23 3.83
5 4 1 5.2 0.4
5 5 1 34.99 0.76
5 6 1 69.75 1.14
5 7 1 151.4 1.92
5 8 1 3.14 0.41
5 9 1 57.27 1.11
5 10 1 12.48 0.6
5 11 1 67.14 1.26
5 12 1 21.34 0.8
5 13 1 18.64 0.82
5 14 1 15.89 0.77
5 15 1 213.87 2.87
5 16 1 60.26 1.41
5 17 1 4.18 0.44
5 18 1 7.57 0.67
5 19 1 52.64 1.46
5 20 1 50.77 1.43
5 21 1 3.45 0.47
5 22 1 0.89 0.4
5 23 1 1.85 0.42
5 24 1 14.38 0.92
5 0 2 324.64 3.44
5 1 2 166.23 2.01
5 3 2 247.64 2.79
5 4 2 84.2 1.27
5 5 2 41.82 0.87
5 6 2 6.47 0.45
5 7 2 12.7 0.57
5 8 2 28.62 0.79
5 9 2 36.76 0.9
5 10 2 1.37 0.43
5 11 2 15.97 0.71
5 12 2 122.14 1.9
5 14 2 7.42 0.65
5 15 2 3.02 0.39
5 16 2 59.5 1.43
5 17 2 14.45 0.84
5 18 2 11.35 0.8
5 19 2 29.81 1.12
5 20 2 2.12 0.43
5 21 2 38.38 1.3
5 22 2 1.74 0.42
5 23 2 5.26 0.56
5 24 2 7.23 0.88
5 0 3 30.55 0.75
5 1 3 195.1 2.32
5 2 3 24.04 0.68
5 3 3 9.39 0.5
5 4 3 1.33 0.38
5 5 3 67.43 1.16
5 6 3 34.17 0.84
5 7 3 62.94 1.17
5 8 3 18.27 0.68
5 9 3 8.91 0.58
5 10 3 42.49 1.04
5 11 3 25.45 0.87
5 12 3 26.97 0.92
5 13 3 18.8 0.83
5 14 3 46.23 1.21
5 15 3 3.66 0.41
5 16 3 49.98 1.36
5 17 3 23.32 1
5 18 3 23.54 1.04
5 19 3 4.35 0.48
5 20 3 55.57 1.54
5 21 3 8.11 0.64
5 22 3 4.72 0.5
5 23 3 8.51 0.63
5 1 4 68.66 1.19
5 2 4 42.88 0.93
5 3 4 27.81 0.79
5 4 4 16.97 0.65
5 5 4 6.13 0.5
5 6 4 27.88 0.82
5 7 4 29.57 0.85
5 8 4 87.86 1.5
5 9 4 2.62 0.37
5 10 4 109.97 1.8
5 11 4 34 1.02
5 12 4 84.17 1.6
5 13 4 4.32 0.42
5 14 4 84.58 1.69
5 15 4 20.32 0.95
5 16 4 21.8 0.98
5 17 4 8.11 0.68
5 18 4 25.07 1.07
5 19 4 74.39 1.76
5 21 4 43.38 1.38
5 22 4 11.53 0.92
5 0 5 6.94 0.55
5 1 5 182.8 2.34
5 2 5 31.25 0.87
5 3 5 15.81 0.66
5 4 5 71.62 1.34
5 5 5 58.46 1.22
5 6 5 18.29 0.77
5 7 5 33.88 0.96
5 8 5 49.32 1.18
5 9 5 10.72 0.69
5 10 5 18.6 0.82
5 11 5 20.04 0.88
5 12 5 0.95 0.34
5 13 5 17.45 0.89
5 14 5 41.51 1.22
5 15 5 1.29 0.39
5 16 5 18.38 0.93
5 17 5 3.61 0.46
5 18 5 29 1.15
5 19 5 3.09 0.47
5 20 5 11.71 0.92
5 21 5 8.66 0.65
5 0 6 46.5 1.13
5 1 6 44.62 1.09
5 2 6 10.89 0.68
5 3 6 52.97 1.21
5 4 6 48.86 1.18
5 5 6 78.8 1.52
5 6 6 13.19 0.72
5 7 6 102.81 1.79
5 8 6 21.57 0.89
5 9 6 20.68 0.87
5 10 6 67.74 1.49
5 11 6 78.63 1.64
5 13 6 66.05 1.57
5 14 6 52.94 1.44
5 15 6 15.01 0.89
5 16 6 5.23 0.5
5 17 6 51.85 1.5
5 18 6 7.11 0.63
5 19 6 5.13 0.51
5 0 7 1.46 0.36
5 1 7 29.36 0.98
5 2 7 16.42 0.83
5 3 7 3.95 0.42
5 4 7 105.62 1.85
5 5 7 10.17 0.66
5 6 7 20.63 0.89
5 7 7 9.54 0.73
5 8 7 98.36 1.86
5 9 7 11.2 0.75
5 10 7 1.98 0.4
5 11 7 4.19 0.46
5 12 7 13.02 0.78
5 13 7 15.93 0.91
5 14 7 6.29 0.53
5 15 7 17.97 0.98
5 16 7 7.71 0.73
5 17 7 4.82 0.5
5 18 7 2.88 0.45
5 0 8 35.96 1.15
5 1 8 46.89 1.29
5 2 8 3.19 0.42
5 4 8 19.15 0.94
5 5 8 137.68 2.29
5 7 8 5.16 0.48
5 8 8 2.89 0.43
5 9 8 23.71 1.04
5 10 8 2.02 0.42
5 11 8 12.49 0.86
5 12 8 7.93 0.62
5 13 8 31.87 1.24
5 14 8 8.01 0.64
5 15 8 8.66 0.64
5 16 8 11.73 0.88
5 17 8 57.84 1.56
5 1 9 29.52 1.12
5 2 9 34.84 1.39
5 3 9 5.4 0.6
5 4 9 6.11 0.62
5 5 9 13.93 1.04
5 6 9 26.77 1.26
5 7 9 9.36 0.82
5 8 9 1.09 0.5
5 9 9 1.3 0.41
5 10 9 20.95 1.05
5 11 9 15.24 0.96
5 12 9 1.68 0.42
5 13 9 8.62 0.65
5 14 9 6.67 0.54
5 15 9 2.58 0.44
5 0 10 73.64 3.07
5 1 10 5.11 0.88
5 2 10 2.79 0.56
5 3 10 50.19 1.69
5 4 10 24.14 1.26
5 5 10 29.46 1.42
5 6 10 6.49 0.67
5 7 10 17.52 1.16
5 8 10 6.85 0.67
5 9 10 32.12 1.39
5 11 10 1.99 0.52
5 12 10 5.77 0.52
5 0 11 3.67 1.49
5 1 11 23.38 1.96
5 2 11 12.06 1.58
5 3 11 16.07 1.15
5 4 11 10.79 0.89
5 6 11 39.01 1.5
5 7 11 2.38 0.55
6 0 0 131.59 1.72
6 1 0 64.9 1.1
6 2 0 4.74 0.43
6 3 0 30.99 0.78
6 4 0 9.72 0.51
6 5 0 74.83 1.26
6 6 0 69.02 1.22
6 7 0 82.56 1.39
6 8 0 57.69 1.15
6 10 0 86.04 1.53
6 12 0 62.69 1.33
6 13 0 21 0.88
6 14 0 9.04 0.63
6 15 0 27.84 1
6 16 0 7.13 0.62
6 17 0 8.74 0.68
6 18 0 20.76 1.01
6 19 0 6.82 0.67
6 21 0 2.22 0.44
6 22 0 23.04 1.08
6 0 1 38.69 0.86
6 1 1 115.97 1.6
6 2 1 83.81 1.31
6 3 1 74.48 1.23
6 4 1 85.66 1.35
6 5 1 102.27 1.53
6 6 1 9.27 0.53
6 7 1 59.7 1.16
6 8 1 51.66 1.1
6 9 1 1.43 0.46
6 10 1 1.43 0.33
6 11 1 26.07 0.88
6 12 1 12.5 0.73
6 13 1 116.95 1.94
6 14 1 40.23 1.15
6 15 1 18.15 0.87
6 16 1 11.48 0.77
6 17 1 70.31 1.61
6 18 1 64.88 1.59
6 19 1 18.11 0.96
6 20 1 12.88 0.9
6 21 1 7.86 0.64
6 22 1 21.33 1.07
6 23 1 9.13 0.85
6 0 2 18.78 0.64
6 1 2 111.46 1.59
6 2 2 170.3 2.15
6 3 2 3.24 0.42
6 5 2 46.27 1
6 6 2 9.29 0.55
6 7 2 17.54 0.7
6 8 2 45.5 1.06
6 9 2 5.33 0.56
6 10 2 103.94 1.73
6 11 2 3.62 0.4
6 12 2 29.8 1
6 13 2 10.52 0.66
6 14 2 89.11 1.75
6 15 2 1 0.36
6 16 2 6.81 0.57
6 17 2 13.93 0.87
6 18 2 7.29 0.6
6 19 2 6.77 0.59
6 20 2 1.79 0.43
6 21 2 8.54 0.75
6 22 2 6.08 0.53
6 23 2 13.13 1.51
6 0 3 12 0.58
6 1 3 97.02 1.5
6 2 3 16.18 0.66
6 3 3 194.9 2.41
6 4 3 65.02 1.22
6 5 3 4.43 0.5
6 6 3 23.83 0.78
6 7 3 56.04 1.18
6 8 3 22.27 0.81
6 9 3 24.72 0.87
6 10 3 1.26 0.35
6 11 3 6.66 0.51
6 12 3 20.18 0.88
6 13 3 4.28 0.42
6 14 3 46.78 1.3
6 15 3 31.44 1.11
6 16 3 27.61 1.09
6 17 3 12.46 0.85
6 18 3 67.75 1.67
6 19 3 45.75 1.43
6 20 3 2.94 0.46
6 21 3 20.38 1.08
6 22 3 28.15 1.17
6 0 4 1.02 0.42
6 1 4 91.48 1.52
6 2 4 20.44 0.74
6 3 4 55.26 1.16
6 5 4 35.83 0.98
6 6 4 65.17 1.32
6 7 4 4.8 0.41
6 8 4 16.45 0.77
6 9 4 38.89 1.09
6 10 4 47.01 1.22
6 11 4 2.42 0.37
6 12 4 26.6 0.99
6 13 4 4.55 0.45
6 14 4 38.61 1.22
6 15 4 3.71 0.45
6 16 4 31.07 1.15
6 17 4 78.15 1.77
6 18 4 9.62 0.77
6 19 4 30.56 1.22
6 20 4 12.03 0.9
6 21 4 53.02 1.51
6 0 5 13.91 0.73
6 1 5 63.26 1.3
6 2 5 19.13 0.78
6 3 5 103.17 1.73
6 4 5 18.57 0.8
6 5 5 4.07 0.4
6 6 5 42.64 1.11
6 7 5 9.88 0.69
6 9 5 32.81 1.06
6 10 5 2.23 0.38
6 11 5 18.81 0.9
6 12 5 22.54 0.97
6 13 5 9.28 0.61
6 14 5 22.02 1.01
6 15 5 1.86 0.41
6 16 5 16.37 0.97
6 17 5 1.84 0.42
6 18 5 17.27 0.98
6 19 5 5.85 0.53
6 0 6 49.51 1.22
6 1 6 98.36 1.74
6 2 6 70.41 1.47
6 3 6 54.38 1.29
6 4 6 19.12 0.85
6 5 6 77.46 1.57
6 6 6 71.89 1.53
6 7 6 6.17 0.47
6 8 6 10.54 0.76
6 9 6 73.94 1.62
6 10 6 12.37 0.84
6 11 6 32.3 1.14
6 12 6 39.42 1.24
6 13 6 33.82 1.21
6 14 6 12.82 0.91
6 15 6 42.37 1.34
6 16 6 28.05 1.15
6 17 6 22.19 1.07
6 18 6 8.4 0.58
6 19 6 13.93 0.92
6 0 7 17.24 0.84
6 1 7 2.19 0.38
6 2 7 48.61 1.29
6 3 7 11.5 0.78
6 4 7 7.96 0.64
6 5 7 20.14 0.9
6 6 7 95.97 1.85
6 7 7 2.25 0.41
6 8 7 18.52 0.92
6 9 7 4.96 0.53
6 10 7 56.46 1.48
6 11 7 4.99 0.49
6 12 7 17.04 0.98
6 13 7 15.13 0.95
6 14 7 13.46 0.93
6 15 7 3.43 0.47
6 17 7 11.59 0.85
6 18 7 6.9 0.54
6 0 8 27.69 1.06
6 1 8 1.22 0.38
6 2 8 14.42 0.85
6 3 8 48.17 1.35
6 4 8 7.59 0.67
6 5 8 3.32 0.44
6 6 8 12.87 0.87
6 7 8 51.93 1.43
6 9 8 3.07 0.46
6 10 8 7.64 0.64
6 11 8 17.23 1.01
6 12 8 2.35 0.45
6 13 8 10.22 0.73
6 14 8 14.93 0.95
6 15 8 40.35 1.34
6 16 8 20.67 1.06
6 0 9 38.19 1.28
6 1 9 1.09 0.4
6 2 9 11.18 0.85
6 3 9 10.96 0.8
6 4 9 8.78 0.74
6 5 9 2.65 0.44
6 6 9 12.78 0.88
6 7 9 6.87 0.55
6 8 9 29.43 1.16
6 9 9 5.7 0.52
6 10 9 41.23 1.37
6 11 9 6.42 0.6
6 12 9 35.65 1.28
6 13 9 13.65 0.93
6 0 10 4.83 0.51
6 1 10 42.55 1.36
6 2 10 44.83 1.42
6 3 10 1.58 0.45
6 4 10 6.88 0.55
6 5 10 50.53 1.48
6 6 10 8.38 0.65
6 7 10 22.09 1.09
6 8 10 1.54 0.42
6 9 10 4.44 0.49
6 0 11 7.28 0.62
6 1 11 28.99 1.36
6 2 11 4.2 0.59
7 2 0 69.94 1.27
7 3 0 13.38 0.61
7 4 0 3.73 0.5
7 5 0 51.46 1.13
7 6 0 20.66 0.78
7 7 0 2.37 0.35
7 8 0 33.93 0.97
7 9 0 42.03 1.09
7 10 0 95.93 1.71
7 11 0 32.03 1.03
7 12 0 23.77 0.93
7 14 0 17.05 0.87
7 15 0 14.81 0.87
7 16 0 2.43 0.43
7 17 0 11.25 0.84
7 18 0 1.2 0.41
7 19 0 3.03 0.46
7 20 0 24.31 1.09
7 21 0 17.46 1
7 22 0 1.4 0.43
7 0 1 214.23 2.64
7 1 1 55.2 1.12
7 2 1 15.56 0.67
7 3 1 40.59 0.97
7 4 1 68.45 1.28
7 5 1 71.33 1.33
7 6 1 38.99 1
7 7 1 22.34 0.81
7 8 1 1.12 0.34
7 9 1 98 1.71
7 10 1 18.63 0.83
7 11 1 17.78 0.84
7 13 1 36.15 1.13
7 14 1 17.67 0.94
7 15 1 10.49 0.77
7 16 1 16.95 0.94
7 17 1 35.15 1.23
7 18 1 41.86 1.35
7 19 1 25.73 1.14
7 20 1 10.93 0.88
7 21 1 24.64 1.13
7 22 1 32.84 1.25
7 0 2 11.23 0.62
7 1 2 2 0.47
7 2 2 37.9 0.96
7 3 2 28.43 0.85
7 4 2 12.34 0.65
7 5 2 49.4 1.12
7 6 2 203.91 2.63
7 7 2 6.92 0.49
7 8 2 17.08 0.79
7 9 2 23.02 0.91
7 10 2 139.03 2.17
7 11 2 10.41 0.65
7 12 2 56.97 1.39
7 13 2 5.15 0.51
7 14 2 5.63 0.49
7 15 2 19.54 0.93
7 16 2 14.82 0.91
7 17 2 6.01 0.58
7 18 2 10.97 0.85
7 19 2 1.62 0.42
7 20 2 1.84 0.44
7 21 2 0.95 0.4
7 0 3 3.67 0.52
7 1 3 115.35 1.8
7 2 3 29.46 0.9
7 3 3 17.52 0.76
7 4 3 23.97 0.84
7 5 3 100.32 1.69
7 6 3 43.27 1.1
7 7 3 11.73 0.69
7 8 3 36.57 1.06
7 9 3 5.55 0.5
7 10 3 5.85 0.5
7 11 3 5.81 0.58
7 12 3 14.53 0.82
7 13 3 20.85 0.96
7 14 3 41.56 1.29
7 15 3 15.95 0.91
7 16 3 23.99 1.11
7 17 3 31.69 1.22
7 18 3 7.72 0.63
7 19 3 20.63 1.06
7 20 3 12.35 0.9
7 21 3 8.65 0.73
7 0 4 2.55 0.37
7 1 4 64.72 1.34
7 2 4 11.66 0.7
7 3 4 22.83 0.87
7 4 4 55.66 1.26
7 5 4 50.65 1.24
7 6 4 47.4 1.2
7 7 4 4.41 0.43
7 8 4 8.93 0.63
7 9 4 16.11 0.83
7 10 4 11.52 0.76
7 11 4 13.66 0.83
7 12 4 26.58 1.05
7 13 4 38.42 1.27
7 14 4 11.52 0.85
7 15 4 37.29 1.28
7 16 4 34.6 1.23
7 17 4 22.61 1.05
7 18 4 15.71 0.96
7 19 4 25.01 1.16
7 20 4 1.89 0.43
7 0 5 2.93 0.39
7 1 5 21.51 0.87
7 2 5 21.17 0.85
7 3 5 7.07 0.6
7 4 5 30.65 1.02
7 5 5 31.83 1.04
7 6 5 26.61 0.98
7 7 5 43.83 1.23
7 8 5 61.09 1.46
7 9 5 4.71 0.46
7 10 5 43.12 1.27
7 11 5 11.73 0.83
7 12 5 27.46 1.12
7 13 5 4.47 0.48
7 14 5 51.89 1.46
7 15 5 3.07 0.46
7 16 5 11.87 0.81
7 17 5 3.93 0.48
7 18 5 5.53 0.52
7 19 5 5.35 0.51
7 0 6 14.03 0.8
7 1 6 59.81 1.42
7 2 6 75.19 1.6
7 3 6 56.21 1.4
7 4 6 53.44 1.35
7 5 6 6.33 0.53
7 6 6 11.82 0.81
7 7 6 32.8 1.15
7 8 6 27.67 1.08
7 9 6 8.68 0.7
7 10 6 7.29 0.67
7 11 6 24.59 1.05
7 12 6 6.51 0.59
7 13 6 13.07 0.89
7 14 6 10.53 0.76
7 15 6 17.02 1
7 16 6 18.43 1.02
7 17 6 14.43 0.96
7 18 6 6.86 0.61
7 0 7 29.81 1.11
7 1 7 1.19 0.37
7 2 7 70.51 1.62
7 3 7 7.98 0.68
7 4 7 3.05 0.43
7 5 7 4.69 0.47
7 6 7 3.18 0.44
7 7 7 21.7 1.01
7 8 7 34.6 1.2
7 9 7 16.72 0.98
7 10 7 36.04 1.27
7 11 7 12.56 0.8
7 12 7 20.01 1.07
7 13 7 7.44 0.62
7 14 7 28.3 1.21
7 15 7 6.7 0.54
7 0 8 1.16 0.4
7 1 8 31.41 1.19
7 2 8 69.36 1.65
7 3 8 17.75 0.96
7 4 8 6.18 0.58
7 5 8 10.22 0.82
7 6 8 4.38 0.48
7 7 8 8.44 0.72
7 8 8 3.81 0.52
7 9 8 22.88 1.09
7 10 8 2.05 0.44
7 11 8 26.9 1.15
7 12 8 16.74 0.98
7 13 8 20.51 1.03
7 14 8 2.37 0.43
7 0 9 4.54 0.5
7 1 9 4.34 0.49
7 2 9 10.16 0.78
7 3 9 7.01 0.58
7 4 9 18.79 1.02
7 5 9 10.44 0.68
7 6 9 10.07 0.72
7 7 9 3.72 0.48
7 8 9 56.16 1.56
7 10 9 30.94 1.2
7 11 9 6.44 0.53
7 1 10 30.43 1.21
7 2 10 3.84 0.47
7 3 10 64.56 1.65
7 4 10 7.28 0.55
7 6 10 9.49 0.86
8 0 0 2.3 0.36
8 1 0 1.67 0.34
8 2 0 48.29 1.13
8 4 0 2.32 0.36
8 5 0 10.36 0.67
8 6 0 128.31 2.03
8 7 0 17.57 0.83
8 8 0 5.59 0.5
8 9 0 62.67 1.44
8 10 0 17.41 0.86
8 11 0 22.27 0.94
8 12 0 9.96 0.65
8 13 0 57.11 1.46
8 14 0 1.25 0.39
8 15 0 1.75 0.41
8 16 0 35.41 1.23
8 17 0 16.63 0.95
8 19 0 9.07 0.66
8 0 1 30.79 0.96
8 1 1 30.4 0.94
8 2 1 94.15 1.64
8 3 1 1.21 0.34
8 4 1 31.9 0.98
8 5 1 65.26 1.38
8 6 1 2.49 0.39
8 7 1 21.35 0.87
8 8 1 4.99 0.48
8 9 1 59.68 1.43
8 10 1 4.24 0.43
8 11 1 3.88 0.44
8 12 1 20.74 0.96
8 13 1 25.66 1.04
8 14 1 4.44 0.48
8 15 1 18.14 0.96
8 16 1 8.53 0.74
8 17 1 17.97 1.01
8 18 1 3.84 0.48
8 19 1 39.67 1.33
8 20 1 36.62 1.27
8 1 2 3.06 0.38
8 2 2 31.57 0.98
8 3 2 11.15 0.7
8 4 2 126.55 2.02
8 5 2 3.01 0.4
8 6 2 48.83 1.23
8 7 2 12.21 0.79
8 8 2 178.4 2.57
8 9 2 1.92 0.37
8 10 2 22.63 0.96
8 11 2 4.11 0.45
8 12 2 27.12 1.06
8 13 2 2.68 0.43
8 14 2 26.6 1.09
8 15 2 3.62 0.46
8 16 2 20.77 1.03
8 17 2 5.27 0.52
8 18 2 2.86 0.46
8 19 2 2.95 0.46
8 20 2 10.19 0.75
8 0 3 81.03 1.57
8 1 3 1.86 0.37
8 2 3 14.39 0.77
8 3 3 34.19 1.03
8 4 3 41.13 1.15
8 5 3 22.49 0.92
8 6 3 35.05 1.08
8 7 3 34.2 1.09
8 8 3 20.8 0.9
8 9 3 58.42 1.44
8 10 3 69.41 1.59
8 11 3 10.74 0.8
8 12 3 61.74 1.55
8 13 3 36.69 1.23
8 14 3 15.59 0.91
8 16 3 12.01 0.88
8 17 3 3.17 0.47
8 18 3 5.84 0.52
8 19 3 1.81 0.43
8 0 4 5.39 0.48
8 1 4 13.78 0.75
8 2 4 16 0.81
8 3 4 44.91 1.21
8 4 4 23.27 0.94
8 5 4 11.82 0.73
8 6 4 6.76 0.51
8 7 4 40.26 1.21
8 8 4 63.87 1.52
8 9 4 24.04 1
8 10 4 30.13 1.12
8 11 4 53.21 1.44
8 12 4 15.34 0.9
8 13 4 24.16 1.07
8 14 4 24.47 1.11
8 15 4 38.06 1.3
8 16 4 8.23 0.58
8 17 4 7 0.61
8 1 5 22.92 0.93
8 2 5 17.83 0.87
8 3 5 14.56 0.83
8 4 5 16.74 0.86
8 5 5 33.23 1.14
8 6 5 45.61 1.3
8 7 5 8.14 0.68
8 8 5 36.23 1.22
8 9 5 13.2 0.87
8 10 5 48.56 1.41
8 11 5 1.08 0.39
8 12 5 52.74 1.51
8 13 5 1.2 0.41
8 14 5 5.37 0.52
8 15 5 13.77 0.92
8 16 5 10.02 0.86
8 17 5 5.3 0.51
8 0 6 83.85 1.77
8 1 6 1.85 0.4
8 2 6 8.24 0.68
8 3 6 12.06 0.83
8 4 6 36.2 1.2
8 5 6 21.95 1
8 6 6 16.09 0.92
8 7 6 27.76 1.15
8 8 6 12.74 0.91
8 9 6 5.17 0.5
8 11 6 28.96 1.19
8 13 6 9.61 0.72
8 14 6 3.23 0.47
8 15 6 14.5 0.96
8 16 6 18.37 1.01
8 0 7 53.7 1.5
8 1 7 4.91 0.49
8 2 7 1.28 0.4
8 3 7 11.11 0.75
8 4 7 58.8 1.54
8 5 7 0.99 0.4
8 6 7 3.05 0.45
8 7 7 35.16 1.26
8 8 7 29.83 1.19
8 9 7 10.15 0.77
8 11 7 27.79 1.2
8 12 7 32.12 1.21
8 13 7 8.5 0.64
8 14 7 12.92 0.91
8 0 8 46.56 1.42
8 1 8 43.98 1.39
8 2 8 9.8 0.75
8 3 8 34.61 1.28
8 4 8 11.52 0.8
8 5 8 13.87 0.95
8 6 8 8.73 0.62
8 7 8 13.11 0.92
8 8 8 3.04 0.46
8 9 8 3.84 0.48
8 10 8 4.37 0.49
8 11 8 22.01 1.07
8 0 9 6.13 0.53
8 1 9 5.7 0.53
8 2 9 19.57 1.06
8 3 9 16.81 0.99
8 4 9 17.57 1.02
8 6 9 43.35 1.34
8 7 9 22.75 1.08
8 8 9 7.37 0.63
9 2 0 23.63 0.93
9 4 0 174.43 2.57
9 6 0 6.56 0.53
9 7 0 7.09 0.63
9 8 0 124.02 2.16
9 9 0 4.31 0.46
9 10 0 15.48 0.89
9 11 0 24.64 1.05
9 12 0 5.44 0.5
9 13 0 6.66 0.54
9 14 0 41.5 1.35
9 15 0 36.83 1.28
9 18 0 4.58 0.49
9 0 1 7.31 0.53
9 1 1 11.7 0.74
9 2 1 26.08 0.97
9 3 1 12.78 0.78
9 4 1 5.77 0.51
9 5 1 6.86 0.6
9 6 1 19.33 0.9
9 7 1 38.74 1.22
9 8 1 14.07 0.82
9 9 1 38.19 1.19
9 10 1 4.25 0.47
9 11 1 34.07 1.2
9 12 1 3.22 0.45
9 13 1 58.7 1.56
9 14 1 13.42 0.92
9 15 1 4.14 0.49
9 16 1 10.09 0.83
9 17 1 21.57 1.06
9 18 1 1.37 0.41
9 0 2 110.44 1.96
9 1 2 1.79 0.36
9 2 2 4.5 0.43
9 3 2 2.76 0.4
9 4 2 90.82 1.78
9 5 2 32.14 1.08
9 6 2 9.86 0.77
9 7 2 11.01 0.81
9 8 2 6.2 0.5
9 9 2 62.91 1.54
9 10 2 9.91 0.76
9 11 2 15.64 0.91
9 12 2 19.13 1
9 13 2 34.83 1.26
9 14 2 10.45 0.78
9 15 2 10.73 0.83
9 16 2 18.06 1.01
9 17 2 3.62 0.47
9 18 2 12.87 0.88
9 0 3 19.85 0.89
9 1 3 20.28 0.92
9 2 3 72.52 1.58
9 4 3 7.66 0.57
9 5 3 21.31 0.97
9 6 3 27.44 1.07
9 7 3 16.26 0.9
9 8 3 84.87 1.81
9 9 3 9.84 0.81
9 10 3 49 1.41
9 11 3 15.44 0.93
9 12 3 43.79 1.36
9 13 3 3.88 0.48
9 14 3 30.18 1.22
9 15 3 3.53 0.47
9 16 3 2.12 0.43
9 17 3 4.82 0.5
9 0 4 65.62 1.56
9 1 4 1.56 0.39
9 2 4 3.4 0.43
9 3 4 15.06 0.85
9 4 4 41.85 1.26
9 5 4 18.96 0.94
9 6 4 28.73 1.08
9 7 4 13.04 0.87
9 8 4 34.57 1.21
9 9 4 20.24 0.98
9 10 4 48.36 1.44
9 12 4 35.21 1.25
9 13 4 1.29 0.42
9 14 4 4.41 0.5
9 15 4 5.25 0.52
9 16 4 4.67 0.5
9 0 5 68.28 1.65
9 1 5 12.06 0.84
9 2 5 43.02 1.31
9 3 5 39.66 1.27
9 4 5 13.06 0.87
9 5 5 1.13 0.39
9 6 5 17.58 0.97
9 7 5 36.17 1.24
9 8 5 20.34 1
9 9 5 1.59 0.42
9 10 5 2.87 0.46
9 11 5 20.48 1.04
9 12 5 11.51 0.86
9 13 5 7.68 0.64
9 14 5 2.76 0.46
9 15 5 9.32 0.75
9 0 6 0.87 0.39
9 1 6 2.82 0.45
9 2 6 15.81 0.94
9 3 6 29.88 1.16
9 4 6 9.05 0.73
9 5 6 10.68 0.84
9 6 6 9.96 0.81
9 7 6 15.78 0.96
9 8 6 3.15 0.47
9 9 6 23.45 1.09
9 10 6 5.15 0.57
9 11 6 20.81 1.05
9 12 6 9.07 0.73
9 13 6 7.73 0.56
9 0 7 18.07 1.01
9 1 7 5.97 0.59
9 2 7 20.42 1.06
9 3 7 5.43 0.52
9 4 7 19.36 1.05
9 5 7 19.83 1.05
9 6 7 62.33 1.63
9 7 7 1.33 0.41
9 8 7 20.81 1.02
9 9 7 11.35 0.91
9 10 7 13.23 0.91
9 11 7 1.39 0.42
9 0 8 4.33 0.49
9 1 8 2.31 0.44
9 2 8 2.91 0.46
9 3 8 13.45 0.93
9 4 8 23.27 1.12
9 5 8 6.86 0.61
9 6 8 18.66 0.99
9 7 8 28.95 1.19
9 8 8 5 0.5
10 0 0 269.5 3.53
10 2 0 10.15 0.78
10 3 0 1.72 0.4
10 4 0 117.77 2.13
10 5 0 10.37 0.8
10 6 0 24.21 1.04
10 7 0 1.31 0.4
10 8 0 3.04 0.45
10 9 0 18.3 0.98
10 10 0 3.66 0.47
10 11 0 2.42 0.44
10 12 0 1.9 0.43
10 14 0 7.37 0.7
10 15 0 1.58 0.42
10 1 1 40.47 1.25
10 2 1 13.06 0.79
10 3 1 18.89 0.93
10 4 1 12.95 0.87
10 5 1 5.74 0.55
10 6 1 40.98 1.28
10 7 1 11.7 0.77
10 8 1 2.15 0.43
10 9 1 9.95 0.83
10 10 1 10.92 0.84
10 11 1 48.05 1.44
10 12 1 8.85 0.76
10 13 1 9.22 0.67
10 14 1 8.75 0.75
10 15 1 16.77 0.98
10 16 1 2.33 0.44
10 0 2 51.15 1.41
10 1 2 3.63 0.45
10 2 2 50.12 1.42
10 3 2 14.25 0.86
10 4 2 18.61 0.93
10 5 2 5.29 0.5
10 6 2 2.67 0.44
10 7 2 36.59 1.23
10 8 2 7.32 0.69
10 9 2 2.67 0.45
10 10 2 32.29 1.24
10 11 2 44.11 1.41
10 12 2 2.31 0.45
10 13 2 0.95 0.4
10 14 2 34.4 1.26
10 15 2 33.04 1.24
10 0 3 7.5 0.69
10 2 3 14.98 0.88
10 3 3 5.05 0.49
10 4 3 15.45 0.9
10 5 3 8.17 0.62
10 6 3 57.14 1.51
10 7 3 2.4 0.43
10 9 3 10.73 0.85
10 10 3 22.82 1.11
10 11 3 1.8 0.43
10 12 3 21.75 1.05
10 13 3 27.16 1.17
10 14 3 2.5 0.45
10 15 3 2.46 0.44
10 0 4 3.17 0.45
10 1 4 8.7 0.71
10 2 4 14.64 0.88
10 3 4 17.77 0.99
10 4 4 15.45 0.92
10 5 4 32.39 1.22
10 6 4 3.88 0.47
10 7 4 38.8 1.34
10 8 4 21.95 1.07
10 9 4 15.55 0.95
10 10 4 22.71 1.1
10 11 4 20.98 1.06
10 12 4 1.53 0.42
10 13 4 0.94 0.4
10 14 4 19.66 1.02
10 0 5 17.87 0.98
10 1 5 32.36 1.21
10 2 5 30.1 1.22
10 3 5 1.27 0.41
10 4 5 23.02 1.07
10 5 5 56.77 1.58
10 6 5 19.71 1.04
10 7 5 2.18 0.45
10 8 5 12.48 0.89
10 9 5 41.25 1.38
10 10 5 13.05 0.93
10 11 5 2.15 0.44
10 12 5 9.28 0.76
10 1 6 9.25 0.63
10 2 6 11.63 0.91
10 4 6 1.97 0.43
10 5 6 3.93 0.49
10 6 6 3.15 0.46
10 7 6 13.01 0.83
10 8 6 6.24 0.53
10 9 6 6.63 0.6
10 10 6 15.54 0.94
10 0 7 3.38 0.47
10 1 7 5.78 0.52
10 2 7 85.05 1.91
10 3 7 3.66 0.47
10 4 7 9.21 0.76
10 5 7 4.61 0.49
10 6 7 36.84 1.28
10 7 7 11.67 0.9
11 2 0 183.71 2.87
11 3 0 10.41 0.77
11 6 0 19.74 1.02
11 7 0 58.62 1.57
11 8 0 0.89 0.41
11 9 0 1.71 0.42
11 10 0 10.4 0.79
11 11 0 55.67 1.53
11 12 0 4.47 0.49
11 13 0 9.71 0.78
11 1 1 30.5 1.19
11 2 1 1.58 0.42
11 3 1 8.61 0.73
11 4 1 8.09 0.63
11 5 1 26.23 1.13
11 6 1 1.64 0.43
11 7 1 28.55 1.15
11 8 1 15.11 0.95
11 9 1 2.11 0.44
11 10 1 7.99 0.64
11 11 1 5.22 0.51
11 12 1 0.86 0.4
11 13 1 13.51 0.8
11 0 2 7.55 0.69
11 1 2 10.13 0.83
11 2 2 14.58 0.96
11 3 2 20.98 1.07
11 4 2 12.96 0.88
11 5 2 1.49 0.42
11 6 2 1.94 0.43
11 7 2 19.92 1.04
11 8 2 9.43 0.75
11 9 2 2.28 0.45
11 10 2 3.21 0.47
11 11 2 21.76 1.06
11 12 2 6 0.58
11 0 3 15.98 0.96
11 1 3 19.5 1
11 2 3 8.74 0.73
11 4 3 27.78 1.17
11 5 3 19.28 1
11 6 3 18.3 1.01
11 7 3 12.63 0.91
11 8 3 15.42 0.99
11 9 3 3.15 0.46
11 10 3 3.72 0.47
11 11 3 16.36 1
11 0 4 7.02 0.61
11 1 4 14.6 0.94
11 2 4 27.82 1.16
11 3 4 35.56 1.28
11 4 4 7.47 0.57
11 5 4 3.27 0.46
11 6 4 16.55 0.94
11 7 4 5.1 0.52
11 8 4 1.42 0.41
11 9 4 10.96 0.79
11 10 4 3.39 0.46
11 0 5 9.02 0.66
11 1 5 14.56 0.97
11 2 5 35.17 1.28
11 3 5 22.77 1.05
11 4 5 2.43 0.44
11 5 5 3.09 0.46
11 6 5 48.35 1.48
11 7 5 12.23 0.87
11 0 6 18.27 1.03
11 1 6 4.8 0.5
11 2 6 0.92 0.43
11 3 6 27.9 1.15
11 4 6 7 0.6
12 0 0 8.97 0.67
12 1 0 13.9 0.94
12 2 0 5.37 0.57
12 3 0 24.79 1.12
12 4 0 2.33 0.44
12 5 0 17.59 0.98
12 6 0 20.44 1.03
12 7 0 8.05 0.57
12 9 0 35.87 1.28
12 0 1 12.35 0.88
12 1 1 5.12 0.51
12 2 1 3.81 0.48
12 3 1 22.42 1.1
12 4 1 8.85 0.69
12 5 1 34.48 1.28
12 7 1 22.75 1.1
12 8 1 10.07 0.85
12 0 2 0.99 0.4
12 1 2 5.13 0.51
12 2 2 47.45 1.48
12 3 2 1.52 0.42
12 4 2 8.65 0.75
12 5 2 7.74 0.62
12 6 2 15.1 0.97
12 7 2 4.89 0.5
12 8 2 5.31 0.57
12 1 3 18.01 0.97
12 3 3 20.75 1.05
12 4 3 1.85 0.42
12 5 3 7.03 0.69
12 6 3 0.89 0.4
12 0 4 14.18 0.92
12 1 4 44.01 1.39
12 2 4 9.06 0.83
12 3 4 17.12 0.99
_iucr_refine_fcf_details
;
data_L-Ala_23K_NoSpherA2_ORCA_NoSpherA2_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x+1/2,-y+1/2,-z
3 -x,y+1/2,-z+1/2
4 -x+1/2,-y,z+1/2
_space_group_crystal_system orthorhombic
_space_group_IT_number 19
_space_group_name_H-M_alt 'P 21 21 21'
_space_group_name_Hall ' P 2ac 2ab'
_symmetry_space_group_name_H-M 'P 21 21 21'
_symmetry_space_group_name_Hall ' P 2ac 2ab'
_symmetry_Int_Tables_number 19
_cell_length_a 5.9279(10)
_cell_length_b 12.2597(17)
_cell_length_c 5.7939(9)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 421.07(11)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
0 0 2 2912.100 2782.450 32.606 0.049 o
0 0 4 202.286 205.249 3.822 3.564 o
0 0 8 23.987 23.962 1.481 23.744 o
0 0 10 4.683 4.712 1.201 36.118 o
0 1 1 723.722 709.131 7.173 1.012 o
0 1 2 519.155 521.921 6.413 1.266 o
0 1 3 82.973 82.220 1.711 17.787 o
0 1 4 35.857 38.979 1.181 37.353 o
0 1 5 237.095 231.121 4.422 2.662 o
0 1 6 91.637 91.764 2.401 9.030 o
0 1 7 61.522 57.538 2.011 12.873 o
0 1 8 3.060 3.512 0.930 60.134 o
0 1 9 6.404 8.344 1.141 40.020 o
0 1 12 26.587 26.443 2.201 10.746 o
0 2 0 180.003 179.907 1.721 17.580 o
0 2 1 112.387 117.016 1.191 36.728 o
0 2 2 178.180 177.736 2.031 12.621 o
0 2 3 148.803 154.434 2.861 6.358 o
0 2 4 88.329 91.094 2.011 12.873 o
0 2 5 128.880 134.375 2.891 6.227 o
0 2 6 15.324 15.858 1.000 52.010 o
0 2 7 531.915 529.775 9.525 0.574 o
0 2 8 9.427 8.524 1.121 41.462 o
0 2 9 47.745 45.402 2.151 11.252 o
0 2 10 21.047 20.270 1.701 17.997 o
0 2 11 2.180 2.641 1.211 35.523 o
0 2 12 18.500 19.779 1.921 14.109 o
0 3 1 696.156 693.624 6.263 1.327 o
0 3 2 56.002 55.007 0.780 85.486 o
0 3 3 198.781 201.097 2.401 9.030 o
0 3 4 6.487 7.834 0.440 268.646 o
0 3 5 47.839 48.173 1.501 23.116 o
0 3 6 0.742 1.461 0.630 131.040 o
0 3 8 17.015 15.387 1.321 29.850 o
0 3 9 61.383 62.010 2.481 8.456 o
0 3 10 48.851 47.933 2.361 9.338 o
0 3 11 7.678 6.653 1.451 24.737 o
0 3 12 115.661 113.775 3.872 3.473 o
0 4 0 5310.530 5076.150 43.511 0.027 o
0 4 1 94.920 96.196 1.040 48.086 o
0 4 2 169.304 167.601 1.751 16.983 o
0 4 3 709.083 723.418 7.614 0.898 o
0 4 4 218.470 224.618 2.781 6.730 o
0 4 5 368.743 380.863 4.492 2.580 o
0 4 6 15.695 15.648 1.061 46.289 o
0 4 7 11.371 11.536 1.081 44.590 o
0 4 9 20.829 21.750 1.591 20.573 o
0 4 10 26.795 27.743 1.901 14.407 o
0 5 2 544.395 554.867 5.213 1.916 o
0 5 3 78.601 79.598 1.171 37.994 o
0 5 5 177.494 173.974 2.381 9.182 o
0 5 6 81.638 84.431 1.541 21.930 o
0 5 7 24.916 23.571 1.401 26.536 o
0 5 10 31.898 32.015 2.011 12.873 o
0 5 12 8.929 9.575 1.681 18.428 o
0 6 0 87.134 87.802 1.020 49.990 o
0 6 1 469.864 464.954 4.482 2.591 o
0 6 2 92.452 94.676 1.141 40.020 o
0 6 3 259.368 266.598 2.781 6.730 o
0 6 4 68.831 69.433 1.201 36.118 o
0 6 6 12.280 10.945 0.640 126.977 o
0 6 7 42.268 42.260 1.191 36.728 o
0 6 8 9.759 10.055 0.800 81.266 o
0 6 10 40.699 40.740 2.281 10.005 o
0 6 11 8.455 7.554 1.501 23.116 o
0 6 12 54.876 54.606 2.701 7.134 o
0 7 1 36.209 36.147 0.600 144.472 o
0 7 2 4.606 5.303 0.330 477.593 o
0 7 3 21.853 21.931 0.560 165.848 o
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0 18 7 1.532 2.261 0.430 281.287 o
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0 19 1 15.180 15.818 0.870 68.714 o
0 19 2 114.627 117.347 2.051 12.376 o
0 19 3 2.849 2.451 0.400 325.062 o
0 19 4 3.751 3.292 0.430 281.287 o
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0 19 7 5.042 6.713 0.540 178.361 o
0 19 8 10.156 9.034 0.750 92.462 o
0 20 1 26.740 26.863 1.020 49.990 o
0 20 2 0.905 0.960 0.400 325.062 o
0 20 3 41.770 43.501 1.311 30.307 o
0 20 4 1.506 1.791 0.400 325.062 o
0 20 6 1.370 1.801 0.420 294.841 o
0 20 7 128.774 132.374 2.401 9.030 o
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0 21 1 2.152 2.631 0.410 309.399 o
0 21 2 44.791 44.972 1.331 29.402 o
0 21 3 0.737 0.850 0.380 360.180 o
0 21 5 21.403 19.219 1.020 49.990 o
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0 22 0 129.088 132.684 2.311 9.747 o
0 22 2 36.765 36.037 1.261 32.760 o
0 22 3 0.616 1.131 0.400 325.062 o
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0 23 1 1.837 1.691 0.410 309.399 o
0 23 2 16.326 17.639 1.010 50.985 o
0 23 3 26.239 27.563 1.141 40.020 o
0 23 5 13.589 12.256 0.940 58.861 o
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0 24 2 1.716 2.441 0.450 256.839 o
0 24 3 10.831 12.446 0.890 65.661 o
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0 25 1 2.209 2.921 0.550 171.934 o
0 25 2 19.976 21.991 1.231 34.378 o
0 25 3 5.789 4.872 0.560 165.848 o
0 25 4 2.338 2.841 0.500 208.040 o
0 26 0 5.145 6.313 0.600 144.472 o
0 26 1 18.227 19.369 1.211 35.523 o
0 26 2 1.722 2.501 0.490 216.618 o
1 0 1 74.016 75.186 0.810 79.271 o
1 0 2 3237.870 3040.780 35.387 0.042 o
1 0 3 31.168 31.375 0.900 64.210 o
1 0 4 321.545 321.605 5.713 1.595 o
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1 0 7 240.274 242.857 5.042 2.048 o
1 0 8 10.051 10.235 1.181 37.353 o
1 0 10 2.666 3.412 1.151 39.327 o
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1 1 0 254.044 246.239 2.311 9.747 o
1 1 1 125.651 130.783 1.331 29.402 o
1 1 2 71.522 70.174 0.920 61.448 o
1 1 3 292.199 296.283 5.122 1.984 o
1 1 4 238.553 254.673 4.632 2.426 o
1 1 5 119.394 119.898 2.651 7.406 o
1 1 7 25.529 26.303 1.421 25.794 o
1 1 8 34.030 34.627 1.751 16.983 o
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1 1 10 23.622 25.222 1.841 15.362 o
1 1 11 13.374 11.766 1.581 20.834 o
1 1 12 72.064 74.496 3.122 5.343 o
1 2 0 5343.160 5372.220 56.887 0.016 o
1 2 1 104.573 101.949 1.081 44.590 o
1 2 2 572.647 560.540 5.993 1.450 o
1 2 3 220.340 220.106 2.581 7.814 o
1 2 4 26.501 28.154 1.020 49.990 o
1 2 5 455.242 454.179 7.954 0.823 o
1 2 6 7.550 7.394 0.810 79.271 o
1 2 7 58.020 60.109 2.071 12.138 o
1 2 8 18.418 19.459 1.411 26.161 o
1 2 9 49.509 50.514 2.221 10.553 o
1 2 11 33.478 33.156 2.211 10.649 o
1 2 12 9.421 8.134 1.701 17.997 o
1 3 0 56.439 57.868 0.670 115.861 o
1 3 1 1084.120 1064.920 9.475 0.580 o
1 3 2 188.273 190.062 1.981 13.267 o
1 3 3 88.595 89.833 1.251 33.286 o
1 3 4 22.101 22.931 0.630 131.040 o
1 3 5 177.477 172.673 3.562 4.104 o
1 3 6 11.724 12.166 0.970 55.277 o
1 3 7 77.860 79.788 2.441 8.736 o
1 3 8 30.655 31.475 1.671 18.649 o
1 3 10 17.610 19.759 1.681 18.428 o
1 3 11 24.219 22.941 1.911 14.257 o
1 4 0 1711.740 1643.450 14.457 0.249 o
1 4 1 159.434 153.764 1.601 20.316 o
1 4 2 1050.060 1042.130 9.435 0.585 o
1 4 3 89.333 93.685 1.311 30.307 o
1 4 4 107.361 107.412 1.531 22.218 o
1 4 5 105.988 105.891 1.651 19.104 o
1 4 6 16.172 15.668 1.061 46.289 o
1 4 7 141.011 138.427 3.442 4.395 o
1 4 8 32.156 32.126 1.721 17.580 o
1 4 9 3.735 3.192 1.111 42.212 o
1 4 10 21.690 21.280 1.781 16.415 o
1 4 11 12.262 11.666 1.591 20.573 o
1 4 12 28.833 28.474 2.171 11.045 o
1 5 0 334.341 331.320 3.222 5.016 o
1 5 1 437.185 428.756 4.142 3.034 o
1 5 2 17.302 18.219 0.400 325.062 o
1 5 3 21.867 22.561 0.510 199.961 o
1 5 4 78.552 81.960 1.311 30.307 o
1 5 5 8.174 8.384 0.520 192.344 o
1 5 6 11.948 13.016 0.650 123.100 o
1 5 7 28.846 29.954 1.020 49.990 o
1 5 8 103.038 100.208 3.051 5.591 o
1 5 9 27.528 28.023 1.801 16.052 o
1 5 10 32.617 32.045 2.051 12.376 o
1 5 11 5.268 6.023 1.421 25.794 o
1 5 12 70.787 67.262 3.051 5.591 o
1 6 0 61.257 60.579 0.780 85.486 o
1 6 1 20.595 21.430 0.430 281.287 o
1 6 2 214.184 214.934 2.261 10.183 o
1 6 3 133.028 135.255 1.601 20.316 o
1 6 4 126.607 127.671 1.831 15.530 o
1 6 5 218.603 225.018 2.951 5.976 o
1 6 6 20.438 21.440 0.800 81.266 o
1 6 7 61.282 60.469 1.441 25.082 o
1 6 8 15.766 14.747 0.900 64.210 o
1 6 9 8.824 9.855 1.271 32.246 o
1 6 10 38.887 40.780 2.261 10.183 o
1 6 11 2.768 3.872 1.321 29.850 o
1 7 0 18.045 18.849 0.430 281.287 o
1 7 1 332.352 332.280 3.342 4.662 o
1 7 2 156.980 158.676 1.781 16.415 o
1 7 3 4.586 5.072 0.370 379.912 o
1 7 4 81.475 81.990 1.201 36.118 o
1 7 5 73.519 71.454 1.361 28.120 o
1 7 6 6.952 7.624 0.610 139.774 o
1 7 7 10.200 9.314 0.750 92.462 o
1 7 8 93.290 89.533 1.921 14.109 o
1 7 9 13.994 15.557 0.990 53.066 o
1 7 10 32.076 31.075 2.061 12.256 o
1 7 11 7.951 8.444 1.551 21.648 o
1 7 12 23.571 22.411 2.041 12.498 o
1 8 0 390.155 393.750 3.922 3.385 o
1 8 1 230.495 229.701 2.431 8.808 o
1 8 2 10.139 10.035 0.420 294.841 o
1 8 3 249.037 252.311 2.751 6.877 o
1 8 4 44.548 44.241 0.870 68.714 o
1 8 5 68.447 67.903 1.351 28.538 o
1 8 6 9.430 8.904 0.670 115.861 o
1 8 7 56.124 55.197 1.421 25.794 o
1 8 8 3.428 3.182 0.480 225.738 o
1 8 9 7.674 8.184 0.730 97.598 o
1 8 10 24.354 24.042 1.231 34.378 o
1 8 11 15.819 15.317 1.161 38.652 o
1 9 0 2.499 3.192 0.340 449.913 o
1 9 1 224.031 227.450 2.481 8.456 o
1 9 2 56.555 60.519 0.960 56.434 o
1 9 3 27.722 28.414 0.690 109.242 o
1 9 4 2.279 2.131 0.380 360.180 o
1 9 5 90.266 88.192 1.431 25.434 o
1 9 6 11.151 10.845 0.750 92.462 o
1 9 7 68.120 66.002 1.581 20.834 o
1 9 8 50.217 50.214 1.491 23.427 o
1 9 9 19.736 19.439 1.091 43.776 o
1 9 10 7.214 7.233 0.790 83.336 o
1 9 11 24.620 23.061 1.281 31.744 o
1 10 0 39.444 42.160 0.790 83.336 o
1 10 1 132.035 128.482 1.641 19.337 o
1 10 2 57.944 58.238 0.980 54.154 o
1 10 3 77.203 78.038 1.211 35.523 o
1 10 4 21.199 22.241 0.690 109.242 o
1 10 5 9.469 9.324 0.570 160.080 o
1 10 6 2.442 2.381 0.430 281.287 o
1 10 7 17.895 18.379 0.940 58.861 o
1 10 8 40.831 38.939 1.351 28.538 o
1 10 9 30.812 28.994 1.291 31.254 o
1 10 10 62.353 54.866 1.761 16.790 o
1 10 11 19.297 18.359 1.201 36.118 o
1 11 0 91.429 94.866 1.331 29.402 o
1 11 1 17.033 16.788 0.550 171.934 o
1 11 2 113.303 115.506 1.561 21.372 o
1 11 3 14.901 16.318 0.580 154.607 o
1 11 4 61.790 61.059 1.151 39.327 o
1 11 5 34.315 35.117 0.930 60.134 o
1 11 6 10.472 9.635 0.660 119.398 o
1 11 7 21.226 21.400 0.890 65.661 o
1 11 8 93.001 93.635 2.081 12.021 o
1 11 9 44.742 45.192 1.541 21.930 o
1 11 10 14.986 15.978 1.121 41.462 o
1 11 11 2.751 3.532 0.580 154.607 o
1 12 0 26.824 26.353 0.690 109.242 o
1 12 2 113.327 113.014 1.591 20.573 o
1 12 3 31.588 31.625 0.820 77.350 o
1 12 4 142.036 137.966 1.951 13.678 o
1 12 5 24.436 24.562 0.840 73.710 o
1 12 6 28.481 28.404 0.940 58.861 o
1 12 7 2.397 1.871 0.450 256.839 o
1 12 8 12.668 11.536 0.950 57.629 o
1 12 9 7.942 8.764 0.810 79.271 o
1 12 10 48.865 44.672 1.611 20.065 o
1 12 11 0.864 1.581 0.520 192.344 o
1 13 0 57.206 56.127 1.061 46.289 o
1 13 1 123.953 124.980 1.731 17.378 o
1 13 2 110.560 107.932 1.601 20.316 o
1 13 3 34.239 33.106 0.890 65.661 o
1 13 4 25.113 26.573 0.840 73.710 o
1 13 5 43.737 43.811 1.131 40.731 o
1 13 6 7.546 7.384 0.590 149.411 o
1 13 7 40.535 41.490 1.221 34.944 o
1 13 8 27.078 27.753 1.241 33.825 o
1 13 9 16.548 15.778 1.111 42.212 o
1 14 1 28.624 28.964 0.810 79.271 o
1 14 2 53.205 53.576 1.111 42.212 o
1 14 3 112.417 112.474 1.741 17.179 o
1 14 4 41.080 38.599 1.040 48.086 o
1 14 5 38.769 39.379 1.101 42.983 o
1 14 6 27.461 27.443 0.980 54.154 o
1 14 7 25.691 24.122 1.030 49.024 o
1 14 8 1.895 1.181 0.500 208.040 o
1 14 9 7.144 7.764 0.810 79.271 o
1 14 10 7.314 6.443 0.650 123.100 o
1 15 0 83.335 84.511 1.451 24.737 o
1 15 1 85.709 85.801 1.481 23.744 o
1 15 2 30.237 30.985 0.900 64.210 o
1 15 3 33.469 32.796 0.960 56.434 o
1 15 4 2.170 2.921 0.390 341.946 o
1 15 5 29.192 29.234 1.000 52.010 o
1 15 6 11.619 10.785 0.800 81.266 o
1 15 7 34.485 31.665 1.151 39.327 o
1 15 8 43.476 45.362 1.351 28.538 o
1 15 9 20.538 21.800 1.211 35.523 o
1 15 10 10.197 10.325 0.860 70.322 o
1 16 0 24.054 23.951 0.830 75.497 o
1 16 1 60.950 60.499 1.261 32.760 o
1 16 2 28.709 27.053 0.920 61.448 o
1 16 3 9.775 9.104 0.600 144.472 o
1 16 4 22.082 23.091 0.890 65.661 o
1 16 5 72.645 76.997 1.601 20.316 o
1 16 6 2.879 2.921 0.420 294.841 o
1 16 7 23.605 25.332 1.051 47.175 o
1 16 8 5.575 5.473 0.510 199.961 o
1 16 9 41.751 42.090 1.551 21.648 o
1 17 0 29.298 28.924 0.940 58.861 o
1 17 1 24.578 24.902 0.880 67.162 o
1 17 2 76.379 74.156 1.491 23.427 o
1 17 3 25.478 24.512 0.920 61.448 o
1 17 4 26.534 27.513 1.000 52.010 o
1 17 5 10.833 11.225 0.780 85.486 o
1 17 6 20.419 21.080 0.980 54.154 o
1 17 7 18.970 20.090 0.990 53.066 o
1 17 8 30.281 26.293 1.161 38.652 o
1 17 9 17.829 17.939 1.030 49.024 o
1 18 0 0.780 0.910 0.370 379.912 o
1 18 1 22.950 23.291 0.910 62.806 o
1 18 2 107.326 107.812 1.891 14.560 o
1 18 3 27.235 25.973 0.980 54.154 o
1 18 4 55.707 57.378 1.431 25.434 o
1 18 5 7.531 6.813 0.630 131.040 o
1 18 6 13.483 13.576 0.880 67.162 o
1 18 7 43.830 42.180 1.361 28.120 o
1 18 8 4.840 5.353 0.510 199.961 o
1 18 9 11.780 11.345 0.880 67.162 o
1 19 0 32.820 33.026 1.081 44.590 o
1 19 1 14.378 14.987 0.810 79.271 o
1 19 2 39.715 40.359 1.181 37.353 o
1 19 3 27.047 26.653 1.030 49.024 o
1 19 4 40.013 39.969 1.221 34.944 o
1 19 5 17.719 18.299 0.950 57.629 o
1 19 6 10.825 11.566 0.840 73.710 o
1 19 7 6.507 6.613 0.600 144.472 o
1 19 8 1.760 2.221 0.430 281.287 o
1 20 0 41.615 39.429 1.221 34.944 o
1 20 1 6.370 5.703 0.470 235.446 o
1 20 2 10.211 9.505 0.690 109.242 o
1 20 3 7.832 7.604 0.650 123.100 o
1 20 4 8.978 9.054 0.780 85.486 o
1 20 5 65.618 63.340 1.611 20.065 o
1 20 6 32.475 30.955 1.221 34.944 o
1 20 7 13.576 15.137 0.970 55.277 o
1 21 0 1.243 1.401 0.420 294.841 o
1 21 1 1.448 2.021 0.400 325.062 o
1 21 2 21.637 22.401 1.000 52.010 o
1 21 3 23.876 23.101 1.030 49.024 o
1 21 4 11.095 10.575 0.770 87.721 o
1 21 5 24.785 24.592 1.091 43.776 o
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1 22 0 3.383 3.912 0.460 245.794 o
1 22 1 32.832 34.046 1.181 37.353 o
1 22 2 38.272 35.827 1.251 33.286 o
1 22 3 6.190 7.043 0.600 144.472 o
1 22 4 20.558 21.320 1.020 49.990 o
1 22 5 1.672 1.691 0.420 294.841 o
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1 23 0 5.650 6.863 0.590 149.411 o
1 23 1 9.222 10.435 0.870 68.714 o
1 23 2 42.546 42.511 1.391 26.919 o
1 23 3 2.727 2.691 0.450 256.839 o
1 23 4 14.200 14.767 0.940 58.861 o
1 23 5 3.568 4.482 0.490 216.618 o
1 23 6 11.946 11.786 0.870 68.714 o
1 24 0 9.793 9.585 0.770 87.721 o
1 24 1 21.291 20.500 1.051 47.175 o
1 24 2 9.876 10.435 0.780 85.486 o
1 24 3 7.689 7.964 0.630 131.040 o
1 24 4 2.081 2.091 0.420 294.841 o
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1 26 1 0.859 1.961 0.470 235.446 o
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2 0 4 51.396 55.607 1.501 23.116 o
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3 17 3 8.574 8.004 0.620 135.302 o
3 17 4 31.463 31.495 1.091 43.776 o
3 17 5 2.807 3.071 0.430 281.287 o
3 17 6 23.561 23.461 1.040 48.086 o
3 17 7 3.106 2.771 0.440 268.646 o
3 17 8 10.322 10.975 0.880 67.162 o
3 17 9 21.579 21.330 1.061 46.289 o
3 18 0 1.506 2.091 0.370 379.912 o
3 18 1 52.087 49.994 1.301 30.775 o
3 18 2 8.784 8.854 0.700 106.143 o
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3 18 5 5.443 6.263 0.520 192.344 o
3 18 6 10.547 9.965 0.750 92.462 o
3 18 7 7.674 7.664 0.620 135.302 o
3 18 8 8.691 8.144 0.630 131.040 o
3 19 0 2.516 2.881 0.410 309.399 o
3 19 1 18.691 19.309 0.900 64.210 o
3 19 2 6.129 5.413 0.530 185.155 o
3 19 3 9.427 10.065 0.800 81.266 o
3 19 4 17.048 16.508 0.920 61.448 o
3 19 5 12.353 10.375 0.760 90.045 o
3 19 6 21.197 21.350 1.061 46.289 o
3 19 7 20.971 20.400 1.061 46.289 o
3 19 8 22.059 22.601 1.091 43.776 o
3 20 0 25.910 27.333 1.051 47.175 o
3 20 1 3.809 3.622 0.440 268.646 o
3 20 2 11.489 11.315 0.820 77.350 o
3 20 3 6.873 5.983 0.510 199.961 o
3 20 4 20.550 20.400 0.990 53.066 o
3 20 5 2.054 2.771 0.450 256.839 o
3 20 6 60.551 62.100 1.621 19.818 o
3 20 7 10.250 8.974 0.730 97.598 o
3 21 0 29.033 29.734 1.121 41.462 o
3 21 1 62.319 66.242 1.601 20.316 o
3 21 3 1.898 1.581 0.410 309.399 o
3 21 4 23.471 25.192 1.091 43.776 o
3 21 5 3.066 3.502 0.470 235.446 o
3 21 6 4.937 5.653 0.520 192.344 o
3 21 7 5.207 5.092 0.500 208.040 o
3 22 0 3.526 3.992 0.470 235.446 o
3 22 1 63.023 60.669 1.601 20.316 o
3 22 2 2.831 2.751 0.440 268.646 o
3 22 3 6.511 6.253 0.530 185.155 o
3 22 4 6.544 6.823 0.610 139.774 o
3 22 5 15.230 14.807 0.970 55.277 o
3 22 6 5.785 5.042 0.500 208.040 o
3 23 1 14.901 15.137 0.930 60.134 o
3 23 2 9.509 9.605 0.850 71.986 o
3 23 3 39.303 38.959 1.351 28.538 o
3 23 4 9.791 9.835 0.840 73.710 o
3 23 5 2.907 3.692 0.470 235.446 o
3 24 0 8.731 7.884 0.640 126.977 o
3 24 1 26.502 29.194 1.181 37.353 o
3 24 2 26.218 26.983 1.151 39.327 o
3 24 3 6.726 8.324 0.710 103.174 o
3 24 4 0.955 1.071 0.400 325.062 o
3 25 0 26.336 28.944 1.401 26.536 o
3 25 1 6.127 7.634 0.750 92.462 o
3 25 2 4.534 4.442 0.550 171.934 o
4 0 0 384.919 384.345 3.812 3.583 o
4 0 1 1.112 1.431 0.290 618.430 o
4 0 2 9.915 10.515 0.430 281.287 o
4 0 3 4.469 4.582 0.380 360.180 o
4 0 4 73.617 75.707 1.171 37.994 o
4 0 5 27.345 27.353 0.760 90.045 o
4 0 7 138.343 135.535 2.061 12.256 o
4 0 8 40.540 43.441 2.051 12.376 o
4 0 9 18.623 18.879 1.621 19.818 o
4 0 11 27.665 27.353 2.091 11.907 o
4 1 0 376.289 378.602 3.802 3.602 o
4 1 1 145.096 145.550 1.671 18.649 o
4 1 2 258.978 258.845 2.771 6.778 o
4 1 3 219.803 219.956 2.431 8.808 o
4 1 4 119.392 121.468 1.601 20.316 o
4 1 5 20.966 22.551 0.700 106.143 o
4 1 6 87.531 86.672 1.471 24.069 o
4 1 7 10.134 9.244 0.700 106.143 o
4 1 8 18.957 19.259 1.221 34.944 o
4 1 9 12.870 13.447 1.461 24.399 o
4 1 10 78.633 81.479 3.162 5.208 o
4 2 0 39.099 39.449 0.690 109.242 o
4 2 1 34.770 33.906 0.650 123.100 o
4 2 2 10.213 9.485 0.440 268.646 o
4 2 3 36.606 37.638 0.770 87.721 o
4 2 4 32.785 33.416 0.770 87.721 o
4 2 5 5.752 6.073 0.480 225.738 o
4 2 6 14.115 15.007 0.670 115.861 o
4 2 7 13.230 12.586 0.820 77.350 o
4 2 8 13.614 13.466 0.890 65.661 o
4 2 9 12.330 13.056 1.431 25.434 o
4 2 10 13.489 13.937 1.611 20.065 o
4 2 11 2.894 3.111 1.321 29.850 o
4 3 0 1.963 1.721 0.300 577.888 o
4 3 1 146.911 147.571 1.711 17.787 o
4 3 2 74.625 73.595 1.061 46.289 o
4 3 3 449.319 454.309 4.592 2.469 o
4 3 4 93.797 94.746 1.371 27.710 o
4 3 5 161.803 160.527 2.071 12.138 o
4 3 6 26.897 25.212 0.820 77.350 o
4 3 7 11.483 11.876 0.800 81.266 o
4 3 8 11.988 11.586 0.870 68.714 o
4 3 9 23.316 23.721 1.181 37.353 o
4 3 10 3.971 3.041 1.261 32.760 o
4 3 11 9.132 8.854 1.541 21.930 o
4 4 0 33.726 36.237 0.690 109.242 o
4 4 1 12.728 11.886 0.450 256.839 o
4 4 2 191.029 195.854 2.201 10.746 o
4 4 3 94.215 93.135 1.311 30.307 o
4 4 4 34.446 34.387 0.790 83.336 o
4 4 5 27.618 28.014 0.780 85.486 o
4 4 6 11.805 11.626 0.650 123.100 o
4 4 7 64.437 63.931 1.551 21.648 o
4 4 8 27.739 28.624 1.161 38.652 o
4 4 9 55.441 58.198 1.681 18.428 o
4 4 10 30.091 29.694 1.341 28.965 o
4 4 11 32.826 32.396 2.211 10.649 o
4 5 0 14.746 15.107 0.500 208.040 o
4 5 1 58.705 58.788 0.930 60.134 o
4 5 2 135.900 132.994 1.671 18.649 o
4 5 3 105.410 106.211 1.461 24.399 o
4 5 4 81.124 85.521 1.331 29.402 o
4 5 5 80.566 82.950 1.381 27.310 o
4 5 6 137.005 135.245 1.981 13.267 o
4 5 7 15.207 16.078 0.890 65.661 o
4 5 8 4.346 4.322 0.530 185.155 o
4 5 9 14.349 13.627 0.990 53.066 o
4 5 10 58.382 56.677 1.791 16.232 o
4 5 11 12.891 12.886 1.321 29.850 o
4 6 0 126.861 128.982 1.601 20.316 o
4 6 1 43.318 42.600 0.800 81.266 o
4 6 2 32.358 31.675 0.710 103.174 o
4 6 3 4.964 5.313 0.420 294.841 o
4 6 4 53.539 54.926 1.051 47.175 o
4 6 5 12.889 13.496 0.610 139.774 o
4 6 6 41.011 40.459 1.051 47.175 o
4 6 7 19.543 19.750 0.840 73.710 o
4 6 8 9.610 8.864 0.750 92.462 o
4 6 9 37.767 35.517 1.421 25.794 o
4 6 10 28.075 27.603 1.341 28.965 o
4 7 0 86.757 86.292 1.241 33.825 o
4 7 1 239.739 240.416 2.671 7.296 o
4 7 2 176.542 173.424 2.101 11.794 o
4 7 3 59.039 59.218 1.061 46.289 o
4 7 4 41.346 42.090 0.940 58.861 o
4 7 5 35.335 34.497 0.920 61.448 o
4 7 6 41.479 39.599 1.061 46.289 o
4 7 7 26.418 25.642 0.950 57.629 o
4 7 8 34.026 31.965 1.271 32.246 o
4 7 9 5.052 5.493 0.610 139.774 o
4 7 10 16.545 15.297 1.091 43.776 o
4 7 11 5.451 6.633 0.660 119.398 o
4 8 0 134.054 129.742 1.671 18.649 o
4 8 1 42.651 42.080 0.850 71.986 o
4 8 2 157.413 158.126 1.971 13.402 o
4 8 3 86.709 85.321 1.361 28.120 o
4 8 4 8.142 8.744 0.530 185.155 o
4 8 5 46.457 47.243 1.071 45.428 o
4 8 6 55.182 53.126 1.251 33.286 o
4 8 7 52.094 50.624 1.291 31.254 o
4 8 8 3.771 3.662 0.530 185.155 o
4 8 9 81.952 83.640 2.081 12.021 o
4 8 10 14.080 15.207 1.091 43.776 o
4 8 11 21.345 20.210 1.251 33.286 o
4 9 0 131.243 127.561 1.691 18.210 o
4 9 1 3.955 4.162 0.400 325.062 o
4 9 2 5.002 5.523 0.440 268.646 o
4 9 3 30.059 31.325 0.810 79.271 o
4 9 4 2.190 1.411 0.440 268.646 o
4 9 5 45.119 44.011 1.091 43.776 o
4 9 6 137.115 133.004 2.081 12.021 o
4 9 7 6.368 6.113 0.580 154.607 o
4 9 8 91.357 87.432 2.071 12.138 o
4 9 9 16.305 16.708 1.081 44.590 o
4 9 11 8.957 9.655 0.840 73.710 o
4 10 0 66.621 67.703 1.171 37.994 o
4 10 1 33.467 33.536 0.810 79.271 o
4 10 2 38.914 40.369 0.910 62.806 o
4 10 3 16.921 16.578 0.660 119.398 o
4 10 4 34.065 35.357 0.940 58.861 o
4 10 5 24.194 26.603 0.870 68.714 o
4 10 6 27.394 25.892 0.960 56.434 o
4 10 7 41.709 43.061 1.211 35.523 o
4 10 8 18.716 18.799 0.970 55.277 o
4 10 9 17.883 19.539 1.131 40.731 o
4 10 10 14.166 14.797 1.091 43.776 o
4 11 0 12.194 12.406 0.600 144.472 o
4 11 1 259.271 260.936 3.031 5.665 o
4 11 2 17.410 18.319 0.680 112.478 o
4 11 3 29.950 29.084 0.850 71.986 o
4 11 4 22.535 24.052 0.820 77.350 o
4 11 5 8.528 9.685 0.650 123.100 o
4 11 6 34.797 35.807 1.071 45.428 o
4 11 7 50.457 51.095 1.361 28.120 o
4 11 8 9.819 8.674 0.720 100.328 o
4 11 10 6.574 6.933 0.670 115.861 o
4 12 0 239.254 235.493 2.911 6.142 o
4 12 1 66.572 66.372 1.251 33.286 o
4 12 2 46.369 45.362 1.040 48.086 o
4 12 3 40.677 41.190 1.040 48.086 o
4 12 4 67.827 67.573 1.371 27.710 o
4 12 5 19.307 18.929 0.850 71.986 o
4 12 6 60.939 61.930 1.441 25.082 o
4 12 7 36.406 39.249 1.211 35.523 o
4 12 8 0.319 0.830 0.390 341.946 o
4 12 9 23.313 23.371 1.271 32.246 o
4 12 10 1.411 1.591 0.530 185.155 o
4 13 0 66.207 67.793 1.281 31.744 o
4 13 1 43.750 42.080 1.030 49.024 o
4 13 3 12.073 12.066 0.690 109.242 o
4 13 4 25.538 25.562 0.910 62.806 o
4 13 5 6.081 6.593 0.580 154.607 o
4 13 6 48.911 48.333 1.301 30.775 o
4 13 7 10.369 10.315 0.720 100.328 o
4 13 8 53.208 51.545 1.481 23.744 o
4 13 9 8.796 9.124 0.750 92.462 o
4 13 10 10.111 8.524 0.700 106.143 o
4 14 0 3.513 2.761 0.360 401.311 o
4 14 1 45.158 45.212 1.101 42.983 o
4 14 2 13.872 14.127 0.720 100.328 o
4 14 3 23.021 22.051 0.870 68.714 o
4 14 4 8.198 9.004 0.620 135.302 o
4 14 5 9.021 8.334 0.630 131.040 o
4 14 6 12.587 12.246 0.810 79.271 o
4 14 7 30.938 30.015 1.151 39.327 o
4 14 8 33.595 33.466 1.241 33.825 o
4 14 9 10.074 11.546 0.880 67.162 o
4 15 0 12.343 12.386 0.700 106.143 o
4 15 1 44.492 44.091 1.141 40.020 o
4 15 2 14.944 14.747 0.760 90.045 o
4 15 3 73.030 72.145 1.491 23.427 o
4 15 4 41.994 39.219 1.171 37.994 o
4 15 5 2.164 1.921 0.390 341.946 o
4 15 6 53.510 53.556 1.441 25.082 o
4 15 7 1.454 2.081 0.420 294.841 o
4 15 8 1.821 2.201 0.440 268.646 o
4 15 9 26.267 26.032 1.131 40.731 o
4 16 0 88.249 88.683 1.661 18.874 o
4 16 1 53.208 51.385 1.261 32.760 o
4 16 2 17.991 16.208 0.820 77.350 o
4 16 3 26.690 26.783 0.990 53.066 o
4 16 4 53.611 52.825 1.371 27.710 o
4 16 5 20.421 20.770 0.970 55.277 o
4 16 6 16.842 17.909 0.950 57.629 o
4 16 7 2.831 3.302 0.460 245.794 o
4 16 8 10.919 9.625 0.770 87.721 o
4 16 9 1.527 2.411 0.440 268.646 o
4 17 0 0.916 1.161 0.340 449.913 o
4 17 1 17.166 16.698 0.850 71.986 o
4 17 2 19.960 18.959 0.890 65.661 o
4 17 3 1.593 0.940 0.350 424.571 o
4 17 4 60.294 58.348 1.481 23.744 o
4 17 5 9.745 10.155 0.790 83.336 o
4 17 6 40.536 41.500 1.331 29.402 o
4 17 7 9.724 9.224 0.760 90.045 o
4 18 0 1.980 2.001 0.380 360.180 o
4 18 1 31.526 30.375 1.051 47.175 o
4 18 2 5.789 5.993 0.530 185.155 o
4 18 3 20.653 21.170 0.970 55.277 o
4 18 4 1.800 1.551 0.400 325.062 o
4 18 5 1.838 2.261 0.430 281.287 o
4 18 6 25.418 26.063 1.111 42.212 o
4 18 7 6.235 5.593 0.520 192.344 o
4 18 8 16.267 15.948 0.970 55.277 o
4 19 0 8.953 7.103 0.650 123.100 o
4 19 1 40.140 41.740 1.251 33.286 o
4 19 2 10.332 10.975 0.810 79.271 o
4 19 3 31.871 34.327 1.171 37.994 o
4 19 4 8.910 8.324 0.620 135.302 o
4 19 5 5.411 5.343 0.510 199.961 o
4 19 6 35.614 36.328 1.271 32.246 o
4 19 7 14.153 12.676 0.890 65.661 o
4 20 1 31.315 32.005 1.161 38.652 o
4 20 2 7.742 8.264 0.600 144.472 o
4 20 3 12.679 12.936 0.860 70.322 o
4 20 4 22.587 22.071 1.071 45.428 o
4 20 5 28.471 28.464 1.171 37.994 o
4 20 6 1.164 1.821 0.420 294.841 o
4 20 7 1.349 1.911 0.420 294.841 o
4 21 0 7.640 7.824 0.610 139.774 o
4 21 1 8.012 7.564 0.680 112.478 o
4 21 2 7.748 9.314 0.810 79.271 o
4 21 3 33.108 33.076 1.231 34.378 o
4 21 4 18.467 19.709 1.020 49.990 o
4 21 5 1.423 2.181 0.430 281.287 o
4 21 6 22.584 22.041 1.081 44.590 o
4 22 1 16.512 13.997 0.940 58.861 o
4 22 2 8.109 9.515 0.650 123.100 o
4 22 3 26.395 24.922 1.141 40.020 o
4 22 4 1.854 2.041 0.460 245.794 o
4 22 5 1.161 1.061 0.400 325.062 o
4 23 0 3.585 4.692 0.500 208.040 o
4 23 1 2.287 2.141 0.440 268.646 o
4 23 2 17.694 17.358 1.010 50.985 o
4 23 3 0.980 0.970 0.400 325.062 o
4 23 4 62.826 62.670 1.621 19.818 o
4 24 0 20.976 21.400 1.061 46.289 o
4 24 1 18.662 19.209 1.030 49.024 o
4 24 2 1.750 1.581 0.410 309.399 o
4 24 3 14.590 13.667 0.950 57.629 o
4 25 1 4.562 5.122 0.570 160.080 o
5 0 1 5.301 5.853 0.400 325.062 o
5 0 2 324.502 324.796 3.442 4.395 o
5 0 3 30.088 30.565 0.750 92.462 o
5 0 5 7.246 6.943 0.550 171.934 o
5 0 6 46.811 46.522 1.131 40.731 o
5 0 7 1.250 1.461 0.360 401.311 o
5 0 8 37.139 35.977 1.151 39.327 o
5 0 10 76.823 73.675 3.071 5.518 o
5 0 11 5.417 3.672 1.491 23.427 o
5 1 0 39.153 39.399 0.760 90.045 o
5 1 1 132.237 131.163 1.631 19.575 o
5 1 2 169.132 166.310 2.011 12.873 o
5 1 3 193.380 195.194 2.321 9.663 o
5 1 4 69.584 68.693 1.191 36.728 o
5 1 5 184.784 182.888 2.341 9.498 o
5 1 6 47.056 44.642 1.091 43.776 o
5 1 7 29.341 29.374 0.980 54.154 o
5 1 8 47.559 46.913 1.291 31.254 o
5 1 9 30.852 29.534 1.121 41.462 o
5 1 10 5.815 5.112 0.880 67.162 o
5 1 11 25.114 23.391 1.961 13.539 o
5 2 0 41.446 42.811 0.810 79.271 o
5 2 1 88.221 89.223 1.261 32.760 o
5 2 3 23.657 24.052 0.680 112.478 o
5 2 4 42.292 42.901 0.930 60.134 o
5 2 5 31.736 31.265 0.870 68.714 o
5 2 6 12.509 10.895 0.680 112.478 o
5 2 7 16.313 16.428 0.830 75.497 o
5 2 8 2.964 3.192 0.420 294.841 o
5 2 9 35.134 34.857 1.391 26.919 o
5 2 10 2.465 2.791 0.560 165.848 o
5 2 11 11.250 12.066 1.581 20.834 o
5 3 0 227.404 226.649 2.521 8.190 o
5 3 1 377.824 374.410 3.832 3.546 o
5 3 2 247.749 247.759 2.791 6.682 o
5 3 3 9.104 9.395 0.500 208.040 o
5 3 4 28.683 27.823 0.790 83.336 o
5 3 5 15.194 15.818 0.660 119.398 o
5 3 6 55.331 52.995 1.211 35.523 o
5 3 7 3.926 3.952 0.420 294.841 o
5 3 9 6.591 5.403 0.600 144.472 o
5 3 10 51.406 50.214 1.691 18.210 o
5 3 11 17.166 16.078 1.151 39.327 o
5 4 0 59.924 59.859 1.000 52.010 o
5 4 1 4.818 5.203 0.400 325.062 o
5 4 2 86.750 84.241 1.271 32.246 o
5 4 3 1.000 1.331 0.380 360.180 o
5 4 4 16.197 16.978 0.650 123.100 o
5 4 5 71.505 71.654 1.341 28.965 o
5 4 6 51.709 48.883 1.181 37.353 o
5 4 7 109.373 105.671 1.851 15.197 o
5 4 8 20.355 19.159 0.940 58.861 o
5 4 9 5.080 6.113 0.620 135.302 o
5 4 10 24.421 24.152 1.261 32.760 o
5 4 11 11.665 10.795 0.890 65.661 o
5 5 0 69.946 71.684 1.121 41.462 o
5 5 1 35.507 35.007 0.760 90.045 o
5 5 2 41.856 41.840 0.870 68.714 o
5 5 3 67.590 67.463 1.161 38.652 o
5 5 4 7.203 6.133 0.500 208.040 o
5 5 5 59.182 58.488 1.221 34.944 o
5 5 6 80.026 78.838 1.521 22.511 o
5 5 7 10.024 10.175 0.660 119.398 o
5 5 8 140.121 137.746 2.291 9.918 o
5 5 9 15.320 13.937 1.040 48.086 o
5 5 10 30.944 29.474 1.421 25.794 o
5 6 1 70.616 69.784 1.141 40.020 o
5 6 2 6.414 6.473 0.450 256.839 o
5 6 3 33.738 34.187 0.840 73.710 o
5 6 4 26.703 27.893 0.820 77.350 o
5 6 5 18.852 18.299 0.770 87.721 o
5 6 6 12.683 13.196 0.720 100.328 o
5 6 7 18.899 20.640 0.890 65.661 o
5 6 9 27.120 26.783 1.261 32.760 o
5 6 10 5.385 6.493 0.670 115.861 o
5 6 11 38.219 39.029 1.501 23.116 o
5 7 0 10.821 11.566 0.530 185.155 o
5 7 1 151.545 151.473 1.921 14.109 o
5 7 2 14.097 12.706 0.570 160.080 o
5 7 3 63.138 62.970 1.171 37.994 o
5 7 4 29.151 29.584 0.850 71.986 o
5 7 5 33.718 33.896 0.960 56.434 o
5 7 6 104.583 102.860 1.791 16.232 o
5 7 7 9.010 9.545 0.730 97.598 o
5 7 8 5.119 5.162 0.480 225.738 o
5 7 9 9.520 9.365 0.820 77.350 o
5 7 10 17.826 17.528 1.161 38.652 o
5 7 11 1.950 2.381 0.550 171.934 o
5 8 0 15.245 16.038 0.600 144.472 o
5 8 1 2.586 3.142 0.410 309.399 o
5 8 2 28.648 28.634 0.790 83.336 o
5 8 3 17.923 18.279 0.680 112.478 o
5 8 4 89.223 87.902 1.501 23.116 o
5 8 5 50.731 49.344 1.181 37.353 o
5 8 6 22.012 21.580 0.890 65.661 o
5 8 7 99.499 98.407 1.861 15.034 o
5 8 8 2.742 2.891 0.430 281.287 o
5 8 9 0.590 1.091 0.500 208.040 o
5 8 10 6.058 6.853 0.670 115.861 o
5 9 0 24.713 25.082 0.730 97.598 o
5 9 1 55.919 57.298 1.111 42.212 o
5 9 2 37.015 36.778 0.900 64.210 o
5 9 3 8.446 8.914 0.580 154.607 o
5 9 4 1.926 2.621 0.370 379.912 o
5 9 5 11.500 10.725 0.690 109.242 o
5 9 6 20.915 20.690 0.870 68.714 o
5 9 7 10.030 11.205 0.750 92.462 o
5 9 8 24.064 23.721 1.040 48.086 o
5 9 9 0.737 1.301 0.410 309.399 o
5 9 10 33.740 32.136 1.391 26.919 o
5 10 0 37.291 37.838 0.910 62.806 o
5 10 1 11.898 12.486 0.600 144.472 o
5 10 2 0.553 1.371 0.430 281.287 o
5 10 3 44.397 42.511 1.040 48.086 o
5 10 4 113.022 110.023 1.801 16.052 o
5 10 5 19.271 18.609 0.820 77.350 o
5 10 6 66.172 67.773 1.491 23.427 o
5 10 7 1.934 1.981 0.400 325.062 o
5 10 8 1.991 2.021 0.420 294.841 o
5 10 9 20.918 20.960 1.051 47.175 o
5 11 0 36.359 36.207 0.940 58.861 o
5 11 1 64.505 67.172 1.261 32.760 o
5 11 2 15.914 15.978 0.710 103.174 o
5 11 3 26.455 25.462 0.870 68.714 o
5 11 4 33.852 34.016 1.020 49.990 o
5 11 5 19.518 20.050 0.880 67.162 o
5 11 6 77.007 78.668 1.641 19.337 o
5 11 7 4.249 4.192 0.460 245.794 o
5 11 8 10.881 12.496 0.860 70.322 o
5 11 9 15.025 15.247 0.960 56.434 o
5 11 10 1.193 1.991 0.520 192.344 o
5 12 0 1.382 1.591 0.470 235.446 o
5 12 1 21.926 21.350 0.800 81.266 o
5 12 2 123.668 122.199 1.901 14.407 o
5 12 3 27.795 26.983 0.920 61.448 o
5 12 4 83.596 84.211 1.601 20.316 o
5 12 5 0.391 0.950 0.340 449.913 o
5 12 7 13.893 13.026 0.780 85.486 o
5 12 8 8.300 7.934 0.620 135.302 o
5 12 9 0.994 1.681 0.420 294.841 o
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8 13 2 2.868 2.681 0.430 281.287 o
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8 13 5 0.931 1.201 0.410 309.399 o
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8 14 1 4.127 4.442 0.480 225.738 o
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9 7 7 1.001 1.331 0.410 309.399 o
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9 13 4 1.221 1.291 0.420 294.841 o
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10 1 2 3.936 3.632 0.450 256.839 o
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10 2 2 49.864 50.144 1.421 25.794 o
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10 2 4 14.260 14.647 0.880 67.162 o
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10 3 1 18.413 18.899 0.930 60.134 o
10 3 2 13.479 14.257 0.860 70.322 o
10 3 3 5.034 5.052 0.490 216.618 o
10 3 4 18.431 17.779 0.990 53.066 o
10 3 5 1.037 1.271 0.410 309.399 o
10 3 7 3.231 3.662 0.470 235.446 o
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10 4 1 14.294 12.956 0.870 68.714 o
10 4 2 16.945 18.619 0.930 60.134 o
10 4 3 15.510 15.457 0.900 64.210 o
10 4 4 13.317 15.457 0.920 61.448 o
10 4 5 22.603 23.031 1.071 45.428 o
10 4 6 1.909 1.971 0.430 281.287 o
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10 5 1 5.655 5.743 0.550 171.934 o
10 5 2 5.993 5.293 0.500 208.040 o
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10 5 5 56.081 56.797 1.581 20.834 o
10 5 6 3.410 3.932 0.490 216.618 o
10 5 7 4.306 4.612 0.490 216.618 o
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10 6 1 40.271 41.000 1.281 31.744 o
10 6 2 2.426 2.671 0.440 268.646 o
10 6 3 56.042 57.167 1.511 22.810 o
10 6 4 4.382 3.882 0.470 235.446 o
10 6 5 17.712 19.720 1.040 48.086 o
10 6 6 3.643 3.152 0.460 245.794 o
10 6 7 36.242 36.858 1.281 31.744 o
10 7 0 0.985 1.311 0.400 325.062 o
10 7 1 11.223 11.706 0.770 87.721 o
10 7 2 36.459 36.608 1.231 34.378 o
10 7 3 2.286 2.401 0.430 281.287 o
10 7 4 39.302 38.819 1.341 28.965 o
10 7 5 2.602 2.181 0.450 256.839 o
10 7 6 13.254 13.016 0.830 75.497 o
10 7 7 11.531 11.676 0.900 64.210 o
10 8 0 3.203 3.041 0.450 256.839 o
10 8 1 1.919 2.151 0.430 281.287 o
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10 8 4 21.196 21.961 1.071 45.428 o
10 8 5 11.728 12.486 0.890 65.661 o
10 8 6 6.103 6.243 0.530 185.155 o
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10 9 1 8.771 9.955 0.830 75.497 o
10 9 2 2.222 2.671 0.450 256.839 o
10 9 3 10.616 10.735 0.850 71.986 o
10 9 4 13.208 15.557 0.950 57.629 o
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10 9 6 6.722 6.633 0.600 144.472 o
10 10 0 4.345 3.662 0.470 235.446 o
10 10 1 11.046 10.925 0.840 73.710 o
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10 10 3 24.303 22.831 1.111 42.212 o
10 10 4 22.666 22.721 1.101 42.983 o
10 10 5 12.491 13.056 0.930 60.134 o
10 10 6 14.822 15.547 0.940 58.861 o
10 11 0 1.997 2.421 0.440 268.646 o
10 11 1 50.104 48.073 1.441 25.082 o
10 11 2 45.223 44.131 1.411 26.161 o
10 11 3 1.669 1.801 0.430 281.287 o
10 11 4 20.083 20.990 1.061 46.289 o
10 11 5 2.301 2.151 0.440 268.646 o
10 12 0 0.907 1.901 0.430 281.287 o
10 12 1 10.640 8.854 0.760 90.045 o
10 12 2 1.487 2.311 0.450 256.839 o
10 12 3 21.259 21.761 1.051 47.175 o
10 12 4 1.108 1.531 0.420 294.841 o
10 12 5 10.891 9.284 0.760 90.045 o
10 13 1 9.169 9.224 0.670 115.861 o
10 13 2 0.527 0.950 0.400 325.062 o
10 13 3 27.148 27.173 1.171 37.994 o
10 13 4 0.715 0.940 0.400 325.062 o
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10 14 1 9.064 8.754 0.750 92.462 o
10 14 2 34.491 34.417 1.261 32.760 o
10 14 3 1.999 2.501 0.450 256.839 o
10 14 4 20.596 19.669 1.020 49.990 o
10 15 0 1.318 1.581 0.420 294.841 o
10 15 1 15.583 16.778 0.980 54.154 o
10 15 2 33.133 33.056 1.241 33.825 o
10 15 3 3.754 2.461 0.440 268.646 o
10 16 1 2.188 2.331 0.440 268.646 o
11 0 2 8.328 7.554 0.690 109.242 o
11 0 3 15.784 15.988 0.960 56.434 o
11 0 4 7.347 7.023 0.610 139.774 o
11 0 5 8.316 9.024 0.660 119.398 o
11 0 6 21.072 18.279 1.030 49.024 o
11 1 1 31.058 30.515 1.191 36.728 o
11 1 2 9.599 10.135 0.830 75.497 o
11 1 3 18.655 19.509 1.000 52.010 o
11 1 4 13.254 14.607 0.940 58.861 o
11 1 5 15.143 14.567 0.970 55.277 o
11 1 6 5.402 4.802 0.500 208.040 o
11 2 0 186.169 183.799 2.871 6.314 o
11 2 1 1.485 1.581 0.420 294.841 o
11 2 2 17.029 14.587 0.960 56.434 o
11 2 3 8.711 8.744 0.730 97.598 o
11 2 4 26.750 27.833 1.161 38.652 o
11 2 5 36.183 35.187 1.281 31.744 o
11 2 6 0.386 0.920 0.430 281.287 o
11 3 0 10.794 10.415 0.770 87.721 o
11 3 1 9.894 8.614 0.730 97.598 o
11 3 2 23.515 20.990 1.071 45.428 o
11 3 4 34.301 35.577 1.281 31.744 o
11 3 5 22.754 22.781 1.051 47.175 o
11 3 6 29.305 27.913 1.151 39.327 o
11 4 1 7.934 8.094 0.630 131.040 o
11 4 2 10.885 12.966 0.880 67.162 o
11 4 3 28.969 27.793 1.171 37.994 o
11 4 4 7.363 7.474 0.570 160.080 o
11 4 5 2.338 2.431 0.440 268.646 o
11 4 6 6.938 7.003 0.600 144.472 o
11 5 1 26.644 26.243 1.131 40.731 o
11 5 2 1.136 1.491 0.420 294.841 o
11 5 3 17.352 19.289 1.000 52.010 o
11 5 4 3.515 3.272 0.460 245.794 o
11 5 5 3.528 3.091 0.460 245.794 o
11 6 0 16.369 19.750 1.020 49.990 o
11 6 1 1.531 1.641 0.430 281.287 o
11 6 2 1.720 1.941 0.430 281.287 o
11 6 3 16.964 18.309 1.010 50.985 o
11 6 4 15.282 16.558 0.940 58.861 o
11 6 5 46.563 48.373 1.481 23.744 o
11 7 0 57.072 58.648 1.571 21.100 o
11 7 1 26.538 28.564 1.151 39.327 o
11 7 2 19.560 19.930 1.040 48.086 o
11 7 3 13.755 12.636 0.910 62.806 o
11 7 4 5.202 5.102 0.520 192.344 o
11 7 5 10.991 12.236 0.870 68.714 o
11 8 0 0.388 0.890 0.410 309.399 o
11 8 1 14.279 15.117 0.950 57.629 o
11 8 2 8.074 9.435 0.750 92.462 o
11 8 3 15.811 15.427 0.990 53.066 o
11 8 4 0.929 1.421 0.410 309.399 o
11 9 0 1.246 1.711 0.420 294.841 o
11 9 1 2.713 2.111 0.440 268.646 o
11 9 2 2.250 2.281 0.450 256.839 o
11 9 3 2.525 3.152 0.460 245.794 o
11 9 4 12.709 10.965 0.790 83.336 o
11 10 0 11.034 10.405 0.790 83.336 o
11 10 1 7.434 7.994 0.640 126.977 o
11 10 2 3.154 3.212 0.470 235.446 o
11 10 3 3.749 3.722 0.470 235.446 o
11 10 4 3.878 3.392 0.460 245.794 o
11 11 0 56.220 55.697 1.531 22.218 o
11 11 1 5.415 5.223 0.510 199.961 o
11 11 2 21.550 21.770 1.061 46.289 o
11 11 3 18.203 16.368 1.000 52.010 o
11 12 0 4.938 4.472 0.490 216.618 o
11 12 1 0.732 0.860 0.400 325.062 o
11 12 2 6.878 6.003 0.580 154.607 o
11 13 0 11.057 9.715 0.780 85.486 o
11 13 1 14.117 13.517 0.800 81.266 o
12 0 0 8.675 8.974 0.670 115.861 o
12 0 1 10.986 12.356 0.880 67.162 o
12 0 2 0.827 0.990 0.400 325.062 o
12 0 4 11.073 14.187 0.920 61.448 o
12 1 0 12.468 13.907 0.940 58.861 o
12 1 1 4.693 5.122 0.510 199.961 o
12 1 2 5.317 5.132 0.510 199.961 o
12 1 3 15.971 18.019 0.970 55.277 o
12 1 4 42.903 44.031 1.391 26.919 o
12 2 0 5.320 5.373 0.570 160.080 o
12 2 1 4.707 3.812 0.480 225.738 o
12 2 2 50.172 47.473 1.481 23.744 o
12 2 4 7.630 9.064 0.830 75.497 o
12 3 0 25.290 24.802 1.121 41.462 o
12 3 1 25.290 22.431 1.101 42.983 o
12 3 2 1.099 1.521 0.420 294.841 o
12 3 3 20.849 20.760 1.051 47.175 o
12 3 4 15.780 17.128 0.990 53.066 o
12 4 0 2.053 2.331 0.440 268.646 o
12 4 1 7.636 8.854 0.690 109.242 o
12 4 2 9.733 8.654 0.750 92.462 o
12 4 3 1.029 1.851 0.420 294.841 o
12 5 0 17.871 17.599 0.980 54.154 o
12 5 1 38.066 34.497 1.281 31.744 o
12 5 2 8.512 7.744 0.620 135.302 o
12 5 3 6.639 7.033 0.690 109.242 o
12 6 0 19.341 20.450 1.030 49.024 o
12 6 2 15.555 15.107 0.970 55.277 o
12 6 3 1.141 0.890 0.400 325.062 o
12 7 0 6.981 8.054 0.570 160.080 o
12 7 1 20.619 22.761 1.101 42.983 o
12 7 2 4.852 4.892 0.500 208.040 o
12 8 1 8.530 10.075 0.850 71.986 o
12 8 2 5.424 5.313 0.570 160.080 o
12 9 0 35.437 35.887 1.281 31.744 o
;
_iucr_refine_instructions_details
;
TITL L-ALA_23K_TONTO_IAM OLEX2: imported from CIF
CELL 0.71073 5.9279 12.2597 5.7939 90 90 90
ZERR 4 0.001 0.0017 0.0009 0 0 0
LATT -1
SYMM 0.5-X,-Y,0.5+Z
SYMM 0.5+X,0.5-Y,-Z
SYMM -X,0.5+Y,0.5-Z
SFAC C H N O
UNIT 12 28 4 8
CONF
MORE -1
BOND $H
ACTA
LIST -3
WGHT 0 0
FVAR 0.999759
REM
REM
REM
N1 3 0.64723 0.13752 0.18292 11.00000 0.00557 0.00616 0.00434 =
-0.00012 0.00070 0.00012
H1a 2 0.70386 0.05931 0.20145 11.00000 0.02934 0.03445 0.01472 =
-0.00277 0.00886 -0.00488
H1b 2 0.77742 0.18996 0.21155 11.00000 0.02245 0.02493 0.02165 =
-0.00163 0.00166 0.00434
H1c 2 0.58046 0.14950 0.01821 11.00000 0.02328 0.01539 0.03295 =
-0.00842 0.02059 -0.00228
C1 1 0.46639 0.16112 0.35429 11.00000 0.00535 0.00488 0.00368 =
0.00009 -0.00054 0.00039
H1 2 0.42672 0.24810 0.34261 11.00000 0.02735 0.01496 0.02301 =
0.00218 -0.00726 0.00548
C2 1 0.25992 0.09066 0.30333 11.00000 0.00604 0.00898 0.00628 =
-0.00042 -0.00057 -0.00137
H2a 2 0.19115 0.11020 0.13334 11.00000 0.02388 0.04611 0.02041 =
0.00431 -0.00442 -0.01168
H2b 2 0.12592 0.10455 0.43036 11.00000 0.02179 0.03934 0.02858 =
0.00211 0.00391 -0.00714
H2c 2 0.30313 0.00517 0.30831 11.00000 0.02793 0.02532 0.03640 =
0.00007 0.00173 -0.00741
C3 1 0.55406 0.14079 0.59985 11.00000 0.00498 0.00458 0.00363 =
-0.00006 -0.00013 0.00047
O1 4 0.72667 0.08380 0.62429 11.00000 0.00683 0.00711 0.00561 =
0.00047 -0.00062 0.00234
O2 4 0.44091 0.18401 0.76109 11.00000 0.00746 0.00754 0.00397 =
-0.00043 0.00043 0.00210
HKLF 4
END
Q1 1 0.5 0.222222 0.90625 11 0.05 0.16
Q2 1 0.5 0.138889 0.53125 11 0.05 0.16
Q3 1 0.861111 0.041667 0.0625 11 0.05 0.15
Q4 1 0.555556 0.055556 0.46875 11 0.05 0.15
Q5 1 0.194444 0.041667 0.09375 11 0.05 0.15
REM The information below was added by Olex2.
REM
REM R1 = 0.0196 for 2387 Fo > 4sig(Fo) and 0.0196 for all 2387 data
REM 118 parameters refined using 0 restraints
REM Highest difference peak 0.1628, deepest hole -0.1652
REM Mean Shift 0.0000, Max Shift 0.0005.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0196
REM R1_gt = 0.0196
REM wR_ref = 0.0332
REM GOOF = 1.2147
REM Shift_max = 0.0005
REM Shift_mean = 0.0000
REM Reflections_all = 2387
REM Reflections_gt = 2387
REM Parameters = 118
REM Hole = -0.1652
REM Peak = 0.1628
REM Flack = n/a
;
# END of CIF
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_Pau100m71
_database_code_depnum_ccdc_archive 'CCDC 2034389'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-09-28 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-06-19
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.04.27 svn.r7e0b91c7 for OlexSys, GUI svn.r6014)
;
_chemical_formula_moiety 'C6 H6 O2, C0.286 O0.57'
_chemical_formula_sum 'C6.286 H6 O2.57'
_chemical_formula_weight 122.681
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_dispersion_source
H 0.00000 0.00000 Sasaki
C 0.00210 0.00160 Sasaki
O 0.00790 0.00610 Sasaki
_space_group_crystal_system trigonal
_space_group_IT_number 148
_space_group_name_H-M_alt 'R -3'
_space_group_name_Hall '-R 3'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -y,x-y,z
3 -x+y,-x,z
4 -x,-y,-z
5 y,-x+y,-z
6 x-y,x,-z
7 x+1/3,y+2/3,z+2/3
8 -y+1/3,x-y+2/3,z+2/3
9 -x+y+1/3,-x+2/3,z+2/3
10 -x+1/3,-y+2/3,-z+2/3
11 y+1/3,-x+y+2/3,-z+2/3
12 x-y+1/3,x+2/3,-z+2/3
13 x+2/3,y+1/3,z+1/3
14 -y+2/3,x-y+1/3,z+1/3
15 -x+y+2/3,-x+1/3,z+1/3
16 -x+2/3,-y+1/3,-z+1/3
17 y+2/3,-x+y+1/3,-z+1/3
18 x-y+2/3,x+1/3,-z+1/3
_symmetry_Int_Tables_number 148
_cell_length_a 16.2023(11)
_cell_length_b 16.2023(11)
_cell_length_c 5.6943(4)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 120
_cell_volume 1294.57(15)
_cell_formula_units_Z 9
_cell_measurement_temperature 100(2)
_cell_measurement_reflns_used 7311
_cell_measurement_theta_min 2.51
_cell_measurement_theta_max 37.99
_exptl_crystal_description block
_exptl_crystal_colour colourless
_exptl_crystal_size_max 0.5
_exptl_crystal_size_mid 0.4
_exptl_crystal_size_min 0.3
_exptl_absorpt_coefficient_mu 0.111
_exptl_absorpt_correction_type multi-scans
_exptl_absorpt_correction_T_min 0.7063
_exptl_absorpt_correction_T_max 0.7475
_exptl_absorpt_process_details 'SADABS (Bruker-AXS)'
_exptl_crystal_density_diffrn 1.416
_exptl_crystal_F_000 578.780
_diffrn_reflns_av_R_equivalents 0.0173
_diffrn_reflns_av_unetI/netI 0.0133
_diffrn_reflns_Laue_measured_fraction_full 0.9527
_diffrn_reflns_Laue_measured_fraction_max 0.9408
_diffrn_reflns_limit_h_max 27
_diffrn_reflns_limit_h_min -24
_diffrn_reflns_limit_k_max 25
_diffrn_reflns_limit_k_min -27
_diffrn_reflns_limit_l_max 9
_diffrn_reflns_limit_l_min -9
_diffrn_reflns_number 8426
_diffrn_reflns_point_group_measured_fraction_full 0.9527
_diffrn_reflns_point_group_measured_fraction_max 0.9408
_diffrn_reflns_theta_full 25.2417
_diffrn_reflns_theta_max 37.99
_diffrn_reflns_theta_min 3.86
_diffrn_measured_fraction_theta_full 0.9527
_diffrn_measured_fraction_theta_max 0.9408
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.71073
_reflns_Friedel_coverage 0.0
_reflns_limit_h_max 23
_reflns_limit_h_min 0
_reflns_limit_k_max 24
_reflns_limit_k_min 1
_reflns_limit_l_max 9
_reflns_limit_l_min -9
_reflns_number_gt 1375
_reflns_number_total 1477
_reflns_threshold_expression I>=2u(I)
_computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_diffrn_ambient_temperature 100(2)
_diffrn_measurement_device_type 'Bruker APEX-II CCD'
_diffrn_measurement_method '\f and \w scans'
_computing_data_collection 'Bruker APEX2'
_computing_cell_refinement 'Bruker SAINT'
_computing_data_reduction 'Bruker SAINT'
_computing_structure_solution 'SHELXS-97 (Sheldrick 2008)'
_refine_diff_density_max 0.2272
_refine_diff_density_min -0.2533
_refine_diff_density_rms 0.0239
_refine_ls_d_res_high 0.5774
_refine_ls_d_res_low 5.2764
_refine_ls_goodness_of_fit_ref 1.1216
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_constraints 1
_refine_ls_number_parameters 70
_refine_ls_number_reflns 1477
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0162
_refine_ls_R_factor_gt 0.0145
_refine_ls_restrained_S_all 1.1216
_refine_ls_shift/su_max 0.0007
_refine_ls_shift/su_mean 0.0001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0118P)^2^+0.0845P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0332
_refine_ls_wR_factor_ref 0.0338
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be published - 2020
NoSpherA2 implementation of HAR makes use of
tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or DFT using selected funtionals
- for a fragment of the crystal.
This fregment can be embedded in an electrostatic crystal field by employing cluster charges.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
INT ACCURACY: High
METHOD: PBE
BASIS SET: def2-TZVPP
CHARGE: 0
MULTIPLICITY: 1
DATE: 2020-06-19_12-42-38
;
_olex2_refinement_description
;
1. Others
Sof(C4)=Sof(O2)=FVAR(1)
;
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
O1 O 0.436229(12) 0.578735(12) 0.16464(3) 0.01560(4) Uani 1.000000 1 . . .
C1 C 0.469611(14) 0.541809(14) 0.33313(4) 0.01239(4) Uani 1.000000 1 . . .
C2 C 0.522277(15) 0.594862(14) 0.52678(4) 0.01402(4) Uani 1.000000 1 . . .
C3 C 0.552478(15) 0.552592(15) 0.69364(4) 0.01403(4) Uani 1.000000 1 . . .
C4 C 0.333333333333 0.666666666667 0.666666666667 0.02222(15) Uani 0.855(2) 6 S
T P
O2 O 0.333333333333 0.666666666667 0.46383(9) 0.03519(16) Uani 0.855(2) 3 S T P
H2 H 0.5396(3) 0.6685(3) 0.5475(9) 0.0317(12) Uani 1.000000 1 . . .
H3 H 0.5925(4) 0.5917(3) 0.8464(8) 0.0328(12) Uani 1.000000 1 . . .
H1 H 0.4645(4) 0.6468(4) 0.1793(10) 0.0319(14) Uani 1.000000 1 . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O1 0.01426(7) 0.01286(7) 0.01891(8) 0.00621(5) -0.00185(5) 0.00070(5)
C1 0.01045(7) 0.01010(7) 0.01568(9) 0.00444(6) 0.00011(6) -0.00031(6)
C2 0.01405(8) 0.00983(7) 0.01746(9) 0.00542(6) -0.00153(6) -0.00164(6)
C3 0.01386(8) 0.01066(8) 0.01639(9) 0.00526(6) -0.00203(6) -0.00202(6)
C4 0.0225(2) 0.0225(2) 0.0217(3) 0.01125(10) -0.000000 0.000000
O2 0.0419(2) 0.0419(2) 0.0217(2) 0.02097(11) -0.000000 0.000000
H2 0.040(3) 0.018(2) 0.040(3) 0.017(2) -0.009(2) -0.003(2)
H3 0.043(3) 0.029(3) 0.027(3) 0.018(2) -0.010(2) -0.011(2)
H1 0.031(3) 0.028(3) 0.036(4) 0.015(3) -0.007(3) -0.001(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C1 1.3764(3) . ?
O1 H1 0.963(6) . ?
C1 C2 1.3962(3) . ?
C1 C3 1.3940(3) 4_666 ?
C2 C3 1.3951(3) . ?
C2 H2 1.087(4) . ?
C3 H3 1.081(5) . ?
C4 O2 1.1550(5) 16_566 ?
C4 O2 1.1550(5) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
H1 O1 C1 111.8(3) . . ?
C2 C1 O1 122.338(19) . . ?
C3 C1 O1 117.361(19) 4_666 . ?
C3 C1 C2 120.292(19) 4_666 . ?
C3 C2 C1 119.475(19) . . ?
H2 C2 C1 120.3(3) . . ?
H2 C2 C3 120.2(3) . . ?
C2 C3 C1 120.23(2) . 4_666 ?
H3 C3 C1 118.8(2) . 4_666 ?
H3 C3 C2 121.0(2) . . ?
O2 C4 O2 180.0 16_566 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 C1 C2 C3 178.79(2) . . . . ?
O1 C1 C3 C2 -178.838(19) . . 4_666 4_666 ?
C1 C2 C3 C1 0.13(2) . . . 4_666 ?
C1 C3 C2 C1 0.13(2) 4_666 . . . ?
# start Validation Reply Form
_vrf_PLAT927_Pau100m71
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0755 Check
RESPONSE: Non-Spherical refinement, therefore wR2 from CheckCIF is wrong
;
_vrf_PLAT928_Pau100m71
;
PROBLEM: Reported and Calculated S value Differ by . -2.505 Check
RESPONSE: Non-Spherical refinement, therefore S from CheckCIF is wrong
;
_vrf_PLAT029_Pau100m71
;
PROBLEM: _diffrn_measured_fraction_theta_full value Low . 0.953 Why?
RESPONSE: Data was used as published and deposited.
;
_vrf_PLAT926_Pau100m71
;
PROBLEM: Reported and Calculated R1 Differ by ......... -0.0238 Check
RESPONSE: Non-Spherical refinement, therefore R1 from CheckCIF is wrong
;
# end Validation Reply Form
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
0 -1 1 84.67 1.83
0 -1 1 86.87 1.94
0 1 -1 85.11 2.11
0 1 -1 84.24 1.81
-1 1 1 87.19 1.8
-1 1 1 87.69 2.02
2 1 -2 254.88 5.4
2 1 -2 256.98 6.27
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-22 1 -2 17.74 0.69
22 -1 2 17.64 0.7
-2 -22 -1 1.88 0.25
-2 -22 -1 2.25 0.26
2 22 1 2.36 0.27
-22 -2 -2 2.19 0.28
22 2 2 2.75 0.32
22 -20 3 1.91 0.27
22 -17 3 12.12 0.59
22 -14 3 1.27 0.23
22 -14 3 1.18 0.21
22 -11 3 -0.06 0.13
-22 8 -3 0.66 0.18
22 -8 3 0.64 0.19
-22 5 -3 1.26 0.22
22 -5 3 1.57 0.24
-22 2 -3 8 0.47
22 -2 3 7.28 0.46
3 22 -1 9.87 0.53
22 1 3 0.09 0.14
22 -21 4 2.59 0.34
22 -18 4 0.34 0.18
22 -15 4 6.6 0.46
22 -12 4 2.2 0.28
22 -12 4 2 0.28
22 -9 4 8.03 0.49
22 -9 4 6.81 0.46
-22 6 -4 0.11 0.14
22 -6 4 0.14 0.17
22 -6 4 0.21 0.17
-22 3 -4 5.63 0.41
22 -3 4 5.23 0.45
22 -3 4 5.57 0.42
22 0 4 1.14 0.23
22 -16 5 0.2 0.18
22 -13 5 0.8 0.23
22 -13 5 0.63 0.19
22 -10 5 4.18 0.38
22 -10 5 3.58 0.39
-22 7 -5 7.7 0.45
22 -7 5 6.57 0.48
22 -7 5 6.67 0.48
-22 4 -5 1.41 0.25
22 -4 5 1.46 0.26
22 -11 6 8.2 0.53
22 -23 0 5.94 0.38
21 -23 2 2.85 0.29
21 -23 -1 52 1.4
20 -23 1 0.77 0.17
20 -23 -2 12.65 0.56
19 -23 0 7.3 0.41
19 -23 -3 14.57 0.61
18 -23 2 0.27 0.14
18 -23 -1 22.71 0.77
18 -23 -4 1.02 0.21
17 -23 1 9.12 0.44
17 -23 -2 2.98 0.3
16 -23 3 17.73 0.62
16 -23 0 45.09 1.23
16 -23 -3 14.19 0.59
15 -23 2 4.21 0.3
15 -23 -1 6.92 0.4
15 -23 -4 5.49 0.38
14 -23 1 -0.05 0.11
14 -23 -2 10.64 0.5
14 -23 -5 0.4 0.17
14 -23 -5 0.43 0.17
13 -23 3 19.61 0.66
13 -23 0 1.99 0.24
13 -23 -3 41.62 1.18
12 -23 2 2.35 0.26
12 -23 -1 9.38 0.46
12 -23 -4 0.07 0.13
12 -23 -4 0 0.13
11 -23 1 2.28 0.27
11 -23 -2 28 0.9
11 -23 -2 28.19 0.88
11 -23 -5 6.74 0.41
11 -23 -5 7.13 0.45
10 -23 3 0.28 0.12
10 -23 0 20.24 0.69
10 -23 0 20.19 0.7
10 -23 -3 1.61 0.23
10 -23 -3 1.41 0.22
9 -23 2 5.8 0.35
9 -23 -1 1.32 0.22
9 -23 -1 1.17 0.19
9 -23 -4 1.72 0.25
9 -23 -4 1.84 0.25
-9 23 4 2.02 0.24
8 -23 4 10.25 0.45
8 -23 1 14.26 0.56
8 -23 1 13.79 0.52
8 -23 -2 10.81 0.51
8 -23 -2 11.73 0.52
-8 23 2 11.42 0.43
8 -23 -5 0.14 0.14
-8 23 5 0.28 0.14
7 -23 3 1.07 0.19
7 -23 0 11.28 0.51
7 -23 0 11.32 0.49
-7 23 0 11.21 0.42
7 -23 -3 3.85 0.34
7 -23 -3 3.87 0.33
-7 23 3 4.01 0.28
6 -23 2 23.55 0.77
6 -23 -1 70.84 1.8
6 -23 -1 72.54 1.82
-6 23 1 71.46 1.64
6 -23 -4 30.99 0.99
6 -23 -4 29.26 0.93
-6 23 4 30.71 0.9
23 -14 -5 0.66 0.17
23 -11 -5 0.11 0.13
5 -23 4 2.13 0.25
5 -23 1 0.3 0.13
5 -23 1 0.23 0.11
-5 23 -1 0.05 0.1
5 -23 -2 9.23 0.46
5 -23 -2 9.8 0.48
-5 23 2 9.24 0.42
23 -15 -4 10.05 0.48
23 -12 -4 19.69 0.72
23 -9 -4 4.77 0.35
23 -6 -4 3.65 0.33
4 -23 3 8.59 0.44
4 -23 0 22 0.73
4 -23 0 23.08 0.77
-4 23 0 22.61 0.7
4 -23 -3 4.29 0.33
4 -23 -3 4.14 0.35
-4 23 3 4.68 0.32
23 -16 -3 0.98 0.18
23 -13 -3 0.08 0.12
23 -10 -3 20.51 0.74
23 -7 -3 18.48 0.7
23 -4 -3 0.27 0.15
3 -23 2 1.01 0.19
-3 23 -2 0.58 0.16
23 -1 -3 0.49 0.16
3 -23 -1 11.41 0.51
3 -23 -1 12.18 0.53
-3 23 1 11.6 0.48
3 -23 -4 0.92 0.17
-3 23 4 0.96 0.19
23 -23 -2 3.59 0.33
23 -20 -2 0.75 0.17
23 -17 -2 23.85 0.8
23 -14 -2 5.71 0.36
23 -11 -2 2.07 0.25
23 -8 -2 4.38 0.33
23 -5 -2 0.46 0.16
23 -2 -2 3.17 0.31
2 -23 1 0.66 0.16
-2 23 -1 0.67 0.16
23 1 -2 0.25 0.14
2 -23 -2 3.6 0.31
2 -23 -2 4.16 0.33
-2 23 2 4.25 0.32
23 -21 -1 0.52 0.16
23 -18 -1 0.24 0.13
23 -15 -1 14.25 0.58
23 -12 -1 2.41 0.26
23 -9 -1 0.06 0.12
23 -6 -1 9.41 0.47
1 -23 3 -0.05 0.12
23 -3 -1 0.77 0.17
1 -23 -3 1.25 0.22
1 -23 -3 1.15 0.22
1 -23 -3 1.18 0.2
-1 23 3 1.23 0.21
23 -22 0 41.1 1.16
23 -19 0 22.96 0.8
23 -19 0 22.48 0.73
23 -16 0 12.28 0.55
23 -13 0 20.72 0.75
23 -10 0 2.35 0.27
23 -7 0 43.55 1.29
-23 4 0 6.68 0.41
23 -4 0 7.42 0.42
0 -23 2 3.23 0.32
0 23 -2 3.36 0.32
-23 1 0 6.31 0.4
23 -1 0 6.73 0.4
0 -23 -1 1.17 0.21
0 -23 -1 0.99 0.19
0 23 1 0.68 0.17
23 2 0 0.15 0.14
23 -23 1 0.89 0.19
23 -20 1 12.44 0.56
23 -20 1 11.73 0.5
23 -17 1 72.73 1.97
23 -14 1 1.21 0.21
23 -11 1 9.73 0.5
23 -8 1 6.43 0.41
-23 5 -1 23.84 0.82
23 -5 1 23.67 0.85
-23 2 -1 54.66 1.48
23 -2 1 52.11 1.54
1 23 -1 5.71 0.37
-23 -1 -1 7.93 0.45
23 1 1 8.17 0.46
23 -21 2 3.78 0.35
23 -18 2 10.07 0.43
23 -18 2 9.71 0.52
23 -15 2 10.93 0.54
23 -12 2 27.74 0.95
23 -9 2 9.67 0.51
-23 6 -2 3.45 0.34
23 -6 2 3.57 0.34
-23 3 -2 12.9 0.58
23 -3 2 12.43 0.59
-23 0 -2 3.7 0.36
23 0 2 3.56 0.33
23 -19 3 4.26 0.38
23 -16 3 3.47 0.36
23 -13 3 1.44 0.25
23 -10 3 42.52 1.33
-23 7 -3 14.87 0.63
23 -7 3 14.84 0.67
-23 4 -3 14.5 0.63
23 -4 3 14.19 0.65
23 -1 3 2.32 0.3
23 -20 4 0.65 0.21
23 -17 4 31.09 1.1
23 -14 4 2.09 0.31
23 -11 4 0.06 0.16
23 -11 4 -0.02 0.14
-23 8 -4 6.13 0.42
23 -8 4 5.49 0.44
23 -8 4 5.58 0.45
-23 5 -4 1 0.21
23 -5 4 0.68 0.23
23 -5 4 0.8 0.22
23 -15 5 0.17 0.19
23 -12 5 7.53 0.49
23 -12 5 7.35 0.52
23 -9 5 0.42 0.2
23 -9 5 0.6 0.21
23 -24 -1 5.99 0.4
22 -24 1 1.49 0.22
22 -24 -2 1.92 0.27
21 -24 0 2.26 0.27
20 -24 2 0.83 0.18
20 -24 -1 11.06 0.52
19 -24 1 2.94 0.3
19 -24 -2 28.86 0.93
18 -24 0 40.41 1.15
18 -24 -3 33.34 1.03
17 -24 2 1.25 0.2
17 -24 -1 0.29 0.16
17 -24 -4 0.81 0.21
16 -24 1 2.85 0.29
16 -24 -2 3.11 0.32
15 -24 3 4.63 0.32
15 -24 0 7.33 0.42
15 -24 -3 16.64 0.66
14 -24 2 1.91 0.23
14 -24 -1 8.52 0.45
14 -24 -4 2.75 0.33
14 -24 -4 2.71 0.3
13 -24 1 1.06 0.2
13 -24 -2 24.08 0.81
12 -24 3 0.52 0.15
12 -24 0 8.67 0.45
12 -24 -3 4 0.35
12 -24 -3 4.09 0.35
11 -24 2 27.86 0.86
11 -24 -1 7.69 0.43
11 -24 -1 7.87 0.44
11 -24 -4 1.1 0.22
11 -24 -4 1.39 0.23
10 -24 1 6.44 0.36
10 -24 1 6.69 0.39
10 -24 -2 8.63 0.46
10 -24 -2 8.85 0.47
9 -24 3 9.7 0.44
9 -24 0 13.43 0.55
9 -24 0 13.88 0.57
9 -24 -3 2.67 0.31
9 -24 -3 2.37 0.28
8 -24 2 16.4 0.62
8 -24 -1 78.16 1.93
8 -24 -1 75.62 1.93
8 -24 -4 5.73 0.39
8 -24 -4 6.54 0.42
7 -24 4 8.05 0.42
7 -24 1 0.34 0.15
7 -24 1 0.02 0.1
7 -24 -2 9.09 0.47
7 -24 -2 8.83 0.47
-7 24 2 9.06 0.4
6 -24 3 9.38 0.46
6 -24 0 9.77 0.45
6 -24 0 8.98 0.47
-6 24 0 9.38 0.4
6 -24 -3 5.54 0.39
6 -24 -3 5.55 0.39
-6 24 3 5.56 0.34
5 -24 2 1.04 0.18
5 -24 -1 0.09 0.12
5 -24 -1 0.39 0.16
-5 24 1 0.22 0.11
-5 24 4 4.31 0.33
24 -17 -4 7.69 0.42
24 -14 -4 7.74 0.43
24 -11 -4 5.7 0.38
24 -8 -4 1.39 0.23
4 -24 1 9.3 0.46
-4 24 -1 7.99 0.4
4 -24 -2 0.17 0.13
4 -24 -2 0.64 0.17
-4 24 2 0.05 0.11
24 -18 -3 8.27 0.43
24 -15 -3 9.1 0.46
24 -12 -3 0.35 0.15
24 -9 -3 5.07 0.37
24 -6 -3 37.62 1.17
3 -24 3 10.37 0.51
3 -24 0 5.23 0.37
3 -24 0 5.35 0.34
-3 24 0 5.09 0.33
3 -24 -3 1.62 0.23
-3 24 3 1.52 0.22
24 -22 -2 1.9 0.25
24 -19 -2 0.93 0.18
24 -16 -2 15.63 0.62
24 -13 -2 29.03 0.95
24 -10 -2 2.04 0.25
24 -7 -2 1.63 0.24
24 -4 -2 0.76 0.18
2 -24 2 2.8 0.3
-2 24 -2 2.5 0.27
2 -24 -1 4.38 0.33
2 -24 -1 4.77 0.37
-2 24 1 4.83 0.34
24 -23 -1 8.54 0.45
24 -20 -1 7.74 0.43
24 -20 -1 8.29 0.42
24 -17 -1 0.12 0.12
24 -14 -1 6.8 0.41
24 -11 -1 1.18 0.2
24 -8 -1 3.34 0.31
24 -5 -1 2.76 0.29
24 -2 -1 2.08 0.26
1 -24 1 7.67 0.5
-1 24 -1 8.51 0.43
1 -24 -2 0.31 0.16
24 -21 0 5.81 0.37
24 -18 0 9.46 0.48
24 -15 0 13.16 0.58
24 -12 0 9.62 0.49
24 -9 0 7.6 0.44
24 -6 0 39.71 1.22
-24 3 0 2.27 0.27
24 -3 0 2.07 0.26
24 0 0 0.34 0.15
0 24 0 0.2 0.14
24 -22 1 4.28 0.32
24 -19 1 0.17 0.11
24 -19 1 0.16 0.14
24 -16 1 78.25 2.11
24 -13 1 7.24 0.44
24 -10 1 8.06 0.46
24 -7 1 0.35 0.17
-24 4 -1 12.24 0.57
24 -4 1 11.25 0.56
-24 1 -1 6.2 0.43
24 -1 1 6.69 0.42
24 -20 2 0.61 0.19
24 -17 2 9.15 0.52
24 -14 2 8.25 0.48
24 -11 2 22.94 0.86
24 -8 2 3.03 0.33
-24 5 -2 28.32 0.94
24 -5 2 28.18 0.98
-24 2 -2 1.49 0.26
24 -2 2 1.86 0.28
24 -21 3 1.6 0.26
24 -18 3 6.12 0.45
24 -15 3 2.4 0.31
24 -12 3 4.35 0.39
24 -9 3 17.44 0.74
-24 6 -3 35.32 1.09
24 -6 3 32.66 1.14
24 -3 3 1.28 0.25
24 -16 4 5.45 0.45
24 -13 4 1.01 0.22
24 -13 4 1.01 0.24
24 -10 4 3 0.37
24 -10 4 2.75 0.34
-24 7 -4 1 0.22
24 -7 4 1.06 0.24
24 -7 4 1 0.25
21 -25 1 0.99 0.2
20 -25 0 15.67 0.63
19 -25 2 25.44 0.82
19 -25 -1 5.99 0.4
18 -25 1 10.13 0.49
18 -25 -2 1.7 0.26
17 -25 0 0.29 0.16
17 -25 -3 11.62 0.56
16 -25 2 36.38 1.06
16 -25 -1 0.13 0.15
15 -25 1 -0.01 0.13
15 -25 -2 7.9 0.46
14 -25 3 23.29 0.76
14 -25 0 1.65 0.23
14 -25 -3 13.01 0.59
14 -25 -3 12.93 0.6
13 -25 2 0.92 0.19
13 -25 -1 4.8 0.37
13 -25 -4 0.81 0.22
12 -25 1 -0.04 0.11
12 -25 1 0.01 0.13
12 -25 -2 15.32 0.63
12 -25 -2 15.42 0.63
11 -25 0 -0.1 0.13
11 -25 0 0.03 0.12
11 -25 -3 -0.07 0.13
11 -25 -3 -0.02 0.14
10 -25 2 27.78 0.88
10 -25 -1 20.97 0.75
10 -25 -1 22.27 0.78
9 -25 1 3.35 0.31
9 -25 1 3.31 0.28
9 -25 -2 1.64 0.25
9 -25 -2 1.37 0.22
8 -25 3 14.85 0.59
8 -25 0 1.44 0.23
8 -25 0 1.53 0.21
8 -25 -3 41.16 1.2
8 -25 -3 42 1.24
7 -25 2 0.63 0.16
7 -25 -1 1.81 0.24
7 -25 -1 1.39 0.21
6 -25 1 0.28 0.14
6 -25 -2 4.4 0.35
6 -25 -2 4.33 0.36
-6 25 2 4.2 0.3
5 -25 0 4.97 0.35
5 -25 0 4.93 0.33
-5 25 0 5.21 0.32
-5 25 3 28.26 0.86
25 -16 -4 17.32 0.73
25 -13 -4 6.42 0.44
4 -25 -1 16.39 0.63
4 -25 -1 15.61 0.63
-4 25 1 15.4 0.57
25 -17 -3 14.11 0.59
25 -14 -3 0.15 0.13
25 -11 -3 23.54 0.84
25 -8 -3 1.28 0.22
-3 25 -1 1.18 0.2
-3 25 2 6.57 0.41
25 -18 -2 0.38 0.15
25 -15 -2 24.69 0.85
25 -12 -2 1.1 0.2
25 -9 -2 35.21 1.12
25 -6 -2 26.84 0.93
-2 25 0 0.18 0.12
25 -22 -1 0.96 0.21
25 -19 -1 0.25 0.15
25 -16 -1 3.92 0.34
25 -13 -1 0.09 0.13
25 -10 -1 0.13 0.13
25 -7 -1 10.57 0.52
25 -4 -1 1.02 0.2
25 -20 0 5.1 0.38
25 -20 0 4.82 0.33
25 -17 0 1.72 0.25
25 -14 0 0.24 0.15
25 -11 0 2.17 0.27
25 -8 0 0.34 0.16
25 -5 0 15.68 0.66
25 -21 1 15.94 0.68
25 -21 1 16.17 0.61
25 -18 1 1.84 0.27
25 -18 1 2.04 0.21
25 -15 1 22.31 0.83
25 -12 1 4.9 0.39
25 -9 1 0.19 0.15
25 -6 1 5.92 0.42
25 -3 1 10.56 0.54
25 -19 2 4.78 0.4
25 -16 2 1.19 0.23
25 -13 2 16.15 0.71
25 -10 2 8.35 0.5
25 -7 2 1.93 0.28
25 -4 2 9.33 0.54
25 -17 3 41.79 1.35
25 -14 3 -0.05 0.15
25 -14 3 0.13 0.16
25 -11 3 13.45 0.67
25 -8 3 11.91 0.62
25 -12 4 0.99 0.23
20 -26 1 12.34 0.56
19 -26 0 2.71 0.32
18 -26 2 18.8 0.69
18 -26 -1 -0.04 0.15
17 -26 1 10.97 0.52
17 -26 -2 0.02 0.16
16 -26 0 8.41 0.46
15 -26 2 0.01 0.13
15 -26 -1 0.22 0.16
14 -26 1 2.75 0.31
14 -26 -2 0.61 0.19
14 -26 -2 0.09 0.15
13 -26 3 19.91 0.7
13 -26 0 3.73 0.33
13 -26 0 3.97 0.36
12 -26 2 0.46 0.16
12 -26 -1 2.87 0.31
12 -26 -1 3.29 0.34
11 -26 1 1.84 0.25
11 -26 1 1.73 0.22
11 -26 -2 11.18 0.53
11 -26 -2 9.78 0.52
10 -26 3 12.24 0.53
10 -26 0 -0.05 0.13
10 -26 0 0.17 0.13
9 -26 2 0.48 0.15
9 -26 -1 7.23 0.44
9 -26 -1 6.76 0.41
8 -26 1 2.65 0.3
8 -26 -2 31.88 1.02
8 -26 -2 30.53 0.99
7 -26 0 2.52 0.27
7 -26 0 1.86 0.25
6 -26 -1 0.2 0.13
26 -16 -3 9.84 0.51
26 -13 -3 17.66 0.72
26 -17 -2 -0.04 0.13
26 -14 -2 0.42 0.15
26 -11 -2 -0.06 0.12
26 -8 -2 17.68 0.74
26 -18 -1 2.09 0.27
26 -15 -1 1.75 0.25
26 -12 -1 2.75 0.31
26 -9 -1 10.71 0.55
26 -19 0 1.94 0.27
26 -16 0 0.18 0.15
26 -13 0 3.92 0.36
26 -10 0 9.85 0.53
26 -7 0 2.45 0.32
26 -20 1 -0.04 0.11
26 -20 1 0.1 0.15
26 -17 1 6.15 0.44
26 -14 1 3.28 0.34
26 -11 1 0.19 0.16
26 -8 1 0.15 0.16
26 -18 2 31.46 1.09
26 -15 2 11.35 0.59
26 -12 2 0.37 0.18
26 -9 2 0.01 0.15
26 -13 3 3.46 0.38
17 -27 2 0 0.15
16 -27 1 0.04 0.14
15 -27 0 16.11 0.66
14 -27 2 1.21 0.21
14 -27 -1 7.01 0.44
14 -27 -1 6.84 0.45
13 -27 1 -0.07 0.13
12 -27 0 0.05 0.12
12 -27 0 0.04 0.15
11 -27 -1 3.33 0.32
9 -27 0 1.59 0.22
27 -17 -1 4.62 0.38
27 -14 -1 0.11 0.15
27 -11 -1 0.04 0.16
27 -18 0 1.74 0.26
27 -15 0 -0.09 0.13
27 -12 0 16.42 0.72
27 -16 1 2.94 0.35
27 -13 1 6.77 0.46
-3 -9 -3 23.15 0.74
-3 -9 -3 22.84 0.63
6 -12 0 4.87 0.17
-3 -9 -3 23.93 0.69
-6 12 0 5.18 0.18
0 0 0 0 0
_iucr_refine_fcf_details
;
data_Pau100m71_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -y,x-y,z
3 -x+y,-x,z
4 -x,-y,-z
5 y,-x+y,-z
6 x-y,x,-z
7 x+1/3,y+2/3,z+2/3
8 -y+1/3,x-y+2/3,z+2/3
9 -x+y+1/3,-x+2/3,z+2/3
10 -x+1/3,-y+2/3,-z+2/3
11 y+1/3,-x+y+2/3,-z+2/3
12 x-y+1/3,x+2/3,-z+2/3
13 x+2/3,y+1/3,z+1/3
14 -y+2/3,x-y+1/3,z+1/3
15 -x+y+2/3,-x+1/3,z+1/3
16 -x+2/3,-y+1/3,-z+1/3
17 y+2/3,-x+y+1/3,-z+1/3
18 x-y+2/3,x+1/3,-z+1/3
_space_group_crystal_system trigonal
_space_group_IT_number 148
_space_group_name_H-M_alt 'R -3 :H'
_space_group_name_Hall '-R 3'
_symmetry_space_group_name_H-M 'R -3 :H'
_symmetry_space_group_name_Hall '-R 3'
_symmetry_Int_Tables_number 148
_cell_length_a 16.2023(11)
_cell_length_b 16.2023(11)
_cell_length_c 5.6943(4)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 120
_cell_volume 1294.57(15)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
0 1 -7 209.346 202.583 3.812 7.838 o
0 1 -4 783.676 748.063 6.165 1.598 o
0 1 -1 1323.720 1296.900 11.755 0.607 o
0 1 2 3455.000 3477.360 25.334 0.114 o
0 1 5 69.225 65.933 0.976 40.511 o
0 1 8 206.315 203.625 4.102 7.436 o
0 2 -8 261.512 274.540 4.916 5.274 o
0 2 -5 915.554 890.363 8.744 1.111 o
0 2 -2 2184.840 2226.670 15.732 0.269 o
0 2 1 9790.700 9583.770 341.626 0.002 o
0 2 4 206.685 188.246 1.657 11.776 o
0 2 7 19.384 15.781 1.085 108.006 o
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14 11 0 1.337 0.734 0.778 424.840 o
14 11 3 0.496 1.032 1.024 269.703 o
14 12 -1 47.712 47.790 2.484 28.320 o
14 12 2 5.870 5.284 0.995 202.203 o
14 13 1 0.682 -1.215 0.837 403.408 o
15 1 -7 1.716 1.669 0.814 369.649 o
15 1 -4 16.628 14.210 0.874 139.614 o
15 1 -1 399.943 394.235 4.239 4.041 o
15 1 2 156.218 157.298 2.392 13.320 o
15 1 5 131.923 131.168 2.497 15.066 o
15 2 -5 121.510 122.657 2.308 16.838 o
15 2 -2 51.715 50.530 1.354 45.586 o
15 2 1 733.327 732.019 7.530 1.538 o
15 2 4 5.997 8.820 0.846 227.631 o
15 2 7 80.038 81.846 3.349 15.735 o
15 3 -6 75.544 85.388 3.105 17.358 o
15 3 -3 86.860 86.641 2.137 23.010 o
15 3 0 2.439 2.113 1.509 120.428 o
15 3 3 181.677 175.038 6.639 4.675 o
15 3 6 23.427 21.880 2.867 29.135 o
15 4 -4 856.906 849.849 12.202 0.922 o
15 4 -1 71.022 69.043 1.702 31.267 o
15 4 2 1336.340 1326.690 12.809 0.567 o
15 4 5 28.956 28.366 1.818 50.936 o
15 5 -5 384.062 381.213 5.260 3.700 o
15 5 -2 7.112 7.049 0.777 246.451 o
15 5 1 389.621 371.999 4.202 4.217 o
15 5 4 351.272 366.422 5.279 3.936 o
15 6 -6 422.067 453.590 13.882 1.167 o
15 6 -3 81.876 81.088 2.596 20.465 o
15 6 0 472.675 479.047 6.832 2.519 o
15 6 3 0.277 0.000 1.358 160.219 o
15 6 6 4.778 6.649 1.651 93.507 o
15 7 -4 103.112 101.892 2.657 17.319 o
15 7 -1 0.067 0.020 0.565 919.910 o
15 7 2 291.801 290.950 4.981 4.860 o
15 7 5 6.587 5.320 1.173 156.625 o
15 8 -5 4.625 3.137 1.098 191.470 o
15 8 -2 170.321 169.223 3.284 10.212 o
15 8 1 210.728 214.311 3.371 8.383 o
15 8 4 166.500 156.672 3.326 10.429 o
15 9 -3 30.003 37.414 2.604 30.806 o
15 9 0 205.584 204.233 3.415 8.546 o
15 9 3 141.235 142.822 3.182 11.963 o
15 10 -1 325.677 328.281 5.851 3.884 o
15 10 2 405.243 401.891 5.745 3.312 o
15 11 -2 157.204 162.434 7.061 4.460 o
15 11 1 25.453 25.956 1.443 68.705 o
15 12 0 0.004 -0.383 0.778 492.128 o
16 1 -6 1.822 1.279 1.196 189.874 o
16 1 -3 198.867 199.863 3.032 9.441 o
16 1 0 141.192 138.101 3.976 9.805 o
16 1 3 12.157 14.662 1.124 124.950 o
16 1 6 120.894 132.434 3.532 11.832 o
16 2 -4 70.068 71.894 2.167 26.221 o
16 2 -1 210.914 207.430 2.813 9.377 o
16 2 2 219.279 224.935 3.152 8.405 o
16 2 5 102.156 103.259 2.339 19.101 o
16 3 -5 1.102 1.778 0.701 493.494 o
16 3 -2 4.067 3.511 0.735 342.481 o
16 3 1 145.581 144.113 3.500 10.856 o
16 3 4 6.033 5.514 1.280 139.310 o
16 4 -6 47.937 43.586 2.578 27.403 o
16 4 -3 86.745 84.077 2.289 22.038 o
16 4 0 341.484 338.575 4.982 4.269 o
16 4 3 68.730 71.231 2.303 25.134 o
16 4 6 23.180 22.176 2.754 31.079 o
16 5 -4 177.792 171.114 3.413 9.679 o
16 5 -1 2.814 2.239 0.663 449.793 o
16 5 2 407.502 408.550 5.546 3.368 o
16 5 5 78.007 80.892 2.785 19.477 o
16 6 -5 3.345 3.553 0.995 232.781 o
16 6 -2 134.439 131.797 2.784 13.846 o
16 6 1 8.137 9.526 0.799 216.676 o
16 6 4 211.034 222.723 6.082 4.837 o
16 7 -3 55.515 57.083 2.092 31.209 o
16 7 0 177.709 174.494 2.999 10.539 o
16 7 3 12.655 14.286 1.259 109.346 o
16 8 -4 88.068 89.802 4.664 9.823 o
16 8 -1 1162.050 1156.280 14.655 0.595 o
16 8 2 244.114 240.018 4.574 6.000 o
16 9 -2 19.120 21.267 2.024 51.132 o
16 9 1 54.051 55.709 2.200 30.194 o
16 9 4 248.605 261.621 6.202 4.333 o
16 10 0 0.742 0.670 0.865 368.699 o
16 10 3 166.659 165.859 6.665 4.780 o
16 11 -1 43.654 45.422 2.835 24.738 o
16 11 2 76.193 65.036 6.187 6.603 o
17 1 -5 990.860 992.288 10.643 0.891 o
17 1 -2 0.607 0.687 0.508 957.521 o
17 1 1 873.919 866.245 8.807 1.158 o
17 1 4 17.498 19.169 1.317 90.188 o
17 2 -6 36.381 38.768 1.852 44.073 o
17 2 -3 50.702 50.607 1.846 37.034 o
17 2 0 1.994 2.133 0.622 532.482 o
17 2 3 0.074 0.145 0.728 553.553 o
17 2 6 0.003 1.613 1.181 206.851 o
17 3 -4 543.289 533.674 7.903 2.002 o
17 3 -1 136.049 133.443 2.699 14.019 o
17 3 2 201.903 204.946 5.545 5.555 o
17 4 -5 48.377 51.852 2.688 25.357 o
17 4 -2 234.712 233.390 3.213 7.886 o
17 4 1 0.019 0.517 0.553 927.556 o
17 4 4 509.441 502.740 6.735 2.400 o
17 5 -3 183.879 179.269 3.491 9.243 o
17 5 0 216.063 213.477 3.060 8.761 o
17 5 3 2.386 2.855 0.932 274.975 o
17 6 -4 446.079 459.840 7.330 2.479 o
17 6 -1 1093.330 1084.040 13.551 0.674 o
17 6 2 368.249 357.549 8.371 2.494 o
17 7 -2 138.088 136.279 3.462 11.358 o
17 7 1 1.591 1.648 0.803 381.185 o
17 7 4 108.520 118.649 2.998 14.758 o
17 8 -3 640.319 628.241 10.966 1.292 o
17 8 0 21.146 22.831 1.502 71.713 o
17 8 3 225.564 220.520 4.115 6.953 o
17 9 -1 97.147 101.753 3.901 11.963 o
17 9 2 1.611 1.860 1.786 89.406 o
17 10 1 69.007 70.428 3.160 18.030 o
18 1 -4 21.958 21.718 1.290 83.300 o
18 1 -1 76.295 74.316 1.725 29.320 o
18 1 2 1.553 2.549 0.715 443.865 o
18 1 5 1.221 1.714 0.871 340.340 o
18 2 -5 176.979 181.385 3.730 8.912 o
18 2 -2 153.669 156.202 2.538 13.053 o
18 2 1 12.107 12.765 0.868 164.072 o
18 2 4 8.731 6.576 1.210 138.637 o
18 3 -3 91.141 99.856 2.591 18.753 o
18 3 0 456.564 454.831 6.716 2.644 o
18 3 3 63.569 66.532 2.108 28.439 o
18 4 -4 3.235 4.060 0.981 236.346 o
18 4 -1 19.987 21.036 1.113 98.846 o
18 4 2 49.516 51.936 1.907 36.159 o
18 4 5 16.036 23.087 4.678 12.691 o
18 5 -2 141.456 144.530 2.790 13.153 o
18 5 1 1.894 2.510 0.660 485.592 o
18 5 4 30.970 30.096 2.278 37.672 o
18 6 -3 81.513 84.098 2.537 20.781 o
18 6 0 140.995 142.007 3.369 11.425 o
18 6 3 124.285 131.738 3.109 13.174 o
18 7 -1 21.342 25.894 1.771 57.958 o
18 7 2 5.147 6.604 1.119 171.956 o
18 8 -2 479.817 471.964 8.981 1.950 o
18 8 1 28.862 32.126 2.200 39.766 o
18 9 0 22.865 23.367 1.700 60.702 o
19 1 -3 29.887 27.040 3.018 25.538 o
19 1 0 31.262 30.533 1.181 71.830 o
19 1 3 227.631 222.874 5.195 5.599 o
19 2 -4 199.324 203.758 3.533 8.494 o
19 2 -1 31.379 31.225 1.344 64.938 o
19 2 2 187.309 182.175 3.862 8.417 o
19 2 5 45.355 46.973 2.916 23.510 o
19 3 -2 89.366 88.798 2.425 20.514 o
19 3 1 242.521 238.364 5.750 4.841 o
19 3 4 199.239 201.143 8.299 3.262 o
19 4 -3 63.894 64.447 2.263 26.824 o
19 4 0 348.107 343.336 3.969 4.821 o
19 4 3 110.998 127.566 4.798 8.573 o
19 5 -4 63.517 61.210 3.697 15.268 o
19 5 -1 2.235 2.927 0.709 418.978 o
19 5 2 14.216 13.858 1.596 79.163 o
19 6 -2 63.104 66.361 2.617 23.195 o
19 6 1 1.255 3.496 1.027 243.435 o
19 7 0 30.233 31.097 1.767 51.122 o
19 8 -1 77.705 62.923 5.885 7.177 o
20 1 -2 431.922 424.062 4.956 3.441 o
20 1 1 1298.800 1292.460 12.788 0.586 o
20 1 4 185.002 200.917 4.036 7.963 o
20 2 -3 25.419 28.665 1.643 59.181 o
20 2 0 368.348 370.771 4.534 4.209 o
20 2 3 34.445 34.077 1.980 42.677 o
20 3 -4 10.620 13.281 1.637 81.204 o
20 3 -1 173.822 178.824 3.468 9.565 o
20 3 2 9.696 11.992 1.688 79.485 o
20 4 -2 2.908 4.768 1.654 98.199 o
20 4 1 123.505 124.742 3.194 13.061 o
20 5 -3 437.046 432.006 9.528 1.934 o
20 5 0 70.564 75.322 2.105 26.482 o
20 6 -1 0.736 0.855 0.963 299.998 o
21 1 -4 37.734 37.647 1.952 41.431 o
21 1 -1 73.631 73.868 1.936 27.769 o
21 1 2 152.843 155.715 3.752 9.811 o
21 2 -2 57.185 60.157 2.194 29.210 o
21 2 1 9.450 9.506 1.105 146.523 o
21 3 -3 20.873 23.809 2.047 48.844 o
21 3 0 77.575 80.971 2.649 20.506 o
21 3 3 168.566 156.478 7.696 3.875 o
21 4 -1 237.009 237.420 3.523 7.393 o
22 1 -3 19.210 19.320 1.453 78.680 o
22 1 0 599.540 605.264 10.218 1.448 o
22 1 3 0.109 0.221 1.375 156.638 o
22 2 -1 66.668 67.164 2.056 28.388 o
22 2 2 37.008 36.636 2.312 34.452 o
22 3 -2 100.330 99.138 6.187 6.194 o
22 3 1 16.058 16.699 1.825 62.827 o
23 1 -2 3.617 4.195 1.590 104.509 o
23 1 1 123.027 123.781 3.079 13.533 o
23 2 0 1.482 2.507 1.375 145.748 o
;
_iucr_refine_instructions_details
;
TITL Pau100 in R-3
CELL 0.71073 16.2023 16.2023 5.6943 90 90 120
ZERR 9 0.0011 0.0011 0.0004 0 0 0
LATT 3
SYMM -Y,+X-Y,+Z
SYMM +Y-X,-X,+Z
SFAC C H O
DISP C 0.0021 0.0016 11.5003
DISP H 0 0 0.624
DISP O 0.0079 0.0061 32.4922
UNIT 56.57 54 23.14
L.S. 10
PLAN 5
CONF
BOND $H
MORE -1
fmap 2
acta
LIST -6
OMIT 3 9 3
OMIT 6 6 0
WGHT 0.011827 0.08445
FVAR 0.257432 0.85495
REM
REM
REM
O1 3 0.43623 0.57873 0.16464 11.00000 0.01426 0.01286 0.01891 =
0.00070 -0.00185 0.00621
C1 1 0.46961 0.54181 0.33313 11.00000 0.01045 0.01010 0.01568 =
-0.00031 0.00011 0.00444
C2 1 0.52228 0.59486 0.52678 11.00000 0.01405 0.00983 0.01746 =
-0.00164 -0.00153 0.00542
C3 1 0.55248 0.55259 0.69364 11.00000 0.01386 0.01066 0.01639 =
-0.00202 -0.00203 0.00526
C4 1 0.33333 0.66667 0.66667 21.00000 0.02249 0.02249 0.02169 =
0.00000 0.00000 0.01125
O2 3 0.33333 0.66667 0.46383 21.00000 0.04195 0.04195 0.02167 =
0.00000 0.00000 0.02097
H2 2 0.53962 0.66850 0.54754 11.00000 0.04024 0.01791 0.03997 =
-0.00327 -0.00913 0.01681
H3 2 0.59252 0.59174 0.84638 11.00000 0.04278 0.02885 0.02651 =
-0.01095 -0.01046 0.01775
H1 2 0.46455 0.64678 0.17927 11.00000 0.03125 0.02808 0.03610 =
-0.00089 -0.00696 0.01467
HKLF 4
END
Q3 1 0.5 0.569444 0.426667 11 0.05 0.09
Q1 1 0.333333 0.666667 0.413333 11 0.05 0.23
Q2 1 0.430556 0.583333 0.266667 11 0.05 0.11
Q4 1 0.416667 0.569444 0.506667 11 0.05 0.08
Q5 1 0.569444 0.555556 0.586667 11 0.05 0.08
REM The information below was added by Olex2.
REM
REM R1 = 0.0145 for 1375 Fo > 4sig(Fo) and 0.0162 for all 1477 data
REM 70 parameters refined using 0 restraints
REM Highest difference peak 0.2272, deepest hole -0.2533
REM Mean Shift 0.0001, Max Shift 0.0007.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0162
REM R1_gt = 0.0145
REM wR_ref = 0.0338
REM GOOF = 1.1216
REM Shift_max = 0.0007
REM Shift_mean = 0.0001
REM Reflections_all = 1477
REM Reflections_gt = 1375
REM Parameters = 70
REM Hole = -0.2533
REM Peak = 0.2272
REM Flack = n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_GlyAla_12K_NoSpherA2_ORCA_NoSpherA2
_database_code_depnum_ccdc_archive 'CCDC 2035148'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-10-02 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-17-11
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.01.16 svn.ra754ea2f for OlexSys, GUI svn.r6014)
;
#----------------------------------------------------------------------------#
# CHEMICAL INFORMATION #
#----------------------------------------------------------------------------#
_chemical_name_systematic Glycil-L-Alanine
_chemical_name_common Glycil-L-Alanine
_chemical_formula_moiety 'C5 H10 N2 O3'
_chemical_formula_sum 'C5 H10 N2 O3'
_chemical_formula_weight 146.1471
_chemical_absolute_configuration syn
#----------------------------------------------------------------------------#
# UNIT CELL INFORMATION #
#----------------------------------------------------------------------------#
_symmetry_cell_setting Orthorhombic
_symmetry_space_group_name_H-M 'p 21 21 21'
_symmetry_space_group_name_Hall 'p 2ac 2ab'
_symmetry_Int_Tables_number 19
loop_
_symmetry_equiv_pos_as_xyz
'+x, +y, +z'
'-x+1/2, -y, +z+1/2'
'+x+1/2, -y+1/2, -z'
'-x, +y+1/2, -z+1/2'
_cell_length_a 7.4583(4)
_cell_length_b 9.4892(7)
_cell_length_c 9.7301(6)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 688.63(8)
_cell_formula_units_Z 4
_cell_measurement_temperature 12(2)
_cell_measurement_reflns_used 276
_cell_measurement_theta_min 6.05
_cell_measurement_theta_max 21.1
#----------------------------------------------------------------------------#
# CRYSTAL INFORMATION #
#----------------------------------------------------------------------------#
_exptl_crystal_description Prismatic
_exptl_crystal_colour Colourless
_exptl_crystal_size_max 0.1
_exptl_crystal_size_mid 0.08
_exptl_crystal_size_min 0.05
_exptl_crystal_density_diffrn 1.41
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 312
#----------------------------------------------------------------------------#
# ABSORPTION CORRECTION #
#----------------------------------------------------------------------------#
_exptl_absorpt_coefficient_mu 0.071
_exptl_absorpt_correction_type none
#----------------------------------------------------------------------------#
# DATA COLLECTION #
#----------------------------------------------------------------------------#
_diffrn_ambient_temperature 12(2)
_diffrn_radiation_wavelength 0.5259
_diffrn_radiation_type synchrotron
_diffrn_radiation_monochromator 'Si(111) double crystal'
_diffrn_detector_area_resol_mean 0.657
_diffrn_measurement_device_type 'Bruker SMART-CCD'
_diffrn_measurement_method 'area detector'
_diffrn_reflns_av_R_equivalents 0.0253
_diffrn_reflns_av_unetI/netI 0.026
_diffrn_reflns_number 8493
_diffrn_reflns_limit_h_min -11
_diffrn_reflns_limit_h_max 10
_diffrn_reflns_limit_k_min -14
_diffrn_reflns_limit_k_max 13
_diffrn_reflns_limit_l_min -14
_diffrn_reflns_limit_l_max 14
_diffrn_reflns_theta_min 2.57
_diffrn_reflns_theta_max 23.637
_diffrn_reflns_theta_full 18.393
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.976
_diffrn_reflns_Laue_measured_fraction_full 0.979
_diffrn_reflns_Laue_measured_fraction_max 0.976
_diffrn_reflns_point_group_measured_fraction_full 0.982
_diffrn_reflns_point_group_measured_fraction_max 0.969
_reflns_Friedel_fraction_full 0.986
_reflns_Friedel_fraction_max 0.958
_reflns_Friedel_coverage 0.711
_reflns_number_total 2394
_reflns_number_gt 2394
_reflns_threshold_expression I/u(I)>2.1
#----------------------------------------------------------------------------#
# COMPUTER PROGRAMS USED #
#----------------------------------------------------------------------------#
_computing_structure_solution 'SHELXS-2013 (Sheldrick, 2008)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
#----------------------------------------------------------------------------#
# STRUCTURE SOLUTION #
#----------------------------------------------------------------------------#
_atom_sites_solution_hydrogens difmap
#----------------------------------------------------------------------------#
# REFINEMENT INFORMATION #
#----------------------------------------------------------------------------#
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
_atom_type_scat_dispersion_source
H 0.00000 0.00000 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
C 0.00347 0.00161 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
O 0.01158 0.00611 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
N 0.00653 0.00323 'NoSPherA2 (see refine special details)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
_refine_diff_density_max 0.1480
_refine_diff_density_min -0.1877
_refine_diff_density_rms 0.0574
_refine_ls_abs_structure_details
'Flack, H. D. (1983). Acta Cryst. A39, 876-881.'
_refine_ls_abs_structure_Flack 0.1(7)
_refine_ls_d_res_high 0.6558
_refine_ls_d_res_low 5.8638
_refine_ls_goodness_of_fit_ref 1.2843
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 181
_refine_ls_number_reflns 2374
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0158
_refine_ls_R_factor_gt 0.0158
_refine_ls_restrained_S_all 1.2843
_refine_ls_shift/su_max 0.0009
_refine_ls_shift/su_mean 0.0002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details w=1/[\s^2^(Fo^2^)]
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0308
_refine_ls_wR_factor_ref 0.0308
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be publsihed - 2020
NoSpherA2 makes use of tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or B3LYP
- for a fragment of the crystal embedded in
an electrostatic crystal field.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
METHOD: rhf
BASIS SET: 6-311G(d,p)
CHARGE: 0
MULTIPLICITY: 1
DATE: 2020-01-24_12-16-57
;
#----------------------------------------------------------------------------#
# VALIDATION REPLY FORM #
#----------------------------------------------------------------------------#
# end Validation Reply Form
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_refinement_flags_posn
O(1) O -0.26775(4) -0.96250(3) -0.77796(3) 0.00568(5) Uani 1.000000 .
O(2) O -0.43046(4) -1.12553(3) -0.88361(3) 0.00505(6) Uani 1.000000 .
O(3) O -0.70877(4) -0.94883(3) -0.60022(3) 0.00539(5) Uani 1.000000 .
N(1) N -0.44247(4) -1.03635(4) -0.52555(3) 0.00374(6) Uani 1.000000 .
N(2) N -0.73417(4) -0.75564(4) -0.40093(3) 0.00412(6) Uani 1.000000 .
C(1) C -0.37319(5) -1.06533(4) -0.77671(3) 0.00331(6) Uani 1.000000 .
C(2) C -0.42592(5) -1.13472(4) -0.63921(3) 0.00359(6) Uani 1.000000 .
C(3) C -0.28337(6) -1.24507(4) -0.60454(4) 0.00787(7) Uani 1.000000 .
C(4) C -0.58862(5) -0.95479(4) -0.51389(3) 0.00346(6) Uani 1.000000 .
C(5) C -0.59817(5) -0.86705(4) -0.38208(4) 0.00465(7) Uani 1.000000 .
H(1) H -0.3550(9) -1.0420(9) -0.4483(7) 0.0214(18) Uani 1.000000 .
H(2a H -0.8615(9) -0.8016(9) -0.4084(9) 0.022(2) Uani 1.000000 .
H(2b H -0.7328(11) -0.6803(10) -0.3237(8) 0.0238(19) Uani 1.000000 .
H(2c H -0.7043(12) -0.7019(9) -0.4913(7) 0.0200(19) Uani 1.000000 .
H(2) H -0.5555(8) -1.1847(8) -0.6579(5) 0.0150(14) Uani 1.000000 .
H(3a H -0.1545(9) -1.1924(8) -0.5862(7) 0.0253(19) Uani 1.000000 .
H(3b H -0.3210(11) -1.3043(8) -0.5146(8) 0.0310(19) Uani 1.000000 .
H(3c H -0.2674(11) -1.3166(9) -0.6902(7) 0.0289(18) Uani 1.000000 .
H(5a H -0.4657(8) -0.8178(8) -0.3609(7) 0.0180(16) Uani 1.000000 .
H(5b H -0.6357(10) -0.9342(8) -0.2940(6) 0.0210(17) Uani 1.000000 .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O(1) 0.00833(12) 0.00501(12) 0.00371(10) -0.00289(10) 0.00132(9) -0.00131(10)
O(2) 0.00613(12) 0.00623(13) 0.00280(10) -0.00193(10) 0.00020(9) -0.00129(9)
O(3) 0.00624(11) 0.00565(13) 0.00429(10) 0.00139(10) -0.00169(9) -0.00110(10)
N(1) 0.00515(13) 0.00360(14) 0.00246(11) 0.00086(12) 0.00021(10) -0.00107(10)
N(2) 0.00498(14) 0.00311(14) 0.00426(12) 0.00120(11) 0.00064(11) -0.00044(11)
C(1) 0.00438(14) 0.00283(15) 0.00271(12) -0.00016(11) -0.00015(10) -0.00110(12)
C(2) 0.00531(15) 0.00293(16) 0.00251(12) 0.00007(13) 0.00026(11) 0.00044(11)
C(3) 0.01196(17) 0.00592(17) 0.00574(14) 0.00456(14) -0.00019(13) 0.00049(13)
C(4) 0.00450(14) 0.00329(14) 0.00257(12) 0.00076(13) -0.00001(10) -0.00031(11)
C(5) 0.00645(15) 0.00479(16) 0.00269(13) 0.00088(13) -0.00036(11) -0.00100(12)
H(1) 0.019(4) 0.021(5) 0.024(3) 0.009(4) -0.015(3) -0.006(4)
H(2a 0.011(4) 0.021(5) 0.034(5) 0.006(4) 0.003(4) 0.001(4)
H(2b 0.025(5) 0.025(5) 0.022(4) 0.011(4) 0.001(3) -0.000(4)
H(2c 0.026(5) 0.015(5) 0.019(4) -0.004(4) -0.005(3) 0.006(4)
H(2) 0.021(4) 0.010(4) 0.013(3) -0.006(3) 0.001(3) -0.004(3)
H(3a 0.026(4) 0.024(5) 0.026(4) 0.012(4) -0.008(3) -0.005(4)
H(3b 0.042(5) 0.022(5) 0.030(4) 0.013(4) -0.000(4) 0.006(4)
H(3c 0.039(5) 0.026(4) 0.021(4) 0.014(4) 0.002(3) -0.014(4)
H(5a 0.015(4) 0.018(4) 0.021(3) 0.000(3) -0.004(3) -0.006(3)
H(5b 0.042(5) 0.009(4) 0.012(3) -0.001(3) 0.000(3) 0.007(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O(1) C(1) 1.2533(4) . ?
O(2) C(1) 1.2612(4) . ?
O(3) C(4) 1.2295(4) . ?
N(1) C(2) 1.4525(4) . ?
N(1) C(4) 1.3416(5) . ?
N(1) H(1) 0.997(6) . ?
N(2) C(5) 1.4765(5) . ?
N(2) H(2a 1.047(7) . ?
N(2) H(2b 1.037(9) . ?
N(2) H(2c 1.041(7) . ?
C(1) C(2) 1.5422(5) . ?
C(2) C(3) 1.5299(5) . ?
C(2) H(2) 1.092(6) . ?
C(3) H(3a 1.098(7) . ?
C(3) H(3b 1.077(8) . ?
C(3) H(3c 1.082(7) . ?
C(4) C(5) 1.5308(5) . ?
C(5) H(5a 1.112(6) . ?
C(5) H(5b 1.104(6) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C(4) N(1) C(2) 120.27(3) . . ?
H(1) N(1) C(2) 119.0(4) . . ?
H(1) N(1) C(4) 119.9(4) . . ?
H(2a N(2) C(5) 109.5(4) . . ?
H(2b N(2) C(5) 113.4(4) . . ?
H(2b N(2) H(2a 110.3(6) . . ?
H(2c N(2) C(5) 108.0(5) . . ?
H(2c N(2) H(2a 109.8(6) . . ?
H(2c N(2) H(2b 105.8(6) . . ?
O(2) C(1) O(1) 123.86(3) . . ?
C(2) C(1) O(1) 120.06(3) . . ?
C(2) C(1) O(2) 115.83(3) . . ?
C(1) C(2) N(1) 114.07(3) . . ?
C(3) C(2) N(1) 109.33(3) . . ?
C(3) C(2) C(1) 107.84(3) . . ?
H(2) C(2) N(1) 109.3(3) . . ?
H(2) C(2) C(1) 105.5(3) . . ?
H(2) C(2) C(3) 110.8(4) . . ?
H(3a C(3) C(2) 109.5(4) . . ?
H(3b C(3) C(2) 110.8(4) . . ?
H(3b C(3) H(3a 109.5(6) . . ?
H(3c C(3) C(2) 109.6(4) . . ?
H(3c C(3) H(3a 108.3(6) . . ?
H(3c C(3) H(3b 109.1(6) . . ?
N(1) C(4) O(3) 124.12(3) . . ?
C(5) C(4) O(3) 120.89(3) . . ?
C(5) C(4) N(1) 114.99(3) . . ?
C(4) C(5) N(2) 108.50(3) . . ?
H(5a C(5) N(2) 109.4(4) . . ?
H(5a C(5) C(4) 110.0(3) . . ?
H(5b C(5) N(2) 109.6(4) . . ?
H(5b C(5) C(4) 110.4(4) . . ?
H(5b C(5) H(5a 108.9(5) . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O(1) C(1) C(2) N(1) 35.43(4) . . . . ?
O(1) C(1) C(2) C(3) -86.20(4) . . . . ?
O(2) C(1) C(2) N(1) -150.12(3) . . . . ?
O(2) C(1) C(2) C(3) 88.24(4) . . . . ?
O(3) C(4) N(1) C(2) -5.69(5) . . . . ?
O(3) C(4) C(5) N(2) -16.22(4) . . . . ?
N(1) C(4) C(5) N(2) 164.08(3) . . . . ?
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
2 0 0 3691.45 124.97
-3 0 0 2.31 0.87
4 0 0 708.78 24.25
-4 0 0 717.91 24.17
6 0 0 8142.54 262.94
-6 0 0 7417.66 261.83
8 0 0 153.15 7.28
-8 0 0 155.28 6.11
-10 0 0 19.12 5.53
10 0 0 18.13 7.09
-1 -1 0 1110.41 39.29
-1 -1 0 1201.01 40.19
-2 -1 0 9999.99 316.93
2 1 0 8774.4 316.37
4 -1 0 395.71 13.62
4 1 0 390.31 13.73
-4 -1 0 405.3 13.66
-5 -1 0 1397.37 47.41
5 -1 0 1434.56 47.45
5 1 0 1381.13 47.51
-6 -1 0 694.14 23.04
6 1 0 642.43 23.2
6 -1 0 683.76 23.17
8 -1 0 1418.44 48.87
-8 -1 0 1471.32 48.54
8 1 0 1404.28 48.9
-9 -1 0 409.62 16.03
9 -1 0 449.53 16.67
-9 -1 0 476.64 15.92
9 1 0 434.42 16.56
-11 -1 0 571.41 22.45
-11 1 0 650.8 22.48
-1 2 0 3118.27 104.65
-1 -2 0 3036.73 104.05
-1 -2 0 3059.26 104.23
1 2 0 3068.05 104.66
-2 -2 0 936.21 31.75
-2 -2 0 931.43 31.75
2 2 0 949.44 31.76
-3 -2 0 1507.04 51.21
-3 -2 0 1486.87 50.52
3 2 0 1500.37 50.54
4 -2 0 482.9 16.05
-4 -2 0 456.13 16.2
4 2 0 475.45 16.26
-5 -2 0 1027.68 34.26
5 -2 0 1030.29 34.17
5 2 0 969.51 34.3
-6 -2 0 215.62 8
6 -2 0 216.99 7.97
6 2 0 213.34 8.18
-7 -2 0 9 2.91
7 -2 0 15.73 3.48
7 2 0 10.23 3.39
8 2 0 53.89 4.93
-8 -2 0 57.95 4.31
8 -2 0 58.56 4.96
-8 -2 0 58.05 4.06
-9 -2 0 883.02 31.24
9 2 0 881.41 31.71
-9 -2 0 930.53 31.32
9 -2 0 929.55 31.82
-11 -2 0 97.93 8.83
1 3 0 86.21 3.31
-1 -3 0 86.5 3.14
1 -3 0 90.09 3.31
-1 3 0 80.52 3.34
-1 -3 0 87.9 3.43
-3 -3 0 549.35 18.77
-4 -3 0 4992.73 165.51
4 3 0 4913.65 166.61
-4 -3 0 4878.98 166.27
-5 -3 0 8.43 2.22
5 -3 0 11.24 1.36
-5 -3 0 9.58 2.35
5 3 0 10.05 2.38
-6 -3 0 265.8 9.97
6 3 0 287.85 10.16
6 -3 0 262.65 9.69
-6 -3 0 278.76 10.02
7 3 0 96.9 5.1
-7 -3 0 96.38 4.84
-7 -3 0 91.08 4.87
7 -3 0 95.87 4.84
-8 -3 0 8.7 3.79
-9 -3 0 564.97 20.22
-9 -3 0 553.92 20.1
9 3 0 558.85 20.41
9 -3 0 573.65 20.58
-10 -3 0 665.26 23.55
10 -3 0 654.44 24.48
-10 -3 0 658.68 23.61
-10 3 0 664.46 23.35
10 3 0 625.23 23.78
0 -4 0 1242.82 42.21
0 4 0 1258.37 42.2
1 -4 0 39.16 2.25
1 4 0 41.48 2.23
-1 -4 0 43.2 2.43
-1 -4 0 48.09 1.84
-1 4 0 40.06 2.3
-3 4 0 570.59 20.46
3 4 0 604.93 20.46
-3 -4 0 606.97 20.56
-3 -4 0 617.47 20.51
-4 -4 0 4976.29 166.76
5 4 0 704.33 24.6
-5 -4 0 716.57 24.58
-5 -4 0 731.56 24.63
-6 -4 0 21.52 3.23
-6 -4 0 16.6 3.03
6 -4 0 23.61 2
6 4 0 16.78 2.93
7 4 0 956.41 32.84
7 -4 0 967.58 32.58
-7 -4 0 964.1 32.83
-7 -4 0 934.81 32.7
8 -4 0 360.32 13.28
-8 -4 0 358.59 13.25
8 4 0 347.64 13.31
9 4 0 306.66 12.45
-9 -4 0 314.03 12.53
-9 -4 0 305.18 12.44
9 -4 0 335 13.2
10 4 0 79.59 7.25
10 -4 0 77.63 9.33
-10 4 0 69.14 7.18
-10 -4 0 75.6 7.78
-10 -4 0 76.87 7.45
1 5 0 3.95 1.83
-2 -5 0 762.12 26.25
-2 5 0 757.5 26.2
-2 -5 0 787.42 26.11
-3 -5 0 737.43 24.34
-3 5 0 693.51 24.36
-3 -5 0 699.61 24.43
3 5 0 722.65 24.24
-4 -5 0 1130.77 38.88
-4 -5 0 1149.67 38.9
-4 5 0 1127.27 38.84
4 5 0 1176.28 38.84
-6 5 0 281.14 10.37
-6 -5 0 269.23 10.27
-6 5 0 285.31 10.11
-6 -5 0 282.57 10.38
6 5 0 258.59 10.15
7 -5 0 8.45 2.65
8 -5 0 65.09 5.03
-8 5 0 70.93 5.33
8 5 0 61.76 5.02
-8 -5 0 65.35 5.44
-8 -5 0 63.35 5.29
9 -5 0 26.2 6.53
9 5 0 18.24 5.29
-9 -5 0 36.51 5.96
-9 5 0 19.8 5.66
-10 5 0 587.86 20.56
-10 -5 0 562.3 20.67
-10 -5 0 535.89 21.01
10 5 0 528.89 20.5
0 6 0 1484.98 50.24
0 -6 0 1491.35 50.3
-1 -6 0 417.87 14.91
1 6 0 428.06 15.2
-1 6 0 429.85 15.25
-1 -6 0 473.56 15.38
-2 6 0 1953.53 66.26
-2 -6 0 1905.55 66.21
-2 -6 0 2085.25 66.33
2 -6 0 1920.18 66.21
-3 -6 0 168.57 6.39
-3 6 0 170.6 6.75
-3 -6 0 173.76 6.89
3 6 0 168.13 6.13
-4 6 0 127.1 5.74
-4 -6 0 135.14 5.36
4 6 0 126.74 5.13
-4 -6 0 133.32 5.86
-5 -6 0 223.22 8.35
-5 6 0 216.61 8.63
5 6 0 215.93 8.17
-5 -6 0 219.31 8.64
-6 -6 0 33.66 3.65
-6 -6 0 34.88 4.19
6 6 0 34.44 3.45
-7 -6 0 1710.19 58.31
7 6 0 1701.3 58.28
-7 -6 0 1690.89 58.41
-7 6 0 1770.84 58.13
-8 -6 0 212.34 9.08
-8 6 0 202.88 8.72
8 -6 0 208.36 8.25
-8 -6 0 184.07 9.04
8 6 0 196.3 8.6
-9 -6 0 38.78 6.46
-9 -6 0 41.54 6.53
9 6 0 29.21 5.64
9 -6 0 35.8 6.73
-9 6 0 43.42 5.96
-1 7 0 156.29 6.44
-1 -7 0 162.03 6.65
-3 7 0 7.69 3.2
-3 -7 0 7.87 3.29
-3 -7 0 6.23 2.19
-4 7 0 104.41 5.4
4 7 0 99.23 4.23
-4 -7 0 96.76 5.36
-4 -7 0 104.35 4.64
5 7 0 635.76 21.96
-5 -7 0 680.08 22.46
-5 -7 0 623.96 22.17
-5 7 0 614.19 22.39
-6 -7 0 119.37 6.02
6 7 0 122.25 5.65
-6 -7 0 135.58 6.4
-7 -7 0 130.49 6.62
-7 -7 0 118.71 6.98
7 7 0 129.48 6.22
-8 -7 0 281.72 12.08
-8 -7 0 305.83 12.01
8 7 0 292.56 11.58
-9 -7 0 400.67 16.12
9 -7 0 400.99 15.69
-9 -7 0 402.57 16.07
9 7 0 416.64 15.47
0 8 0 187.42 7.43
0 -8 0 182.89 7.69
-2 8 0 120.81 5.85
-2 -8 0 125.25 5.94
2 -8 0 121.88 5.71
-3 -8 0 423.94 14.7
-3 -8 0 408.61 15.19
-3 8 0 423.68 15.18
-4 -8 0 87.01 5.47
-4 8 0 87.75 5.58
-4 -8 0 92.04 4.51
-5 -8 0 56.07 4.05
5 8 0 57.22 3.47
-5 -8 0 55.55 5.01
-6 -8 0 815.55 28.5
-6 -8 0 857.59 28.78
6 8 0 791.57 28.17
-7 -8 0 35.72 5.87
7 8 0 35.99 4.27
-7 -8 0 42.93 5.09
8 8 0 118.57 6.64
-8 -8 0 117.32 8.16
-8 -8 0 125.39 7.66
-9 -8 0 666.54 24.25
-9 -8 0 643.07 24.21
1 -9 0 21.93 4.43
-1 -9 0 21.37 4.39
-2 -9 0 1680.69 55.48
-2 -9 0 1631.48 55.86
2 -9 0 1616.27 55.66
-2 9 0 1639.2 55.71
-3 9 0 25.22 4.43
-3 -9 0 22.23 2.94
-3 -9 0 18.89 4.48
-4 -9 0 945.91 33.3
-4 -9 0 975.65 32.93
-5 -9 0 100.94 5.55
-5 -9 0 107.88 6.67
-6 -9 0 649 22.21
-6 -9 0 603.6 22.58
7 9 0 47.66 4.7
-7 -9 0 54.3 6.8
-7 -9 0 48.11 5.78
-8 -9 0 768.88 27.54
-8 -9 0 755.16 27.29
0 -10 0 6141.73 206.14
-1 -10 0 136.88 7.34
-1 -10 0 140.37 5.55
1 -10 0 134.97 7.58
-2 -10 0 590.03 20.34
-2 -10 0 521.76 19.42
2 -10 0 569.71 20.05
-3 -10 0 341.21 12.25
-3 -10 0 334.51 13.32
-4 -10 0 169.14 8.66
-4 -10 0 176.58 7.4
-6 -10 0 1408.78 48.37
-6 -10 0 1414.96 48.67
-2 -11 0 24.43 6.33
-2 -11 0 35.02 3.58
-3 -11 0 48.58 6.65
-3 -11 0 46.39 4.18
-4 -11 0 1035.05 34.46
-4 -11 0 965.18 35.12
-5 -11 0 361.32 13.8
-5 -11 0 369.44 15.16
-7 -11 0 87.85 7.7
-7 -11 0 83.61 9.73
0 -12 0 1823.93 62.62
-2 -12 0 496.19 18.63
-2 -12 0 560.81 20.5
-4 -12 0 137.3 9.92
-4 -12 0 142.25 7.24
-5 -12 0 56.75 6.13
-5 -12 0 60.04 9.23
-6 -12 0 907.17 33.03
-1 -13 0 16.67 4.23
-2 -13 0 938.49 31.46
-2 -13 0 883.06 33.37
-3 -13 0 24.49 9.87
-3 -13 0 31.59 5.26
-4 -13 0 583.92 23.38
-4 -13 0 590.68 21.24
0 -14 0 479.69 21.45
-1 -14 0 11.47 5.14
-2 -14 0 449.22 20.55
2 0 -1 2746.08 97.71
-2 0 -1 3089.9 97.8
-2 0 1 2922.61 98
2 0 1 2703.03 97.32
-2 0 1 2954.9 98.05
-3 0 1 1024.68 33.8
-3 0 1 1011.62 33.78
-3 0 -1 998.74 33.74
3 0 -1 974.81 33.78
3 0 1 986.61 33.76
-4 0 -1 103.41 3.82
4 0 1 106.62 4
-4 0 1 103.68 3.83
4 0 -1 97.82 4.02
-4 0 1 99.34 4.04
-5 0 -1 77.96 3.19
-5 0 1 80.17 3.14
5 0 1 78.58 3.57
5 0 -1 73.32 3.6
-5 0 1 79 3.55
7 0 -1 997.59 35.37
-7 0 -1 1083.23 35.07
-7 0 1 1008.1 35.15
7 0 1 1043.59 35.38
8 0 1 1062.55 35.82
8 0 -1 1059.4 35.84
-8 0 1 1004.77 35.5
-8 0 -1 1028.54 35.31
9 0 -1 19.18 5.72
-9 0 1 24.22 4.85
9 0 1 22.49 5.55
-10 0 1 40.5 6.26
10 0 1 31.66 7.21
10 0 -1 40.26 7.33
-11 0 1 218.65 11.16
-1 -1 -1 5776.67 196.17
-2 -1 1 4468.79 150.96
-3 1 1 1225.69 42.79
3 1 1 1311.7 42.84
4 1 1 1183.95 39.01
-4 1 -1 1181.01 38.94
-4 -1 1 1153 38.96
4 -1 1 1124.5 38.92
4 1 -1 1137.48 39.01
4 -1 -1 1212.79 38.97
-4 -1 1 1076.87 38.9
5 1 1 56.21 3.17
5 1 -1 61.85 3.24
5 -1 -1 62.17 3
-5 -1 1 53.7 3.08
5 -1 1 59.47 2.93
-5 -1 -1 61.09 2.81
-5 1 1 60.42 3.06
-5 1 -1 59.24 2.47
-5 -1 1 61.02 2.92
6 1 1 387.59 14.28
-6 -1 1 393.61 14.23
-6 1 1 389.17 14.15
6 -1 -1 415.3 14.28
6 1 -1 423.62 14.38
-6 -1 1 405.22 14.09
-6 -1 -1 408.77 14.08
6 -1 1 415.63 14.24
-7 -1 -1 920.26 30.35
7 -1 -1 874.34 30.58
-7 1 1 885.27 30.36
7 -1 1 904.59 30.56
-7 -1 1 866.21 30.4
7 1 1 881.81 30.59
7 1 -1 880.7 30.61
-7 -1 1 900.74 30.32
8 -1 1 161.32 7.71
8 -1 -1 170.05 7.84
-8 -1 -1 174.99 7.04
-8 -1 1 173.25 6.93
8 1 1 177.71 7.71
-8 1 1 173.93 7.51
8 1 -1 174.71 7.7
-8 -1 1 167.01 7.4
9 1 1 125.86 7.46
-9 -1 -1 135.36 6.49
9 -1 -1 140.7 7.68
9 1 -1 128.65 7.76
9 -1 1 127.72 7.82
-9 -1 1 128.68 6.95
-9 -1 1 135.8 6.23
-9 1 1 132.42 6.94
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4 -7 11 153.24 8.11
4 -7 11 156.13 8.67
4 -7 -11 154.98 6.78
-5 -7 11 72.74 9.92
-5 -7 -11 72.58 6.4
0 -8 -11 12.3 3.86
1 -8 11 146.73 8.07
-1 -8 11 168.84 8.67
1 8 -11 153.53 10.8
-1 -8 -11 161.02 6.88
-1 8 -11 146.23 12.16
2 8 -11 231.41 12.9
-2 -8 -11 227.04 9.21
-2 8 -11 219.51 14.14
-2 -8 11 219.87 10.7
2 -8 -11 232.91 8.82
2 -8 11 241.83 11.51
3 8 -11 83.96 10.02
-3 -8 -11 84.72 5.78
-3 -8 11 98.15 8.34
3 -8 -11 88.6 4.88
3 -8 11 93.6 6.57
-4 -8 -11 42.6 5.43
4 -8 11 46.92 6.09
-4 -8 11 52.32 8.56
0 -9 11 715.27 24.88
0 -9 -11 663.5 23.96
-1 -9 11 144.58 8.69
1 -9 -11 140.35 6.62
1 -9 11 140.24 8.12
2 -9 11 148.7 9.34
-2 -9 11 147.51 9.22
0 0 12 680.91 23.32
0 0 12 672.85 24.3
1 0 12 379 14.76
-1 0 12 385.09 14.7
1 0 12 344.29 13.5
-1 0 12 400.65 13.5
1 0 -12 387.38 15.2
2 0 12 175.14 7.04
-2 0 12 169.87 8.91
2 0 -12 166.85 8.16
2 0 12 169.92 8.91
-2 0 12 177.72 6.68
2 0 -12 155.53 9.4
3 0 12 444.55 16.41
3 0 -12 460.94 17.4
3 0 -12 479.99 17.95
-4 0 12 121.83 7.78
4 0 -12 114.74 7.93
4 0 12 118.6 6.34
4 0 -12 113.49 8.75
4 0 12 115.64 8.07
5 0 -12 22.35 7.74
5 0 12 30.72 5.28
5 0 -12 26.28 7.69
5 0 12 27.19 7.23
6 0 12 182.81 8.92
0 -1 12 1100.17 37.72
0 1 12 1096.41 36.79
0 1 12 1069.82 37.59
0 -1 12 1063.73 36.89
1 1 -12 291.75 12.7
1 -1 12 238.11 11.73
-1 -1 12 302.31 10.57
1 1 12 290.89 10.64
-1 1 12 291.36 11.83
-1 -1 12 299.14 12.03
1 -1 12 279.73 10.64
-1 1 12 294.78 10.44
1 1 12 297.43 12.09
-2 1 12 452.15 15.37
-2 -1 12 446.86 16.8
2 1 12 445.12 15.74
2 1 -12 449.17 17.21
-2 1 12 453.6 16.46
2 -1 12 448.23 15.68
2 -1 12 445.99 16.84
2 -1 -12 405.95 16.47
2 -1 -12 420.87 17.09
2 1 12 432.56 16.91
-2 -1 12 435.65 15.57
3 -1 12 150.42 8.27
3 1 -12 143.26 9.14
-3 -1 12 153.7 6.32
3 1 12 146.28 9
3 -1 -12 149.2 8.33
3 1 -12 126.15 7.84
3 -1 12 163.24 6.72
-3 -1 12 143.94 8.66
3 -1 -12 154.96 8.99
3 1 12 149.87 6.79
4 -1 12 263.61 11.84
4 -1 -12 262.42 12.36
4 1 -12 277.44 11.76
-4 -1 12 278.42 12.57
4 -1 12 263.5 10.6
-4 -1 12 282.81 10.15
4 1 12 283.79 12.47
4 -1 -12 263.24 13.21
4 1 -12 285.81 12.6
4 1 12 266.57 10.55
5 -1 12 312.55 12.01
-5 -1 12 314.45 13.63
5 1 12 291.76 11.94
5 -1 -12 310.53 14.11
5 1 -12 308.24 13.78
5 -1 12 308.26 13.34
5 -1 -12 319.82 13.81
5 1 -12 308.94 13.77
6 1 12 44.28 8.72
6 1 12 45.44 5.71
6 -1 12 38.28 6.52
0 -2 12 61.68 4.02
0 2 -12 61.92 7.16
0 -2 12 57.38 6.09
0 2 12 58.86 5.79
0 2 12 56.7 3.74
1 -2 12 365.67 13.35
1 2 12 370.43 14.46
1 2 12 379.15 13.13
-1 2 12 346.52 12.92
-1 -2 12 360.66 14.44
-1 2 12 390.79 14.06
1 2 -12 363.16 14.96
-1 -2 12 361.74 13.2
1 -2 12 365.46 14.38
2 2 -12 51.93 7.42
2 -2 12 49.53 4.15
-2 -2 12 45.54 6.52
2 -2 -12 46.43 6.15
2 2 12 48.69 6.66
2 2 12 44.89 3.87
-2 -2 12 47.81 3.75
2 -2 12 51.99 6.23
2 -2 -12 39.09 7.04
3 -2 12 378.91 14.68
3 2 -12 399.09 14.37
3 2 12 391.69 15.39
3 2 12 337.64 13.53
3 2 -12 387.95 15.49
3 -2 12 359.22 13.7
3 -2 -12 357.43 15.11
-3 -2 12 374.47 15.16
3 -2 -12 383.72 15.25
-3 -2 12 373.77 13.41
-4 -2 12 236.1 8.82
4 -2 -12 241.07 11.34
4 2 -12 224.78 10.29
4 -2 -12 224.54 12.07
-4 -2 -12 228.65 9.61
-4 -2 12 231.79 11.67
4 2 12 233.34 9.18
4 -2 12 216.14 9.35
4 2 -12 235.55 11.45
4 2 12 233.91 11.55
4 -2 12 227.8 10.61
5 2 12 43.99 5.22
5 -2 12 51.14 6.91
5 -2 -12 50.7 8.04
5 2 -12 39.45 8.04
5 2 12 61.42 8.68
5 2 -12 45.27 9.95
-5 -2 12 49.42 8.84
-5 -2 -12 49.78 5.66
5 -2 -12 46.26 9.05
-5 -2 12 33.7 3.9
5 -2 12 43.95 5.33
-6 -2 -12 14.34 6.26
0 -3 12 2325.99 76.56
0 3 -12 2172.12 76.54
0 -3 12 2249.72 75.98
1 3 -12 109.75 8.78
1 -3 12 120.5 5.85
-1 -3 12 127.21 7.68
-1 -3 -12 125.55 5.78
1 3 12 123.09 5.59
1 3 12 124.02 7.48
-1 -3 12 131.07 5.68
1 -3 12 119 7.41
-2 -3 12 165.34 7.03
2 -3 12 162.76 7.39
2 3 -12 167.4 9.99
2 3 12 185.68 9.13
-2 -3 12 163.89 9.04
-2 -3 -12 169.2 7.35
2 -3 -12 173.05 9.11
2 3 12 184.92 7.23
2 -3 12 173.27 8.96
3 -3 -12 114.54 8.79
3 3 -12 110.93 6.67
-3 -3 12 115.12 5.4
3 3 -12 115.75 8.94
-3 -3 -12 116.6 6.11
-3 -3 12 115.5 8.24
3 -3 12 120.16 7.38
3 3 12 123.86 8.69
3 3 12 114.02 5.9
3 -3 -12 102.68 8.61
3 -3 12 110.74 6.01
-4 -3 -12 160.06 7.49
4 -3 -12 156.57 9.62
4 -3 12 152.6 7.44
4 3 12 172.07 10.89
4 -3 -12 136.84 10.22
-4 -3 12 153.49 10.27
4 -3 12 153.78 8.49
-4 -3 12 155.36 6.6
4 3 12 155.89 7.28
4 3 -12 152.22 10
4 3 -12 146.2 8.17
5 -3 12 341.04 14.03
5 -3 -12 307.59 14.73
-5 -3 -12 353.14 13.47
-5 -3 12 328.93 12.5
5 3 -12 350.09 14.97
-5 -3 12 348.71 15.97
5 3 -12 347.19 14.04
5 3 12 346.99 15.7
5 3 12 337.77 13.15
5 -3 12 353.22 13.31
5 -3 -12 362.5 16.03
-6 -3 -12 673.56 25.41
6 3 12 736.13 27.42
0 4 -12 481.37 19.39
0 -4 -12 512.11 17.66
0 -4 12 468.35 17.72
0 -4 12 536.15 18.64
-1 -4 12 684.48 24.24
1 -4 12 679.06 24.07
1 4 -12 705.48 24.89
-1 -4 12 616.39 23.29
1 -4 12 704.76 23.44
-1 4 -12 624.12 24.59
-1 -4 -12 675.28 23.34
-2 -4 -12 715.9 26.75
2 4 -12 765.07 28.17
2 4 12 807.88 27.35
-2 -4 12 777.95 26.75
2 -4 12 777.88 27.5
2 -4 12 812.56 26.94
-2 -4 12 747.93 27.68
2 -4 -12 774.97 27.92
3 -4 12 53.97 4.84
3 -4 -12 42.8 8.21
3 4 12 53.01 7.51
3 -4 12 55.16 6.14
3 -4 -12 46.63 7.84
-3 -4 -12 40.12 4.65
3 4 12 29.84 4.51
3 4 -12 41.35 8.03
-3 -4 12 18.7 7.07
-3 -4 12 45.51 3.99
4 4 -12 173.49 10.63
-4 -4 -12 175.12 7.91
4 -4 -12 176.03 10.27
4 4 -12 162.76 8.6
4 -4 12 178.38 9.03
-4 -4 12 174.99 7.39
-4 -4 12 180.55 10.68
4 -4 -12 164.1 11.38
4 4 12 186.34 11.19
4 -4 12 165.83 8.18
5 -4 12 907.31 31.11
5 4 12 925.35 32.3
5 -4 12 918.55 30.83
5 4 -12 805.52 31.58
-5 -4 12 916.19 32.48
5 -4 -12 853.3 31.46
5 4 -12 814.87 30.92
0 -5 12 257.28 10.95
0 -5 -12 249.4 9.61
0 -5 12 231.35 9.91
0 5 -12 261.46 12.65
-1 -5 12 184.96 9.57
-1 -5 -12 201.5 7.81
1 -5 12 191.37 9.2
1 5 -12 193.91 11.2
-1 -5 12 194.7 8.02
1 -5 12 173.81 8.13
1 -5 -12 189.6 7.72
-1 5 -12 187.24 11.25
-2 5 -12 267.07 13.45
2 -5 12 291.17 11.48
-2 -5 12 300.87 11.19
-2 -5 12 312.01 12.82
-2 -5 -12 286.04 11.1
2 5 -12 297.35 13.77
2 -5 12 309.98 12.48
2 -5 -12 284.4 13.5
3 -5 12 39.11 5.06
3 -5 12 44.7 6.11
3 5 -12 41.54 8.29
3 -5 -12 36.18 8.92
-3 -5 12 37.86 7.74
3 -5 -12 40.02 7.88
-3 -5 -12 40.19 4.44
4 -5 -12 89.97 9.16
4 5 -12 85.61 9.22
4 5 -12 96.61 6.59
-4 -5 12 89.82 9.23
4 -5 -12 80.41 10.83
4 -5 12 92.04 7.17
4 -5 12 94 6.6
4 5 12 92.28 9.56
-4 -5 -12 94.62 5.92
5 -5 12 22.07 6.47
-5 -5 -12 13.33 5.49
-5 -5 12 24.27 10.44
0 6 -12 65.91 9.84
0 -6 12 53.34 6.49
0 -6 -12 56.14 4.23
0 -6 12 62.74 4.99
-1 -6 12 234.16 11.08
-1 6 -12 255.49 13.27
1 -6 12 230.92 9.97
1 -6 12 236.2 10.73
1 6 -12 238.67 13.01
1 -6 -12 244.37 9.38
-1 -6 -12 238.09 9.34
-2 -6 -12 1320.56 44.35
2 -6 -12 1382.3 44.25
2 -6 12 1191.6 44.59
-2 -6 12 1304.43 45.2
-2 6 -12 1299.06 45.71
2 6 -12 1252.44 45.6
2 -6 -12 1312.14 45.77
2 -6 12 1330.82 44.97
3 -6 -12 81.2 10.72
3 6 -12 88.27 9.37
-3 -6 12 87.93 8.48
3 -6 12 93.36 6.97
3 -6 12 84.71 6.62
-3 -6 -12 74.17 5.39
4 -6 12 709.3 24.58
4 -6 -12 687.43 25.6
-4 -6 12 645.73 25.59
-4 -6 -12 670.19 23.97
0 -7 12 1084.01 38.44
0 -7 -12 1092.95 37.67
0 7 -12 1128.91 39.85
1 -7 12 53.62 6.57
1 7 -12 45.71 9.93
-1 -7 -12 41.7 4.37
1 -7 -12 48.78 4.13
-1 7 -12 47.38 11.02
-1 -7 12 55.5 7.22
1 -7 12 50.38 5.85
-2 -7 12 120.02 8.73
2 -7 -12 121.83 5.96
2 7 -12 109.31 10.57
-2 -7 -12 112.78 6.1
2 -7 12 114.82 7.56
2 -7 12 121.9 8.42
-3 -7 12 381.37 16.09
3 -7 12 382.52 14.96
-3 -7 -12 363.73 14.02
0 -8 12 191.91 10.05
1 -8 12 186.57 9.9
-1 -8 12 192.53 10.37
-2 -8 12 181.39 10.61
-1 0 13 59.48 4.11
-1 0 13 53.85 7.32
1 0 13 53.32 7.62
1 0 13 60.53 4.31
1 0 -13 66.58 8.42
-2 0 13 18.81 7.77
2 0 -13 20.17 7.9
-2 0 13 18.83 3.4
2 0 13 17.45 4.01
4 0 -13 190.67 11.03
4 0 13 126.78 10.38
-4 0 13 173.38 9.96
4 0 -13 170.91 9.94
0 1 13 171.01 7.28
0 -1 13 172.48 7.21
0 -1 13 172.86 9.91
0 1 13 171.81 9.73
1 1 13 14.31 4.17
1 1 13 24.41 7.62
-1 -1 13 20.51 7.08
1 -1 13 18.31 3.72
1 -1 13 16.92 7.04
1 1 -13 17.64 8.19
-1 -1 13 14.72 3.66
-1 1 13 18.27 3.68
2 1 -13 408.23 17.6
-2 1 13 429.52 16.85
2 -1 -13 419.97 17.65
-2 -1 13 440.69 15.41
2 -1 13 433.9 15.56
-2 -1 13 445.29 17.32
2 1 13 433.4 17.53
2 1 13 448.25 15.71
3 -1 -13 146.14 10.11
3 1 13 140.49 10.36
-3 -1 13 156.02 6.59
3 1 -13 153.84 10.28
-3 -1 13 163.78 10.32
3 1 -13 142.22 8.42
3 -1 13 160.2 7.04
3 -1 -13 153.7 9.21
3 -1 13 151.79 10.18
3 1 13 132.51 6.97
4 -1 13 51.91 8.26
4 1 13 44.43 5.19
-4 -1 13 59.56 9.6
4 -1 13 45.41 5.42
4 1 -13 45.38 9.01
4 -1 -13 42.55 8.67
4 1 -13 40.08 7.42
4 1 13 58.21 11.42
4 -1 -13 46.22 8.36
-5 -1 13 26.98 9.48
5 1 13 38.14 10.03
5 -1 13 24.45 8.88
0 2 -13 303.26 14.42
0 -2 13 317.64 11.88
0 2 13 332.41 13.34
0 -2 13 316.84 13.74
1 2 13 194.95 10.03
1 2 13 177.54 7.31
1 2 -13 161.67 10.69
-1 -2 13 184.68 10.06
1 -2 13 185.42 7.62
1 -2 13 157.34 9.75
-1 -2 13 174.9 7.47
-2 -2 13 130 6.23
2 -2 13 131.89 6.56
2 -2 13 124.25 8.92
2 2 13 128.06 6.23
2 -2 -13 127.87 9.61
-2 -2 13 131.83 9.4
2 -2 -13 141.71 8.7
2 2 13 139.54 9.37
2 2 -13 140.76 9.88
-3 -2 13 10.8 3.85
3 2 13 13.47 4.12
3 -2 -13 22.64 8.18
3 -2 13 13.77 4.55
3 2 -13 26.39 5.87
4 2 -13 235.26 10.84
4 2 13 239.32 13.59
4 -2 -13 220.58 12.42
4 -2 13 223.79 9.6
4 2 -13 219.44 12.33
4 2 13 209.64 9.36
-4 -2 13 222.53 13.2
4 -2 -13 208.74 12.11
4 -2 13 248.97 11.58
5 -2 13 224.89 12.05
5 2 13 222.9 13.93
0 -3 13 184.96 9.94
0 -3 13 173.61 7.57
0 3 -13 171.26 11.15
1 3 -13 336.84 15.08
-1 3 -13 315.08 14.75
1 -3 13 325.41 13.79
2 -3 -13 25.8 7.53
2 -3 13 30.26 7.16
2 3 13 27.17 8.36
-2 -3 13 23.68 8.07
2 3 -13 34.21 8.98
-2 -3 13 33.07 3.95
2 -3 13 30.38 4.57
3 3 -13 94.58 9.81
3 -3 13 99.34 9.94
3 -3 -13 85.86 9.52
-3 -3 13 89.46 5.23
3 3 13 100.59 10
-3 -3 13 92.64 9.64
3 -3 13 94.45 6.05
3 -3 -13 89.44 9.78
-3 -3 -13 90.39 6.03
4 3 -13 356.99 16.33
4 3 13 388.45 17.15
-4 -3 13 381.14 17.28
4 3 -13 357.03 14.62
4 -3 -13 333.4 16
4 -3 13 360.09 15.24
-4 -3 -13 359.8 14.15
4 -3 13 370.77 13.99
0 4 -13 82.29 10.16
0 -4 13 74.61 7.82
0 -4 13 67.14 5.11
1 4 -13 259.06 13.19
1 -4 13 245.06 9.87
-1 -4 13 228.57 9.63
-1 -4 13 239.84 11.84
-1 4 -13 243.02 13.22
-1 -4 -13 232.02 9.69
1 -4 13 253.51 11.55
2 4 -13 657.67 24.77
-2 -4 13 647.97 24.15
2 -4 13 619.82 22.75
-2 -4 13 643.61 22.55
-2 -4 -13 649.91 22.7
2 -4 13 621.44 23.72
2 -4 -13 659.67 24.4
3 -4 13 76.79 6.2
-3 -4 13 80.46 5.14
3 -4 13 85.12 10.48
3 4 -13 67.44 9.99
3 4 13 77.41 9.7
3 -4 -13 93.3 9.89
-3 -4 13 76.03 9.66
-3 -4 -13 77.35 6.03
-4 -4 13 407.44 18.43
4 -4 13 435.33 16.59
-4 -4 -13 385.11 15.52
0 -5 13 666.42 24.1
0 -5 13 643.98 23.04
0 5 -13 645.19 25.42
0 -5 -13 649.97 22.83
-1 5 -13 368.67 17.46
-1 -5 13 328.27 13.75
-1 -5 13 371.74 15.48
1 -5 13 384.69 15.22
1 -5 13 377.93 14.03
1 5 -13 382.32 17.11
-1 -5 -13 375.24 13.79
2 5 -13 466.18 20.03
2 -5 13 498.82 18.71
-2 -5 13 469.61 17.37
2 -5 13 481.28 17.6
-2 -5 -13 465 17.44
-2 -5 13 499.13 19.22
-3 -5 -13 114.01 7.13
-3 -5 13 132.75 10.69
3 -5 13 135.32 12.59
0 -6 13 61.52 7.92
0 -6 -13 56.74 5.01
-2 -6 13 112.16 9.89
2 -6 13 114.73 8.93
-2 -6 -13 105.27 6.26
0 0 14 262.97 10.7
0 0 14 298.9 14.24
1 0 -14 154.28 11.83
1 0 14 171.64 11.58
1 0 14 163.42 7.31
-1 0 14 144.82 11.14
2 0 14 81.74 10.29
-2 0 14 85.17 10.46
2 0 -14 89.6 10.32
2 0 14 67.83 5.51
3 0 14 27.46 10.65
-3 0 14 35.16 10.39
0 1 -14 307.73 15.33
0 1 14 330.89 14.62
0 -1 14 306.58 11.67
0 -1 14 293.1 14.76
1 1 14 255.97 11.82
-1 -1 14 322.1 14.87
1 -1 14 324.01 11.84
-1 1 14 334.29 14.86
1 1 -14 296.9 15.44
1 -1 -14 308.73 15.21
1 -1 14 345.97 15.02
-1 -1 14 290.07 11.6
1 1 14 329.86 15.02
2 -1 -14 231.07 13.71
2 -1 14 239.5 13.25
2 1 -14 231.76 13.69
2 1 14 257.99 13.46
-2 -1 14 248.01 13.79
-3 -1 14 180.24 13.24
3 1 14 168.15 13.17
0 -2 14 250.99 13.23
0 2 14 249.15 12.62
0 2 -14 250.47 14.39
1 2 -14 464.94 20.49
1 -2 14 492.59 19.69
-1 -2 14 503.59 20.06
2 -2 14 515.93 18.27
2 2 14 524.69 21.24
-2 -2 14 480.6 20.7
2 -2 14 496.68 20.42
3 -2 14 205.77 13
1 -3 14 70.39 5.65
1 3 14 74.15 8.9
-1 -3 14 60.6 9.89
1 -3 14 63.6 9.23
2 -3 14 31.77 9.08
2 3 14 24.69 10.1
-2 -3 14 21.57 10.24
0 -4 14 126.5 10.75
-1 -4 14 38.72 9.65
1 -4 14 22.03 8.86
-2 -4 14 140.1 11.96
_iucr_refine_fcf_details
;
data_GlyAla_12K_NoSpherA2_ORCA_NoSpherA2_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 x+1/2,-y+1/2,-z
3 -x,y+1/2,-z+1/2
4 -x+1/2,-y,z+1/2
_space_group_crystal_system orthorhombic
_space_group_IT_number 19
_space_group_name_H-M_alt 'P 21 21 21'
_space_group_name_Hall ' P 2ac 2ab'
_symmetry_space_group_name_H-M 'P 21 21 21'
_symmetry_space_group_name_Hall ' P 2ac 2ab'
_symmetry_Int_Tables_number 19
_cell_length_a 7.4583
_cell_length_b 9.4892
_cell_length_c 9.7301
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 688.63129
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
-11 -2 -1 69.990 73.362 3.674 10.670 o
-11 -1 -3 20.876 21.326 2.306 27.091 o
-11 -1 -2 32.086 29.165 2.718 19.491 o
-11 -1 -1 12.161 11.288 2.339 26.324 o
-10 -6 -3 114.432 115.499 4.745 6.397 o
-10 -6 -1 12.787 11.330 1.380 75.594 o
-10 -5 -4 383.689 374.948 13.281 0.816 o
-10 -5 -3 90.309 81.867 3.938 9.288 o
-10 -5 -2 5.732 5.732 1.221 96.555 o
-10 -5 -1 44.826 44.614 1.604 55.979 o
-10 -4 -5 19.127 18.757 2.682 20.024 o
-10 -4 -3 57.811 55.352 1.555 59.531 o
-10 -4 -1 18.938 18.669 0.997 144.804 o
-10 -3 -6 13.669 12.762 2.573 21.761 o
-10 -3 -5 26.996 26.547 1.539 60.769 o
-10 -3 -4 68.338 68.609 2.557 22.030 o
-10 -3 -3 4.583 5.205 1.474 66.317 o
-10 -3 -2 65.239 66.306 1.632 54.077 o
-10 -3 -1 271.553 264.236 4.180 8.244 o
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6 8 3 46.163 46.966 1.398 73.678 o
6 8 4 536.530 531.790 10.454 1.318 o
6 8 5 146.012 148.311 3.283 13.358 o
6 8 6 68.650 66.236 2.629 20.836 o
6 8 7 13.584 13.936 1.426 70.794 o
6 8 8 102.268 96.280 2.688 19.928 o
6 8 9 19.563 18.634 1.907 39.581 o
6 9 0 194.028 190.359 6.886 3.037 o
6 9 1 77.623 77.247 1.942 38.185 o
6 9 2 48.423 48.513 1.497 64.229 o
6 9 3 24.433 26.874 1.258 90.928 o
6 9 4 66.809 68.015 1.880 40.743 o
6 9 5 118.152 119.326 2.849 17.736 o
6 9 6 18.295 16.340 1.641 53.476 o
6 9 7 124.815 121.141 4.714 6.480 o
6 9 8 25.768 25.089 1.931 38.602 o
6 10 0 416.135 428.306 10.408 1.329 o
6 10 1 57.340 56.751 1.716 48.933 o
6 10 2 32.024 29.313 1.378 75.784 o
6 10 3 225.550 228.121 4.802 6.244 o
6 10 4 6.256 6.500 1.464 67.159 o
6 10 5 108.922 94.710 4.802 6.245 o
6 10 7 80.573 80.862 3.002 15.977 o
6 11 1 9.027 11.109 1.459 67.680 o
6 11 2 20.638 21.230 1.425 70.914 o
6 11 3 8.080 7.282 1.565 58.831 o
6 11 4 111.154 111.102 4.813 6.217 o
6 11 5 15.389 13.010 1.889 40.340 o
6 12 0 279.037 275.202 10.020 1.434 o
6 12 1 45.012 44.198 2.063 33.847 o
6 12 2 46.092 41.565 2.111 32.330 o
7 0 1 305.359 313.786 5.346 5.040 o
7 0 2 92.217 96.441 1.563 58.947 o
7 0 3 371.680 385.344 6.561 3.346 o
7 0 4 36.241 36.581 0.882 185.302 o
7 0 5 11.184 12.574 0.625 368.812 o
7 0 6 524.505 518.870 8.814 1.854 o
7 0 7 29.302 30.228 0.821 213.506 o
7 0 8 24.663 24.421 0.896 179.536 o
7 0 9 98.472 97.295 2.276 27.796 o
7 0 10 56.794 54.317 1.652 52.775 o
7 0 11 217.315 205.865 7.390 2.637 o
7 1 1 265.643 267.264 4.622 6.741 o
7 1 2 378.306 388.828 6.523 3.384 o
7 1 3 124.967 129.993 2.064 33.804 o
7 1 4 7.129 6.857 0.475 639.438 o
7 1 5 3.937 3.986 0.679 312.592 o
7 1 6 83.778 84.951 1.669 51.678 o
7 1 7 92.493 94.901 1.635 53.852 o
7 1 8 31.777 32.957 0.815 216.852 o
7 1 9 24.897 25.463 1.174 104.429 o
7 1 10 15.903 15.398 1.179 103.566 o
7 1 11 33.699 31.425 2.166 30.695 o
7 2 0 2.570 3.648 0.610 387.579 o
7 2 1 68.212 69.181 1.903 39.785 o
7 2 2 99.287 99.930 1.833 42.882 o
7 2 3 68.013 67.735 1.357 78.147 o
7 2 4 145.506 145.371 3.468 11.974 o
7 2 5 66.327 69.069 1.412 72.184 o
7 2 6 99.378 103.432 1.963 37.367 o
7 2 7 25.282 25.441 0.824 211.882 o
7 2 8 43.760 44.176 1.082 123.105 o
7 2 9 27.518 28.009 1.092 120.835 o
7 2 10 152.785 142.797 3.219 13.900 o
7 2 11 65.826 61.834 3.510 11.690 o
7 3 0 28.828 28.844 0.745 259.738 o
7 3 1 97.655 99.219 1.828 43.112 o
7 3 2 269.632 277.674 9.629 1.553 o
7 3 3 67.582 68.898 1.353 78.674 o
7 3 4 231.674 234.735 4.030 8.868 o
7 3 5 4.798 4.075 0.674 317.217 o
7 3 6 358.004 364.252 6.269 3.664 o
7 3 8 100.541 105.290 3.173 14.300 o
7 3 9 37.666 40.198 1.146 109.722 o
7 3 10 27.471 24.791 3.565 11.330 o
7 4 0 289.285 289.985 4.966 5.840 o
7 4 1 9.835 10.803 0.743 261.126 o
7 4 2 51.711 53.633 1.239 93.850 o
7 4 3 30.139 31.723 0.973 152.142 o
7 4 4 5.622 5.887 0.646 344.996 o
7 4 5 150.320 153.289 2.730 19.327 o
7 4 6 51.288 52.122 1.247 92.655 o
7 4 7 26.472 26.121 1.011 140.958 o
7 4 8 45.657 44.455 1.149 109.170 o
7 4 9 6.563 6.930 1.179 103.671 o
7 4 10 142.399 136.304 5.640 4.528 o
7 5 0 2.032 2.563 0.804 222.828 o
7 5 1 20.531 19.642 0.823 212.631 o
7 5 2 21.098 20.642 0.860 194.579 o
7 5 3 17.709 17.031 0.847 200.916 o
7 5 4 15.328 15.873 0.876 187.739 o
7 5 5 28.015 29.579 0.924 168.556 o
7 5 6 70.556 71.995 2.967 16.354 o
7 5 7 6.920 5.586 0.887 182.837 o
7 5 8 121.022 121.595 2.409 24.820 o
7 5 9 13.672 14.057 1.187 102.255 o
7 5 10 65.281 59.289 3.801 9.967 o
7 6 0 523.438 521.472 8.840 1.843 o
7 6 1 18.617 18.980 0.857 196.043 o
7 6 2 48.857 53.069 3.764 10.167 o
7 6 3 39.265 38.169 1.157 107.509 o
7 6 4 94.424 95.034 2.130 31.739 o
7 6 5 55.381 51.626 1.478 65.908 o
7 6 6 45.388 44.037 1.911 39.440 o
7 6 7 16.956 17.522 1.022 137.847 o
7 6 8 124.725 125.977 2.573 21.753 o
7 6 9 9.886 7.861 1.338 80.438 o
7 7 0 40.574 38.475 1.153 108.271 o
7 7 1 29.471 29.763 0.934 165.217 o
7 7 2 83.901 81.371 1.918 39.133 o
7 7 3 57.236 58.150 2.064 33.803 o
7 7 4 63.672 62.214 1.609 55.594 o
7 7 5 20.432 20.126 1.049 130.830 o
7 7 6 180.098 177.536 5.491 4.777 o
7 7 7 56.566 54.793 1.680 51.050 o
7 7 8 37.701 38.294 2.193 29.940 o
7 7 9 104.758 104.501 3.065 15.328 o
7 8 0 11.988 11.647 0.867 191.635 o
7 8 1 33.033 33.068 1.031 135.596 o
7 8 2 119.857 116.453 2.247 28.510 o
7 8 3 8.590 8.990 0.924 168.659 o
7 8 4 2.531 3.865 1.711 49.193 o
7 8 5 67.932 64.432 3.373 12.658 o
7 8 6 28.292 24.940 1.828 43.078 o
7 8 7 19.119 17.253 1.936 38.417 o
7 8 8 32.580 34.863 1.919 39.108 o
7 9 0 15.674 14.995 0.975 151.518 o
7 9 1 206.988 204.057 4.162 8.312 o
7 9 2 158.093 157.011 3.498 11.770 o
7 9 3 14.779 12.953 1.306 84.445 o
7 9 4 19.023 18.421 1.598 56.374 o
7 9 5 9.907 10.333 1.707 49.434 o
7 9 6 60.845 59.145 2.486 23.298 o
7 9 7 55.827 50.150 2.589 21.480 o
7 10 1 73.757 72.798 3.643 10.849 o
7 10 2 18.387 16.056 1.480 65.709 o
7 10 3 106.293 103.936 2.679 20.069 o
7 10 4 40.239 35.578 1.959 37.543 o
7 10 5 6.301 9.086 2.421 24.573 o
7 11 0 28.264 26.170 1.832 42.921 o
7 11 1 181.505 178.840 6.952 2.980 o
7 11 2 131.040 126.669 5.156 5.418 o
8 0 0 46.148 46.841 1.420 71.441 o
8 0 1 307.431 315.232 5.402 4.935 o
8 0 2 286.301 300.203 5.748 4.359 o
8 0 4 117.756 120.099 2.226 29.056 o
8 0 5 3.214 3.382 0.867 191.654 o
8 0 6 113.280 114.961 2.194 29.915 o
8 0 8 69.493 66.024 3.452 12.083 o
8 1 0 425.884 434.453 8.542 1.974 o
8 1 1 50.821 52.202 1.129 112.941 o
8 1 2 99.484 100.156 1.893 40.200 o
8 1 3 37.235 36.340 0.962 155.679 o
8 1 4 290.997 305.418 5.247 5.231 o
8 1 5 23.179 22.653 0.861 194.398 o
8 1 6 171.962 171.969 5.925 4.102 o
8 1 7 24.956 23.835 1.221 96.564 o
8 1 8 111.154 104.337 2.541 22.309 o
8 2 0 18.261 17.386 0.685 307.157 o
8 2 1 124.308 127.970 2.328 26.581 o
8 2 2 241.435 240.875 4.198 8.173 o
8 2 3 61.123 59.971 1.302 84.888 o
8 2 4 31.479 34.453 0.985 148.422 o
8 2 5 50.103 51.733 1.257 91.204 o
8 2 6 36.357 36.702 1.120 114.793 o
8 2 10 26.700 27.063 2.952 16.529 o
8 3 0 1.633 2.639 1.150 108.939 o
8 3 1 46.314 47.001 1.094 120.416 o
8 3 2 58.875 56.265 1.244 93.079 o
8 3 3 215.308 223.121 3.869 9.619 o
8 3 4 13.556 13.798 0.819 214.955 o
8 3 5 186.466 188.694 4.681 6.571 o
8 3 6 90.793 94.331 2.136 31.570 o
8 3 7 29.821 29.641 1.153 108.298 o
8 3 8 45.025 45.157 1.971 37.059 o
8 3 9 56.651 58.546 3.552 11.412 o
8 4 0 106.593 107.882 2.326 26.619 o
8 4 1 16.452 17.705 0.776 238.960 o
8 4 2 88.211 89.064 1.992 36.297 o
8 4 3 13.832 14.180 0.806 221.809 o
8 4 4 154.785 159.867 3.278 13.402 o
8 4 5 71.566 73.336 1.602 56.099 o
8 4 6 28.096 27.982 1.131 112.642 o
8 4 7 36.242 35.684 1.268 89.595 o
8 4 8 93.164 93.456 2.095 32.807 o
8 4 9 9.396 11.145 2.073 33.509 o
8 5 0 20.798 19.823 0.707 287.818 o
8 5 1 31.900 31.517 0.937 164.042 o
8 5 2 164.622 167.228 2.984 16.175 o
8 5 3 32.120 30.323 0.980 149.885 o
8 5 4 24.010 21.874 1.993 36.264 o
8 5 5 11.998 13.259 0.950 159.447 o
8 5 6 17.218 17.446 1.062 127.725 o
8 5 7 13.936 12.529 1.113 116.307 o
8 5 9 33.916 35.157 2.745 19.106 o
8 6 0 63.039 61.117 1.266 89.796 o
8 6 1 52.858 50.386 1.416 71.819 o
8 6 2 131.246 131.104 2.997 16.036 o
8 6 3 56.395 55.279 1.535 61.127 o
8 6 4 8.638 8.152 1.001 143.850 o
8 6 5 87.330 89.132 1.862 41.548 o
8 6 6 6.716 6.245 1.203 99.475 o
8 6 7 134.293 135.455 6.125 3.839 o
8 7 0 90.598 89.103 2.081 33.241 o
8 7 1 44.028 48.955 2.601 21.290 o
8 7 2 48.004 47.922 1.406 72.896 o
8 7 3 105.467 103.763 2.381 25.411 o
8 7 4 49.381 46.603 1.492 64.662 o
8 7 5 39.556 39.438 1.432 70.194 o
8 7 6 73.757 74.032 4.037 8.837 o
8 7 7 43.532 42.574 2.351 26.052 o
8 8 0 37.533 36.539 1.297 85.661 o
8 8 1 62.096 61.878 1.697 49.984 o
8 8 2 94.687 91.558 1.967 37.220 o
8 8 3 7.392 7.484 1.087 121.813 o
8 8 5 35.838 36.283 2.088 33.032 o
8 8 6 12.350 10.225 1.997 36.100 o
8 9 0 227.026 231.169 5.881 4.164 o
8 9 1 56.070 55.129 2.151 31.110 o
8 9 2 88.431 80.051 2.931 16.764 o
8 10 1 220.289 205.559 7.551 2.526 o
9 0 1 6.574 6.802 0.934 165.152 o
9 0 3 183.955 186.919 3.351 12.824 o
9 0 4 119.699 119.421 2.285 27.581 o
9 0 5 57.523 59.615 2.142 31.374 o
9 0 6 21.837 24.360 1.080 123.426 o
9 0 7 9.695 9.583 1.310 83.906 o
9 1 0 130.842 134.709 3.596 11.135 o
9 1 1 38.765 40.362 1.063 127.361 o
9 1 2 113.391 116.769 2.221 29.205 o
9 1 3 93.402 95.365 2.137 31.540 o
9 1 4 112.691 115.349 3.496 11.780 o
9 1 5 285.943 293.840 5.881 4.164 o
9 1 6 97.669 93.647 2.380 25.432 o
9 1 7 48.922 46.539 1.985 36.554 o
9 1 8 107.806 109.714 3.195 14.110 o
9 2 0 278.524 275.058 4.781 6.300 o
9 2 1 123.693 124.149 2.296 27.320 o
9 2 2 20.707 21.024 0.911 173.570 o
9 2 3 15.473 14.637 0.917 171.311 o
9 2 4 113.611 115.054 2.242 28.648 o
9 2 6 24.014 24.417 1.297 85.612 o
9 2 7 96.692 95.928 2.098 32.727 o
9 2 8 132.235 131.119 3.788 10.039 o
9 3 0 176.084 170.745 3.083 15.152 o
9 3 1 31.159 32.189 1.036 134.289 o
9 3 2 80.709 79.750 1.683 50.848 o
9 3 3 12.264 12.728 0.917 171.442 o
9 3 4 61.185 60.962 1.501 63.896 o
9 3 5 13.053 14.405 1.088 121.545 o
9 3 7 11.922 11.488 1.248 92.491 o
9 3 8 50.231 51.482 2.483 23.363 o
9 4 0 97.230 95.584 1.918 39.155 o
9 4 1 150.264 152.001 2.812 18.216 o
9 4 2 73.954 77.710 1.934 38.503 o
9 4 3 34.930 36.517 1.192 101.334 o
9 4 4 10.076 10.310 1.027 136.512 o
9 4 5 56.370 56.687 2.329 26.559 o
9 4 6 24.668 25.144 1.297 85.603 o
9 4 7 110.304 108.918 2.659 20.369 o
9 5 0 6.519 8.099 1.124 114.005 o
9 5 1 18.761 18.786 1.003 143.283 o
9 5 3 64.203 61.860 1.523 62.060 o
9 5 4 26.170 25.856 1.267 89.751 o
9 5 5 24.971 25.307 1.257 91.140 o
9 5 6 7.784 9.670 1.625 54.528 o
9 5 7 13.742 15.437 2.188 30.089 o
9 6 0 10.836 11.590 0.844 201.988 o
9 6 1 43.987 41.976 2.249 28.473 o
9 6 2 45.118 47.196 2.066 33.730 o
9 6 3 48.122 45.737 1.615 55.193 o
9 6 4 183.382 181.245 4.883 6.039 o
9 6 5 5.553 5.591 1.769 46.039 o
9 6 6 22.148 22.604 2.192 29.981 o
9 7 0 125.419 123.015 2.401 24.976 o
9 7 2 199.571 193.402 4.042 8.815 o
9 7 3 18.181 15.661 1.278 88.154 o
9 7 4 158.343 158.268 4.302 7.781 o
9 7 5 30.751 32.270 2.868 17.504 o
9 8 0 209.308 198.702 5.198 5.331 o
9 8 1 212.477 210.063 5.342 5.046 o
9 8 2 13.343 12.756 2.566 21.863 o
9 8 3 33.796 32.241 3.025 15.742 o
10 0 0 4.867 5.679 1.323 82.299 o
10 0 1 10.123 11.581 1.205 99.157 o
10 0 2 10.634 10.926 1.241 93.579 o
10 0 3 53.160 49.677 2.259 28.217 o
10 0 4 62.950 66.656 1.999 36.052 o
10 0 5 25.968 26.298 1.558 59.339 o
10 1 1 6.377 6.678 1.189 101.825 o
10 1 2 6.600 6.608 1.227 95.584 o
10 1 3 242.623 241.733 7.205 2.774 o
10 1 5 101.138 97.061 2.509 22.868 o
10 1 6 66.582 63.925 3.555 11.392 o
10 2 2 11.485 10.839 1.033 134.895 o
10 2 3 30.111 28.432 1.211 98.153 o
10 2 4 43.993 46.167 1.436 69.875 o
10 2 5 19.624 19.821 1.788 45.044 o
10 2 6 25.567 24.852 2.758 18.938 o
10 3 0 195.278 198.423 3.221 13.877 o
10 3 1 271.553 265.032 4.695 6.534 o
10 3 2 65.239 64.136 1.652 52.742 o
10 3 3 4.583 5.405 1.245 92.898 o
10 3 4 68.338 66.696 1.764 46.270 o
10 3 5 26.996 26.317 1.541 60.639 o
10 3 6 13.669 13.882 2.745 19.106 o
10 4 0 22.323 22.979 1.044 132.146 o
10 4 1 18.938 18.534 1.160 107.029 o
10 4 3 57.811 55.360 1.804 44.238 o
10 4 5 19.127 15.781 3.179 14.248 o
10 5 0 171.651 168.322 3.739 10.304 o
10 5 1 44.826 43.687 1.600 56.269 o
10 5 2 5.732 7.715 1.999 36.032 o
10 5 3 90.309 87.863 2.368 25.679 o
10 5 4 383.689 386.415 13.466 0.794 o
10 6 1 12.787 12.927 1.669 51.687 o
10 6 3 114.432 112.344 5.172 5.383 o
11 0 1 75.168 66.330 3.386 12.564 o
11 0 2 8.755 8.558 2.406 24.884 o
11 1 0 192.797 186.153 12.042 0.993 o
11 1 1 12.161 11.088 2.384 25.329 o
11 1 2 32.086 30.452 2.767 18.814 o
11 2 0 26.653 29.708 2.679 20.070 o
11 2 1 69.990 73.108 3.549 11.431 o
;
_iucr_refine_instructions_details
;
TITL GA12 OLEX2: imported from CIF
CELL 0.71073 7.4583 9.4892 9.7301 90 90 90
ZERR 4 0 0 0 0 0 0
LATT -1
SYMM 0.5-X,-Y,0.5+Z
SYMM 0.5+X,0.5-Y,-Z
SYMM -X,0.5+Y,0.5-Z
SFAC C H N O
UNIT 20 40 8 12
CONF
MORE -1
BOND $H
ACTA
LIST -3
WGHT 0 0
FVAR 1.815593
REM
REM
REM
O(1) 4 -0.26775 -0.96250 -0.77796 11.00000 0.00833 0.00501 0.00371 =
-0.00131 0.00132 -0.00289
O(2) 4 -0.43046 -1.12553 -0.88361 11.00000 0.00613 0.00623 0.00280 =
-0.00129 0.00020 -0.00193
O(3) 4 -0.70877 -0.94883 -0.60022 11.00000 0.00624 0.00565 0.00429 =
-0.00110 -0.00169 0.00139
N(1) 3 -0.44247 -1.03635 -0.52555 11.00000 0.00515 0.00360 0.00246 =
-0.00107 0.00021 0.00086
N(2) 3 -0.73417 -0.75564 -0.40093 11.00000 0.00498 0.00311 0.00426 =
-0.00044 0.00064 0.00120
C(1) 1 -0.37319 -1.06533 -0.77671 11.00000 0.00438 0.00283 0.00271 =
-0.00110 -0.00015 -0.00016
C(2) 1 -0.42592 -1.13472 -0.63921 11.00000 0.00531 0.00293 0.00251 =
0.00044 0.00026 0.00007
C(3) 1 -0.28337 -1.24507 -0.60454 11.00000 0.01196 0.00592 0.00574 =
0.00049 -0.00019 0.00456
C(4) 1 -0.58862 -0.95479 -0.51389 11.00000 0.00450 0.00329 0.00257 =
-0.00031 -0.00001 0.00076
C(5) 1 -0.59817 -0.86705 -0.38208 11.00000 0.00645 0.00479 0.00269 =
-0.00100 -0.00036 0.00088
H(1) 2 -0.35505 -1.04196 -0.44827 11.00000 0.01900 0.02118 0.02390 =
-0.00569 -0.01473 0.00867
H(2a 2 -0.86145 -0.80156 -0.40842 11.00000 0.01055 0.02113 0.03407 =
0.00140 0.00323 0.00550
H(2b 2 -0.73277 -0.68031 -0.32372 11.00000 0.02519 0.02462 0.02171 =
-0.00042 0.00073 0.01142
H(2c 2 -0.70434 -0.70187 -0.49131 11.00000 0.02591 0.01460 0.01948 =
0.00577 -0.00459 -0.00418
H(2) 2 -0.55550 -1.18473 -0.65792 11.00000 0.02122 0.01038 0.01336 =
-0.00398 0.00062 -0.00577
H(3a 2 -0.15446 -1.19244 -0.58619 11.00000 0.02578 0.02379 0.02625 =
-0.00500 -0.00820 0.01174
H(3b 2 -0.32098 -1.30430 -0.51460 11.00000 0.04195 0.02157 0.02958 =
0.00599 -0.00010 0.01321
H(3c 2 -0.26741 -1.31662 -0.69022 11.00000 0.03927 0.02603 0.02147 =
-0.01380 0.00194 0.01440
H(5a 2 -0.46568 -0.81780 -0.36092 11.00000 0.01485 0.01803 0.02109 =
-0.00583 -0.00379 0.00023
H(5b 2 -0.63567 -0.93421 -0.29400 11.00000 0.04194 0.00906 0.01193 =
0.00698 0.00050 -0.00082
HKLF 4
END
Q1 1 -1 -0.975 -0.625 11 0.05 0.15
Q2 1 -0.466667 -0.725 -0.475 11 0.05 0.14
Q4 1 -0.666667 -1.2 -0.7 11 0.05 0.13
Q3 1 -0.133333 -1.25 -0.55 11 0.05 0.14
Q5 1 -0.9 -0.7 -0.25 11 0.05 0.13
REM The information below was added by Olex2.
REM
REM R1 = 0.0158 for 2374 Fo > 4sig(Fo) and 0.0158 for all 2374 data
REM 181 parameters refined using 0 restraints
REM Highest difference peak 0.1480, deepest hole -0.1877
REM Mean Shift 0.0002, Max Shift 0.0009.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0158
REM R1_gt = 0.0158
REM wR_ref = 0.0308
REM GOOF = 1.2843
REM Shift_max = 0.0009
REM Shift_mean = 0.0002
REM Reflections_all = 2374
REM Reflections_gt = 2374
REM Parameters = 181
REM Hole = -0.1877
REM Peak = 0.1480
REM Flack = 0.1(7)
;
# END of CIF
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_thpp
_database_code_depnum_ccdc_archive 'CCDC 2034387'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-09-28 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-03-13
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.03.04 svn.rc2590c38 for OlexSys, GUI svn.r6014)
;
_chemical_formula_moiety 'C10 H10 F2 N4'
_chemical_formula_sum 'C10 H10 F2 N4'
_chemical_formula_weight 224.215
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
_atom_type_scat_dispersion_source
H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236
57.79970 0.0030380000826
'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' custom
C 0.00211 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870
51.65120 0.215599998832
'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' custom
F 0.01364 0.01032 3.53920 2.64120 1.51700 1.02430 10.28250 4.29440 0.26150
26.14760 0.277599990368
'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' custom
N 0.00411 0.00331 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750
0.58260 -11.5290002823
'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' custom
_vrf_PLAT927_thpp
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0780 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_vrf_PLAT926_thpp
;
PROBLEM: Reported and Calculated R1 Differ by ......... -0.0255 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_vrf_PLAT928_thpp
;
PROBLEM: Reported and Calculated S value Differ by . -1.748 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/n 1'
_space_group_name_Hall '-P 2ybc (x-z,y,z)'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x+1/2,y+1/2,-z+1/2
3 -x,-y,-z
4 x-1/2,-y-1/2,z-1/2
_symmetry_Int_Tables_number 14
_cell_length_a 6.9196(1)
_cell_length_b 14.5749(2)
_cell_length_c 9.7248(1)
_cell_angle_alpha 90
_cell_angle_beta 90.637(1)
_cell_angle_gamma 90
_cell_volume 980.71(2)
_cell_formula_units_Z 4
_cell_measurement_temperature 120(2)
_cell_measurement_reflns_used 6303
_cell_measurement_theta_min 2.56
_cell_measurement_theta_max 30.96
_exptl_crystal_description prism
_exptl_crystal_colour 'light yellow'
_exptl_crystal_size_max 0.36
_exptl_crystal_size_mid 0.18
_exptl_crystal_size_min 0.10
_exptl_crystal_density_meas ?
_exptl_crystal_density_diffrn 1.519
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 464
_exptl_absorpt_coefficient_mu 0.123
_exptl_absorpt_correction_type none
_diffrn_ambient_temperature 120(2)
_diffrn_radiation_source 'fine-focus sealed tube'
_diffrn_radiation_monochromator graphite
_diffrn_measurement_device_type 'Bruker SMART CCD 6000'
_diffrn_measurement_method \w-scan
_diffrn_reflns_av_R_equivalents 0.0536
_diffrn_reflns_av_unetI/netI 0.0285
_diffrn_reflns_Laue_measured_fraction_full 1.0000
_diffrn_reflns_Laue_measured_fraction_max 1.0000
_diffrn_reflns_limit_h_max 9
_diffrn_reflns_limit_h_min -9
_diffrn_reflns_limit_k_max 20
_diffrn_reflns_limit_k_min -20
_diffrn_reflns_limit_l_max 13
_diffrn_reflns_limit_l_min -13
_diffrn_reflns_number 13911
_diffrn_reflns_point_group_measured_fraction_full 1.0000
_diffrn_reflns_point_group_measured_fraction_max 1.0000
_diffrn_reflns_theta_full 25.2417
_diffrn_reflns_theta_max 30.51
_diffrn_reflns_theta_min 2.52
_diffrn_measured_fraction_theta_full 1.0000
_diffrn_measured_fraction_theta_max 1.0000
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.71073
_reflns_Friedel_coverage 0.0
_reflns_limit_h_max 8
_reflns_limit_h_min -9
_reflns_limit_k_max 20
_reflns_limit_k_min 0
_reflns_limit_l_max 13
_reflns_limit_l_min -7
_reflns_number_gt 2456
_reflns_number_total 2975
_reflns_threshold_expression I>=2u(I)
_computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max 0.1588
_refine_diff_density_min -0.2130
_refine_diff_density_rms 0.0591
_refine_ls_d_res_high 0.6999
_refine_ls_d_res_low 8.0891
_refine_ls_goodness_of_fit_ref 1.0794
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_constraints 3
_refine_ls_number_parameters 258
_refine_ls_number_reflns 2975
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0288
_refine_ls_R_factor_gt 0.0214
_refine_ls_restrained_S_all 1.0794
_refine_ls_shift/su_max 0.0003
_refine_ls_shift/su_mean 0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0177P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0454
_refine_ls_wR_factor_ref 0.0483
_refine_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be published - 2020
NoSpherA2 implementation of HAR makes use of tailor-made
aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or DFT using selected funtionals
- for a fragment of the crystal.
This fregment can be embedded in an electrostatic crystal field by
employing cluster charges.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
INT ACCURACY: High
METHOD: PBE
BASIS SET: def2-TZVPP
CHARGE: 0
MULTIPLICITY: 1
DATE: 2020-03-13_10-35-56
;
_olex2_refinement_description
;
1. Others
Sof(C00h)=Sof(H00k)=Sof(H00l)=Sof(C1)=Sof(H1b)=Sof(H1a)=1-FVAR(1)
Sof(C00F)=Sof(H00g)=Sof(H00h)=Sof(C00G)=Sof(H00i)=Sof(H00j)=FVAR(1)
2.a Secondary CH2 refined with fixed occupancy and ADP/Uiso:
C00h(H00k,H00l), C1(H1b,H1a)
;
_atom_sites_solution_primary dual
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_refinement_flags_posn
_atom_site_disorder_group
F001 F 0.16752(4) 0.57360(2) 0.26258(3) 0.02707(8) Uani 1.000000 . .
F002 F 0.13120(5) 0.68497(2) 0.48746(4) 0.02902(8) Uani 1.000000 . .
N003 N 0.22200(6) 0.56957(3) 0.62956(4) 0.02008(9) Uani 1.000000 . .
N004 N 0.36182(6) 0.33061(3) 0.57637(4) 0.02014(9) Uani 1.000000 . .
N005 N 0.30290(6) 0.45756(3) 0.78542(4) 0.02393(10) Uani 1.000000 . .
N006 N 0.25111(8) 0.36110(4) 0.18032(5) 0.03649(12) Uani 1.000000 . .
C007 C 0.30117(6) 0.41737(3) 0.54235(5) 0.01663(9) Uani 1.000000 . .
C008 C 0.26225(6) 0.45015(3) 0.40935(5) 0.01793(10) Uani 1.000000 . .
C009 C 0.18832(7) 0.59752(3) 0.50240(5) 0.01999(10) Uani 1.000000 . .
C00A C 0.20611(7) 0.54280(3) 0.39025(5) 0.01943(10) Uani 1.000000 . .
C00B C 0.27489(6) 0.48319(3) 0.65269(5) 0.01782(10) Uani 1.000000 . .
C00C C 0.26097(8) 0.39696(4) 0.28619(5) 0.02432(11) Uani 1.000000 . .
C00D C 0.39577(9) 0.26085(4) 0.47323(6) 0.02690(12) Uani 1.000000 . .
H00a H 0.2614(12) 0.2354(6) 0.4272(9) 0.053(2) Uani 1.000000 . .
H00b H 0.4839(11) 0.2892(5) 0.3912(8) 0.042(2) Uani 1.000000 . .
H00c H 0.4731(13) 0.2060(5) 0.5206(9) 0.056(2) Uani 1.000000 . .
C00E C 0.26827(10) 0.52381(4) 0.89396(6) 0.02819(12) Uani 1.000000 . .
H00d H 0.3635(13) 0.5828(5) 0.8859(9) 0.059(3) Uani 1.000000 . .
H00e H 0.1244(12) 0.5515(6) 0.8856(9) 0.059(2) Uani 1.000000 . .
H00f H 0.2912(14) 0.4918(6) 0.9914(9) 0.068(3) Uani 1.000000 . .
C00F C 0.3680(3) 0.36581(8) 0.82064(13) 0.0241(2) Uani 0.882(5) . 1
H00g H 0.5260(13) 0.3652(6) 0.8300(9) 0.047(3) Uani 0.882(5) . 1
H00h H 0.3132(19) 0.3470(6) 0.9204(9) 0.045(5) Uani 0.882(5) . 1
C00G C 0.3055(3) 0.29777(5) 0.71192(7) 0.0241(3) Uani 0.882(5) . 1
H00i H 0.1456(13) 0.2875(6) 0.7156(9) 0.043(2) Uani 0.882(5) . 1
H00j H 0.3785(13) 0.2322(9) 0.7305(9) 0.042(10) Uani 0.882(5) . 1
H1a H 0.157(2) 0.3463(6) 0.8178(10) 0.053(19) Uiso 0.118(5) . 2
C1 C 0.292(2) 0.3652(6) 0.8186(10) 0.0256(18) Uani 0.118(5) . 2
H1b H 0.343(2) 0.3559(6) 0.9108(10) 0.12(9) Uiso 0.118(5) . 2
H00l H 0.5424(17) 0.3129(3) 0.7348(5) 0.031(14) Uiso 0.118(5) . 2
H00k H 0.3724(17) 0.2417(3) 0.7315(5) 0.06(10) Uiso 0.118(5) . 2
C00h C 0.4050(17) 0.3057(3) 0.7173(5) 0.0192(16) Uani 0.118(5) . 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
F001 0.03339(17) 0.02795(17) 0.01982(16) -0.00015(12) -0.00249(12) 0.00687(12)
F002 0.03833(18) 0.01738(15) 0.03124(19) 0.00218(12) -0.00486(14) 0.00264(12)
N003 0.0235(2) 0.0173(2) 0.0194(2) 0.00034(14) -0.00134(16) -0.00071(16)
N004 0.0251(2) 0.01706(19) 0.0183(2) 0.00116(15) 0.00149(16) 0.00095(15)
N005 0.0344(2) 0.0217(2) 0.0156(2) 0.00328(17) -0.00098(17) -0.00015(16)
N006 0.0561(3) 0.0349(3) 0.0184(2) 0.0039(2) -0.0020(2) -0.0062(2)
C007 0.0176(2) 0.0166(2) 0.0157(2) -0.00141(16) 0.00092(17) 0.00054(17)
C008 0.0196(2) 0.0189(2) 0.0153(2) -0.00208(16) 0.00112(17) 0.00040(17)
C009 0.0225(2) 0.0164(2) 0.0209(3) -0.00085(17) -0.00185(18) 0.00160(18)
C00A 0.0216(2) 0.0192(2) 0.0174(2) -0.00188(17) -0.00075(18) 0.00268(18)
C00B 0.0200(2) 0.0176(2) 0.0158(2) -0.00071(16) 0.00033(17) -0.00034(17)
C00C 0.0318(3) 0.0252(3) 0.0159(2) -0.00003(19) 0.00068(19) -0.0011(2)
C00D 0.0367(3) 0.0200(3) 0.0241(3) 0.0038(2) 0.0011(2) -0.0029(2)
H00a 0.057(6) 0.053(6) 0.047(6) -0.010(4) -0.002(5) -0.020(4)
H00b 0.056(5) 0.039(5) 0.031(5) 0.004(4) 0.014(4) -0.002(4)
H00c 0.087(7) 0.034(5) 0.047(6) 0.025(4) -0.005(5) 0.007(4)
C00E 0.0391(3) 0.0280(3) 0.0174(3) 0.0038(2) -0.0008(2) -0.0033(2)
H00d 0.082(6) 0.031(5) 0.066(7) -0.025(5) 0.013(5) -0.017(4)
H00e 0.051(6) 0.068(6) 0.059(7) 0.019(5) 0.004(4) -0.010(5)
H00f 0.126(8) 0.050(6) 0.028(6) 0.027(6) -0.007(5) -0.004(5)
C00F 0.0315(6) 0.0233(3) 0.0175(3) 0.0035(5) -0.0001(5) 0.0037(2)
H00g 0.035(5) 0.052(6) 0.053(7) 0.004(4) -0.010(5) 0.001(5)
H00h 0.093(10) 0.029(6) 0.013(6) 0.010(5) 0.002(5) 0.010(4)
C00G 0.0325(8) 0.0198(3) 0.0200(3) 0.0002(3) 0.0029(3) 0.0039(2)
H00i 0.039(6) 0.048(6) 0.041(6) -0.011(4) 0.012(4) 0.003(5)
H00j 0.076(17) 0.013(7) 0.037(11) 0.001(5) 0.001(5) 0.000(4)
C1 0.033(5) 0.024(3) 0.020(3) 0.007(4) 0.006(4) 0.0047(19)
C00h 0.016(4) 0.019(2) 0.022(2) -0.0013(19) 0.0001(19) 0.0007(16)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
F001 C00A 1.3442(6) . ?
F002 C009 1.3418(5) . ?
N003 C009 1.3202(6) . ?
N003 C00B 1.3296(6) . ?
N004 C007 1.3716(6) . ?
N004 C00D 1.4492(7) . ?
N004 C00G 1.4594(8) . ?
N004 C00h 1.446(5) . ?
N005 C00B 1.3556(6) . ?
N005 C00E 1.4524(7) . ?
N005 C00F 1.4509(13) . ?
N005 C1 1.386(9) . ?
N006 C00C 1.1560(7) . ?
C007 C008 1.4022(7) . ?
C007 C00B 1.4523(7) . ?
C008 C00A 1.4167(7) . ?
C008 C00C 1.4267(7) . ?
C009 C00A 1.3578(7) . ?
C00D H00a 1.092(8) . ?
C00D H00b 1.091(7) . ?
C00D H00c 1.064(7) . ?
C00E H00d 1.087(8) . ?
C00E H00e 1.076(8) . ?
C00E H00f 1.066(9) . ?
C00F H00g 1.096(9) . ?
C00F H00h 1.081(10) . ?
C00F C00G 1.5093(17) . ?
C00G H00i 1.118(9) . ?
C00G H00j 1.095(13) . ?
H1a C1 0.9700 . ?
C1 H1b 0.9700 . ?
C1 C00h 1.534(12) . ?
H00l C00h 0.9700 . ?
H00k C00h 0.9700 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C00B N003 C009 119.74(4) . . ?
C00D N004 C007 122.10(4) . . ?
C00G N004 C007 115.86(5) . . ?
C00G N004 C00D 116.23(5) . . ?
C00h N004 C007 121.33(18) . . ?
C00h N004 C00D 116.49(19) . . ?
C00h N004 C00G 27.8(4) . . ?
C00E N005 C00B 119.06(4) . . ?
C00F N005 C00B 121.30(6) . . ?
C00F N005 C00E 119.64(6) . . ?
C1 N005 C00B 118.8(4) . . ?
C1 N005 C00E 117.8(4) . . ?
C1 N005 C00F 21.3(5) . . ?
C008 C007 N004 126.28(4) . . ?
C00B C007 N004 118.11(4) . . ?
C00B C007 C008 115.60(4) . . ?
C00A C008 C007 119.69(4) . . ?
C00C C008 C007 126.05(5) . . ?
C00C C008 C00A 114.13(4) . . ?
N003 C009 F002 116.31(4) . . ?
C00A C009 F002 120.01(5) . . ?
C00A C009 N003 123.68(5) . . ?
C008 C00A F001 119.39(4) . . ?
C009 C00A F001 121.80(4) . . ?
C009 C00A C008 118.80(5) . . ?
N005 C00B N003 117.27(4) . . ?
C007 C00B N003 122.48(4) . . ?
C007 C00B N005 120.25(4) . . ?
C008 C00C N006 173.30(6) . . ?
H00a C00D N004 112.2(4) . . ?
H00b C00D N004 109.7(4) . . ?
H00b C00D H00a 108.0(6) . . ?
H00c C00D N004 108.2(4) . . ?
H00c C00D H00a 110.1(7) . . ?
H00c C00D H00b 108.6(6) . . ?
H00d C00E N005 111.6(4) . . ?
H00e C00E N005 110.7(5) . . ?
H00e C00E H00d 105.0(7) . . ?
H00f C00E N005 109.3(5) . . ?
H00f C00E H00d 109.0(7) . . ?
H00f C00E H00e 111.0(7) . . ?
H00g C00F N005 109.5(4) . . ?
H00h C00F N005 109.6(5) . . ?
H00h C00F H00g 106.4(8) . . ?
C00G C00F N005 110.76(10) . . ?
C00G C00F H00g 109.3(5) . . ?
C00G C00F H00h 111.2(6) . . ?
C00F C00G N004 109.88(11) . . ?
H00i C00G N004 110.3(5) . . ?
H00i C00G C00F 110.0(5) . . ?
H00j C00G N004 108.0(5) . . ?
H00j C00G C00F 109.2(5) . . ?
H00j C00G H00i 109.4(7) . . ?
H1a C1 N005 109.3(6) . . ?
H1b C1 N005 109.3(5) . . ?
H1b C1 H1a 107.94273350(2) . . ?
C00h C1 N005 111.7(7) . . ?
C00h C1 H1a 109.3(8) . . ?
C00h C1 H1b 109.3(6) . . ?
C1 C00h N004 111.4(7) . . ?
H00l C00h N004 109.3(5) . . ?
H00l C00h C1 109.3(9) . . ?
H00k C00h N004 109.3(3) . . ?
H00k C00h C1 109.3(6) . . ?
H00k C00h H00l 108.0 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
F001 C00A C008 C007 -179.47(4) . . . . ?
F001 C00A C008 C00C -3.36(5) . . . . ?
F001 C00A C009 F002 -0.13(5) . . . . ?
F001 C00A C009 N003 178.96(4) . . . . ?
F002 C009 N003 C00B 178.50(4) . . . . ?
F002 C009 C00A C008 -178.52(4) . . . . ?
N003 C009 C00A C008 0.56(6) . . . . ?
N003 C00B N005 C00E 1.93(6) . . . . ?
N003 C00B N005 C00F -177.57(9) . . . . ?
N003 C00B N005 C1 158.0(6) . . . . ?
N003 C00B C007 N004 178.00(4) . . . . ?
N003 C00B C007 C008 -1.57(5) . . . . ?
N004 C007 C008 C00A -178.05(5) . . . . ?
N004 C007 C008 C00C 6.33(6) . . . . ?
N004 C007 C00B N005 -2.49(5) . . . . ?
N004 C00G C00F N005 51.22(10) . . . . ?
N004 C00h C1 N005 -47.2(6) . . . . ?
N005 C00B C007 C008 177.94(4) . . . . ?
C007 C008 C00A C009 -1.04(5) . . . . ?
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
0 0 -1 0.03 0.05
0 0 -1 0.1 0.08
0 0 -1 -0.03 0.08
0 0 1 0.1 0.05
0 0 1 -0.03 0.08
0 0 1 0.05 0.08
0 0 -2 6.58 0.31
0 0 -2 6.16 0.47
0 0 2 5.85 0.31
0 0 2 6.24 0.42
0 0 -3 0.05 0.16
0 0 -3 0.21 0.26
0 0 3 -0.03 0.13
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8 -10 -1 1.57 0.76
8 10 -1 3.96 1.02
8 10 -1 2.78 0.94
-8 -10 0 6.48 1.23
-8 10 0 5.3 1.1
8 -10 0 4.62 1
8 10 0 6.93 1.26
8 10 0 6.77 1.26
-8 -10 -1 0.81 0.73
-8 10 -1 2.07 0.81
8 -10 1 1.47 0.79
8 10 1 2.26 0.89
8 10 1 2.36 0.92
-8 -10 -2 23.66 1.97
-8 10 -2 18.39 1.63
8 10 2 18.26 1.63
8 10 2 17.68 1.71
-8 -10 -3 5.12 1.18
-8 10 -3 2.99 1.02
8 10 3 4.12 1.05
8 10 3 2.89 0.94
-8 -10 -4 1.02 0.84
-8 10 -4 0.34 0.73
8 10 4 0.71 0.73
8 10 4 0.52 0.68
-8 -11 3 2.6 0.94
-8 11 3 3.28 1.08
8 11 -3 2.78 1
8 11 -3 2.47 1.02
-8 -11 2 14.98 1.65
-8 11 2 13.9 1.6
8 11 -2 16.95 1.73
8 11 -2 15.08 1.71
-8 -11 1 1.68 0.87
-8 11 1 1.42 0.81
8 -11 -1 1.63 0.73
8 11 -1 2.23 0.92
8 11 -1 1.47 0.84
-8 -11 0 0.34 0.68
-8 11 0 -0.34 0.58
8 -11 0 -0.18 0.58
8 11 0 -0.26 0.63
8 11 0 -0.08 0.6
-8 -11 -1 -0.05 0.63
-8 11 -1 0.05 0.6
8 -11 1 -0.03 0.68
8 11 1 -0.18 0.63
8 11 1 -0.29 0.58
-8 11 -2 10.34 1.44
8 11 2 8.5 1.31
8 11 2 6.61 1.26
-8 -11 -3 9.92 1.5
-8 11 -3 9.89 1.47
8 11 3 10.81 1.42
8 11 3 8.76 1.36
-8 -12 1 2.44 1
-8 12 1 1.02 0.81
8 12 -1 1.81 0.89
8 12 -1 1.36 0.84
-8 -12 0 0.16 0.71
-8 12 0 0.21 0.66
8 12 0 -0.5 0.68
8 12 0 -0.16 0.6
-8 -12 -1 1.23 0.84
-8 12 -1 1.55 0.81
-8 12 -1 0.76 0.76
8 12 1 1.71 0.87
8 12 1 1.76 0.84
-9 0 5 36.38 2.47
9 0 -5 39.11 2.49
-9 0 4 -0.05 0.63
9 0 -4 -0.34 0.6
-9 0 3 1.42 0.84
9 0 -3 1.65 0.84
-9 0 2 0.05 0.58
9 0 -2 -0.03 0.6
-9 0 1 8.03 1.26
9 0 -1 8.87 1.44
-9 0 0 0.58 0.6
9 0 0 -0.05 0.6
-9 0 -1 1.26 0.73
9 0 1 1.68 0.84
-9 0 -2 -0.34 0.52
9 0 2 -0.13 0.6
-9 0 -3 13.19 1.42
9 0 3 15.21 1.65
9 0 4 -0.08 0.68
9 0 5 0.29 0.71
-9 -1 5 17.5 1.81
-9 1 5 15.66 1.71
9 -1 -5 18.18 1.81
9 1 -5 18.47 1.81
-9 -1 4 8.89 1.39
-9 1 4 8.95 1.42
9 -1 -4 9.23 1.44
9 1 -4 10.41 1.52
-9 -1 3 1.31 0.76
-9 1 3 0.79 0.76
9 -1 -3 1.63 0.84
9 1 -3 0.76 0.76
-9 -1 2 1.36 0.79
-9 1 2 0.39 0.66
9 -1 -2 1.65 0.84
9 1 -2 0.94 0.76
-9 -1 1 1.15 0.73
-9 1 1 0.18 0.66
9 -1 -1 0.21 0.68
9 1 -1 0.71 0.76
-9 -1 0 17.16 1.63
-9 1 0 18.02 1.63
9 -1 0 19.23 1.78
9 1 0 17.79 1.76
-9 -1 -1 1.5 0.76
-9 1 -1 0.42 0.6
9 -1 1 1.1 0.79
9 1 1 1.23 0.79
-9 -1 -2 5.19 1.08
-9 1 -2 5.43 1.05
9 -1 2 5.8 1.21
9 1 2 5.19 1.13
-9 -1 -3 0.45 0.6
-9 1 -3 0.29 0.63
9 -1 3 1.23 0.81
9 1 3 0.5 0.81
9 -1 4 0.31 0.73
9 1 4 0.21 0.68
9 -1 5 4.25 1.21
9 1 5 2.65 1.05
-9 -2 5 15.27 1.73
-9 2 5 15.24 1.71
9 -2 -5 16.34 1.71
9 2 -5 15.71 1.71
-9 -2 4 5.4 1.21
-9 2 4 3.99 1.1
9 -2 -4 4.35 1.13
9 2 -4 4.72 1.13
-9 -2 3 0.24 0.68
-9 2 3 -0.03 0.6
9 -2 -3 0.52 0.73
9 2 -3 -0.21 0.58
-9 -2 2 -0.24 0.52
-9 2 2 0.24 0.63
9 -2 -2 0.08 0.63
9 2 -2 -0.76 0.58
-9 -2 1 -0.37 0.52
-9 2 1 -0.03 0.58
9 -2 -1 -0.08 0.68
9 2 -1 0.26 0.68
-9 -2 0 8.55 1.34
-9 2 0 7.29 1.23
9 -2 0 6.87 1.26
9 2 0 9.6 1.47
-9 -2 -1 0.52 0.66
-9 2 -1 0.34 0.6
9 -2 1 0.26 0.68
9 2 1 1.23 0.79
-9 -2 -2 -0.03 0.6
-9 2 -2 0.05 0.55
9 -2 2 0.76 0.76
9 2 2 1.97 0.89
-9 -2 -3 0.5 0.6
-9 2 -3 0.84 0.66
9 -2 3 2.36 0.92
9 2 3 0.08 0.68
-9 -2 -4 2.99 0.89
9 -2 4 4.75 1.15
9 2 4 3.99 1.1
9 -2 5 0.68 0.81
9 2 5 -0.76 0.63
-9 -3 5 1.55 0.92
-9 3 5 1.02 0.87
9 -3 -5 1.31 0.81
9 3 -5 1.94 0.92
-9 -3 4 7.42 1.36
-9 3 4 7.82 1.36
9 -3 -4 7.27 1.34
9 3 -4 6.56 1.29
-9 -3 3 2.94 0.97
-9 3 3 3.17 1.02
9 -3 -3 1.73 0.92
9 3 -3 2.44 0.97
-9 -3 2 0.39 0.71
-9 3 2 0 0.6
9 -3 -2 0 0.63
9 3 -2 -0.66 0.55
-9 -3 1 16.66 1.68
-9 3 1 19.12 1.73
9 -3 -1 20.2 1.84
9 3 -1 19.44 1.89
-9 -3 0 3.02 0.94
-9 3 0 2.52 0.87
9 -3 0 2.15 0.89
9 3 0 2.49 0.97
-9 -3 -1 -0.03 0.6
-9 3 -1 -0.16 0.55
9 -3 1 0.21 0.63
9 3 1 0.26 0.66
-9 -3 -2 -0.37 0.5
-9 3 -2 0.21 0.58
9 -3 2 -0.03 0.66
9 3 2 -0.39 0.58
-9 -3 -3 0.42 0.6
-9 3 -3 0.29 0.58
9 -3 3 -0.21 0.66
9 3 3 0.39 0.71
-9 -3 -4 13.8 1.42
9 -3 4 16.05 1.73
9 3 4 16.45 1.73
9 3 5 0.18 0.76
-9 -4 5 -0.26 0.6
-9 4 5 0.47 0.73
9 -4 -5 0.68 0.76
9 4 -5 -0.13 0.66
-9 -4 4 -0.08 0.63
-9 4 4 0.03 0.73
9 -4 -4 -0.18 0.6
9 4 -4 -0.05 0.6
-9 -4 3 2.39 1
-9 4 3 1.29 0.84
9 -4 -3 2.44 0.94
9 4 -3 2.07 0.94
-9 -4 2 1.18 0.81
-9 4 2 1.5 0.81
9 -4 -2 1.39 0.87
9 4 -2 2.57 0.97
-9 -4 1 -0.03 0.63
-9 4 1 0.16 0.66
9 -4 -1 0.52 0.66
9 4 -1 -0.79 0.6
-9 -4 0 2.73 0.94
-9 4 0 1.86 0.84
9 -4 0 2.18 0.89
9 4 0 2.89 1.02
-9 -4 -1 0.84 0.73
-9 4 -1 1.05 0.71
9 -4 1 -0.08 0.63
9 4 1 0.71 0.73
-9 -4 -2 0.84 0.68
-9 4 -2 0.92 0.71
9 -4 2 1.13 0.81
9 4 2 0 0.66
-9 -4 -3 0.45 0.6
9 -4 3 -0.24 0.63
9 4 3 -0.34 0.6
-9 -4 -4 1.44 0.84
9 -4 4 1.84 0.94
9 4 4 1.78 0.92
-9 -5 4 30.93 2.28
-9 5 4 26.99 2.15
9 -5 -4 30.95 2.23
9 5 -4 27.6 2.2
-9 -5 3 34.28 2.39
-9 5 3 33.81 2.33
9 -5 -3 31.11 2.23
9 5 -3 35.73 2.44
-9 -5 2 2.44 0.94
-9 5 2 2.1 0.94
9 -5 -2 2.81 1
9 5 -2 1.5 0.89
-9 -5 1 5.48 1.21
-9 5 1 4.83 1.13
9 -5 -1 7.11 1.29
9 5 -1 5.8 1.29
-9 -5 0 -0.05 0.58
-9 5 0 -0.47 0.58
9 -5 0 -0.37 0.63
9 5 0 -0.47 0.66
-9 -5 -1 -0.31 0.55
-9 5 -1 -0.34 0.55
9 -5 1 -0.1 0.6
9 5 1 0.6 0.73
-9 -5 -2 2.52 0.89
-9 5 -2 3.75 0.94
9 -5 2 2.26 0.92
9 5 2 3.17 1.02
-9 -5 -3 0.05 0.55
9 -5 3 0.24 0.76
9 5 3 0.08 0.68
-9 -5 -4 7.48 1.26
9 -5 4 7.55 1.44
9 5 4 7.5 1.39
-9 -6 4 49.29 2.89
-9 6 4 45.83 2.75
9 -6 -4 42.34 2.52
9 6 -4 45.38 2.75
-9 -6 3 35.23 2.44
-9 6 3 36.86 2.44
9 -6 -3 37.8 2.39
9 6 -3 34.21 2.41
-9 -6 2 10.47 1.55
-9 6 2 11.07 1.55
9 -6 -2 10.18 1.47
9 6 -2 10.73 1.55
-9 -6 1 10.34 1.5
-9 6 1 9.68 1.44
9 -6 -1 10.89 1.52
9 6 -1 12.22 1.71
-9 -6 0 9.92 1.47
-9 6 0 10.76 1.47
9 -6 0 9 1.39
9 6 0 10.55 1.55
-9 -6 -1 0.1 0.6
-9 6 -1 -0.13 0.6
9 -6 1 0.39 0.71
9 6 1 -0.6 0.63
9 6 1 -0.03 0.58
-9 -6 -2 1 0.71
-9 6 -2 0.79 0.68
9 -6 2 1.29 0.84
9 6 2 1.65 0.84
9 6 2 1.86 0.81
-9 -6 -3 0.05 0.66
9 -6 3 -0.24 0.68
9 6 3 -0.18 0.63
9 6 3 0.1 0.6
-9 -7 3 16.6 1.78
-9 7 3 14.98 1.73
9 -7 -3 11.86 1.47
9 7 -3 15.95 1.78
-9 -7 2 1.91 0.92
-9 7 2 1.63 0.89
9 -7 -2 2.18 0.94
9 7 -2 2.49 1
-9 -7 1 4.51 1.15
-9 7 1 5.95 1.23
9 -7 -1 4.43 1.1
9 7 -1 5.61 1.29
-9 -7 0 -0.13 0.63
-9 7 0 0.1 0.71
9 -7 0 -0.21 0.63
9 7 0 -0.21 0.73
9 7 0 -0.16 0.58
-9 -7 -1 3.88 1.08
-9 7 -1 3.1 0.97
9 -7 1 3.52 1
9 7 1 2.73 1.05
9 7 1 3.12 0.97
-9 -7 -2 1.57 0.84
-9 7 -2 1.71 0.81
9 -7 2 1.97 0.94
9 7 2 2.15 0.94
9 7 2 1.31 0.76
-9 -7 -3 -0.1 0.66
9 -7 3 -0.42 0.73
9 7 3 -0.79 0.6
9 7 3 0.21 0.63
-9 -8 2 0.97 0.84
-9 8 2 1.84 0.94
9 -8 -2 2.18 0.89
9 8 -2 2.33 0.94
9 8 -2 1.6 0.89
-9 -8 1 0.05 0.68
-9 8 1 0.21 0.73
9 -8 -1 0.1 0.66
9 8 -1 0.68 0.79
9 8 -1 -0.03 0.6
-9 -8 0 6.16 1.26
-9 8 0 5.12 1.13
9 -8 0 5.14 1.15
9 8 0 5.9 1.29
9 8 0 6.01 1.26
-9 -8 -1 10.28 1.52
-9 8 -1 9.92 1.44
9 -8 1 9.92 1.5
9 8 1 11.49 1.57
9 8 1 9.1 1.44
-9 -8 -2 1.86 0.94
9 -8 2 2.6 1
9 8 2 2.91 1.02
9 8 2 1 0.81
_iucr_refine_fcf_details
;
data_thpp_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x+1/2,y+1/2,-z+1/2
3 -x,-y,-z
4 x-1/2,-y-1/2,z-1/2
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/n 1'
_space_group_name_Hall '-P 2ybc (x-z,y,z)'
_symmetry_space_group_name_H-M 'P 1 21/n 1'
_symmetry_space_group_name_Hall '-P 2ybc (x-z,y,z)'
_symmetry_Int_Tables_number 14
_cell_length_a 6.9196(1)
_cell_length_b 14.5749(2)
_cell_length_c 9.7248(1)
_cell_angle_alpha 90
_cell_angle_beta 90.637(1)
_cell_angle_gamma 90
_cell_volume 980.71(2)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
-9 0 -5 0.244 0.889 2.176 29.219 o
-9 0 -3 40.207 43.281 3.299 12.119 o
-9 0 -1 5.133 4.461 1.689 48.386 o
-9 0 1 26.453 25.793 2.907 15.972 o
-9 0 3 7.109 4.705 1.821 41.593 o
-9 0 5 108.934 115.811 5.375 4.221 o
-9 1 -5 13.699 10.594 2.452 22.823 o
-9 1 -4 0.392 0.792 1.525 59.492 o
-9 1 -3 3.006 1.792 1.061 122.694 o
-9 1 -2 15.761 16.542 1.705 46.298 o
-9 1 -1 3.261 3.126 1.104 113.315 o
-9 1 0 55.197 55.291 2.599 17.941 o
-9 1 1 1.929 1.671 1.079 118.701 o
-9 1 2 2.796 3.196 1.155 103.581 o
-9 1 3 3.312 3.403 1.192 97.138 o
-9 1 4 28.282 28.719 2.207 26.997 o
-9 1 5 48.057 53.554 2.733 16.767 o
-9 2 -5 1.016 -0.398 2.207 28.412 o
-9 2 -4 8.991 11.930 1.817 41.513 o
-9 2 -3 4.047 2.558 1.159 102.694 o
-9 2 -2 2.384 1.684 1.199 96.172 o
-9 2 -1 1.113 1.706 1.031 130.118 o
-9 2 0 22.841 24.758 2.016 32.640 o
-9 2 1 0.017 -0.232 0.924 161.967 o
-9 2 2 0.030 -0.568 0.896 172.480 o
-9 2 3 0.664 0.321 0.980 144.181 o
-9 2 4 14.099 14.215 1.748 44.390 o
-9 2 5 43.401 47.984 2.628 18.346 o
-9 3 -5 1.857 0.552 2.330 25.498 o
-9 3 -4 45.134 46.910 2.841 15.855 o
-9 3 -3 0.407 0.695 0.968 147.721 o
-9 3 -2 0.061 -0.482 0.876 180.303 o
-9 3 -1 0.607 0.180 0.928 160.520 o
-9 3 0 7.863 7.809 1.402 69.693 o
-9 3 1 54.992 57.786 2.727 16.438 o
-9 3 2 0.254 -0.308 0.942 155.936 o
-9 3 3 7.835 7.839 1.484 62.322 o
-9 3 4 22.111 22.308 2.048 31.808 o
-9 3 5 3.495 4.427 1.343 76.522 o
-9 4 -4 6.001 5.143 1.587 54.724 o
-9 4 -3 0.039 -0.123 1.079 118.941 o
-9 4 -2 1.691 2.138 1.086 117.232 o
-9 4 -1 2.838 1.857 1.067 121.399 o
-9 4 0 10.351 7.315 1.403 69.331 o
-9 4 1 1.097 -0.163 0.975 145.629 o
-9 4 2 6.325 4.981 1.315 79.515 o
-9 4 3 8.815 6.192 1.417 68.269 o
-9 4 4 0.807 -0.229 0.972 146.567 o
-9 4 5 0.285 0.474 1.040 127.866 o
-9 5 -4 21.894 23.011 2.401 23.372 o
-9 5 -3 1.112 0.349 1.142 106.029 o
-9 5 -2 9.062 9.123 1.439 65.998 o
-9 5 -1 0.331 -0.242 0.913 165.937 o
-9 5 0 0.221 -1.028 0.934 158.495 o
-9 5 1 16.622 17.924 1.877 38.302 o
-9 5 2 6.535 6.723 1.441 66.227 o
-9 5 3 91.887 103.314 3.592 8.768 o
-9 5 4 85.566 89.393 3.392 9.969 o
-9 6 -3 1.098 -0.195 0.981 143.669 o
-9 6 -2 4.885 3.949 1.051 124.532 o
-9 6 -1 1.330 -0.192 0.849 191.880 o
-9 6 0 27.858 30.845 2.248 26.037 o
-9 6 1 27.321 32.937 2.350 23.901 o
-9 6 2 26.482 32.525 2.343 24.087 o
-9 6 3 100.570 110.611 3.708 8.068 o
-9 6 4 131.524 139.785 4.165 6.011 o
-9 7 -3 0.293 -0.854 0.996 139.479 o
-9 7 -2 6.446 5.268 1.164 101.303 o
-9 7 -1 9.546 10.081 1.386 70.928 o
-9 7 0 0.959 -0.384 0.890 174.839 o
-9 7 1 15.073 15.760 1.817 40.983 o
-9 7 2 7.838 6.251 1.433 66.850 o
-9 7 3 45.219 45.362 2.686 17.606 o
-9 8 -2 6.511 6.208 1.426 67.577 o
-9 8 -1 31.062 31.125 2.045 30.859 o
-9 8 0 18.666 17.337 1.662 48.254 o
-9 8 1 0.379 0.557 0.936 157.814 o
-9 8 2 5.321 5.418 1.230 90.864 o
-8 0 -6 7.591 6.437 2.667 19.416 o
-8 0 -4 25.091 22.698 2.851 16.650 o
-8 0 -2 28.029 27.757 2.631 19.304 o
-8 0 0 15.524 16.182 2.230 27.398 o
-8 0 2 2.246 3.061 1.686 48.658 o
-8 0 4 137.443 145.529 5.394 3.923 o
-8 0 6 1.285 2.145 1.505 61.053 o
-8 0 8 4.372 3.172 1.756 44.828 o
-8 1 -7 50.787 54.437 3.836 8.890 o
-8 1 -6 0.306 -0.736 1.778 43.785 o
-8 1 -5 1.804 1.332 2.054 32.806 o
-8 1 -4 3.901 3.221 1.003 137.082 o
-8 1 -3 41.996 39.094 2.040 29.501 o
-8 1 -2 1.572 0.867 0.867 183.924 o
-8 1 -1 3.021 2.173 0.961 149.480 o
-8 1 0 15.665 15.472 1.548 55.942 o
-8 1 1 11.118 10.916 1.395 69.735 o
-8 1 2 5.631 5.498 1.162 101.742 o
-8 1 3 0.002 -1.187 0.742 251.363 o
-8 1 4 9.954 10.257 1.420 67.594 o
-8 1 5 32.358 32.961 2.099 29.202 o
-8 1 6 23.760 25.600 2.061 31.200 o
-8 1 7 1.642 1.308 1.057 123.754 o
-8 1 8 0.018 -0.514 0.987 141.970 o
-8 2 -7 23.698 22.726 2.869 16.471 o
-8 2 -6 5.646 6.927 2.728 18.566 o
-8 2 -5 34.568 36.185 3.273 12.470 o
-8 2 -4 100.499 100.149 3.824 7.777 o
-8 2 -3 1.717 1.329 0.885 176.395 o
-8 2 -2 29.900 28.698 1.905 35.445 o
-8 2 -1 4.136 4.278 1.074 119.397 o
-8 2 0 31.578 30.768 2.095 29.452 o
-8 2 1 155.443 163.642 3.897 6.001 o
-8 2 2 14.303 13.489 1.499 59.953 o
-8 2 3 38.354 37.212 2.106 28.300 o
-8 2 4 17.869 18.702 1.726 44.898 o
-8 2 5 2.263 1.591 1.002 137.751 o
-8 2 6 2.617 2.318 1.089 116.538 o
-8 2 7 0.072 0.097 0.937 157.469 o
-8 2 8 38.501 40.035 2.515 20.338 o
-8 3 -7 3.780 2.133 1.662 50.031 o
-8 3 -6 0.003 -0.807 1.452 65.668 o
-8 3 -5 46.972 50.139 3.628 9.962 o
-8 3 -4 141.310 142.419 5.365 3.943 o
-8 3 -3 135.865 138.269 3.494 7.652 o
-8 3 -2 4.900 3.176 1.034 128.740 o
-8 3 -1 57.634 55.759 2.394 20.486 o
-8 3 0 45.878 42.556 2.193 25.441 o
-8 3 1 5.488 5.452 1.205 94.722 o
-8 3 2 59.339 61.885 2.590 17.633 o
-8 3 3 3.797 2.485 1.037 128.278 o
-8 3 4 12.814 15.028 1.616 51.837 o
-8 3 5 9.325 10.907 1.501 60.607 o
-8 3 6 0.751 0.193 0.911 166.680 o
-8 3 7 0.066 0.041 0.964 148.951 o
-8 3 8 0.622 -0.210 1.079 118.804 o
-8 4 -7 41.044 38.089 3.443 11.197 o
-8 4 -6 11.486 7.433 2.102 31.082 o
-8 4 -5 241.504 253.817 6.742 2.147 o
-8 4 -4 33.201 31.038 1.987 32.330 o
-8 4 -3 74.675 73.283 2.348 19.100 o
-8 4 -2 40.730 39.005 1.822 36.153 o
-8 4 -1 7.256 4.428 0.975 143.633 o
-8 4 0 0.381 -0.191 0.841 195.637 o
-8 4 1 358.863 368.631 6.375 1.689 o
-8 4 2 141.046 150.573 3.852 6.471 o
-8 4 3 27.186 30.046 2.048 31.142 o
-8 4 4 6.819 6.137 1.271 84.913 o
-8 4 5 5.802 5.287 1.263 86.173 o
-8 4 6 2.971 2.078 1.074 119.794 o
-8 4 7 0.003 -0.768 0.923 162.300 o
-8 5 -7 87.434 94.958 4.879 5.251 o
-8 5 -6 1.621 0.682 1.614 53.130 o
-8 5 -5 93.670 87.346 6.847 2.794 o
-8 5 -4 208.704 209.411 8.331 1.664 o
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3 14 6 30.691 32.710 2.088 29.631 o
3 14 7 14.039 12.724 1.587 53.684 o
3 14 8 10.742 8.661 1.467 63.345 o
3 14 9 24.698 24.411 2.105 29.952 o
3 15 3 194.701 194.926 4.554 4.234 o
3 15 4 43.984 41.417 2.071 28.398 o
3 15 5 0.043 -0.765 0.805 213.629 o
3 15 6 63.919 62.953 3.017 13.336 o
3 15 7 28.756 30.230 2.880 16.158 o
3 15 8 66.346 65.876 3.932 8.219 o
3 16 3 0.233 -0.096 0.822 204.972 o
3 16 4 2.517 2.607 1.210 94.395 o
3 16 5 0.017 -0.282 1.055 124.332 o
3 16 6 25.958 29.057 2.558 20.439 o
3 16 7 1.366 -0.139 1.225 92.237 o
3 17 3 9.132 10.697 1.442 65.646 o
3 17 4 0.078 -0.358 1.032 129.843 o
3 17 5 113.232 125.200 4.556 5.517 o
3 17 6 18.344 22.406 2.565 20.653 o
3 18 3 80.153 84.443 3.087 11.903 o
3 18 4 0.100 -0.266 1.175 100.175 o
3 18 5 32.448 33.997 2.823 16.652 o
3 19 3 118.514 131.491 4.686 5.181 o
4 0 4 2213.010 2246.220 50.233 0.034 o
4 0 6 156.422 157.350 4.758 4.557 o
4 0 8 34.510 31.853 2.531 20.459 o
4 0 10 3.336 2.756 1.686 48.639 o
4 0 12 35.093 38.815 3.616 10.255 o
4 1 4 10.662 10.116 0.620 330.312 o
4 1 5 546.848 555.549 12.577 0.546 o
4 1 6 12.488 11.352 0.653 292.728 o
4 1 7 54.381 52.675 2.995 14.003 o
4 1 8 135.152 137.239 3.623 7.307 o
4 1 9 22.484 22.184 1.706 45.108 o
4 1 10 1.908 0.994 0.900 170.857 o
4 1 11 21.795 24.698 1.995 33.394 o
4 1 12 23.815 22.904 2.070 31.034 o
4 2 4 150.029 148.793 3.142 8.180 o
4 2 5 1.773 1.765 0.422 773.227 o
4 2 6 91.245 86.994 2.516 15.601 o
4 2 7 0.176 0.201 0.433 738.370 o
4 2 8 0.137 0.290 0.729 260.638 o
4 2 9 198.408 202.220 4.265 4.502 o
4 2 10 81.850 85.511 2.961 12.651 o
4 2 11 10.747 12.164 1.570 55.223 o
4 2 12 2.888 3.164 1.238 90.196 o
4 3 4 179.640 161.919 10.737 1.109 o
4 3 5 18.383 16.239 0.931 143.350 o
4 3 6 36.598 36.795 1.718 41.015 o
4 3 7 145.949 151.242 4.059 5.929 o
4 3 8 355.690 374.093 9.065 1.122 o
4 3 9 32.429 29.798 1.883 35.863 o
4 3 10 110.097 116.651 6.112 3.349 o
4 3 11 6.543 6.565 1.346 75.769 o
4 3 12 7.213 4.113 1.306 80.524 o
4 4 4 126.189 125.452 2.710 11.219 o
4 4 5 53.849 51.666 1.644 38.539 o
4 4 6 1.442 1.140 0.579 411.615 o
4 4 7 547.305 576.339 13.477 0.495 o
4 4 8 6.926 7.028 1.120 108.912 o
4 4 9 2.540 2.107 0.934 158.245 o
4 4 10 0.019 -0.791 0.819 206.131 o
4 4 11 12.804 11.335 1.593 53.540 o
4 4 12 15.079 13.965 1.808 41.490 o
4 5 4 385.247 388.532 6.356 1.584 o
4 5 5 20.938 19.455 0.914 143.001 o
4 5 6 49.928 52.059 1.671 38.435 o
4 5 7 4.130 3.996 0.794 217.525 o
4 5 8 129.846 129.804 4.898 4.724 o
4 5 9 16.856 17.338 1.752 43.785 o
4 5 10 18.920 17.086 1.707 45.816 o
4 5 11 50.872 53.399 4.030 8.100 o
4 5 12 17.221 17.314 1.936 36.032 o
4 6 4 14.147 13.537 0.818 189.276 o
4 6 5 388.100 393.236 10.660 0.857 o
4 6 6 167.733 168.662 2.847 8.144 o
4 6 7 229.071 232.974 5.192 3.170 o
4 6 8 7.704 7.092 0.963 146.396 o
4 6 9 3.532 3.291 1.030 129.960 o
4 6 10 2.909 1.453 0.984 142.631 o
4 6 11 0.511 -1.064 0.972 146.559 o
4 7 4 468.814 480.169 8.661 0.952 o
4 7 5 1049.630 1090.660 20.241 0.181 o
4 7 6 213.009 212.841 3.241 5.585 o
4 7 7 19.588 22.573 1.372 68.626 o
4 7 8 45.776 44.960 1.811 35.209 o
4 7 9 0.799 0.596 0.863 185.594 o
4 7 10 34.766 31.479 2.129 28.305 o
4 7 11 0.227 -1.530 1.113 111.725 o
4 8 4 214.311 215.938 4.028 4.500 o
4 8 5 650.677 652.094 11.051 0.541 o
4 8 6 96.182 91.439 2.278 17.284 o
4 8 7 3.829 3.196 0.788 221.375 o
4 8 8 6.575 5.189 0.963 147.377 o
4 8 9 2.621 2.188 1.006 136.453 o
4 8 10 0.064 -0.814 1.097 115.023 o
4 8 11 27.475 26.992 2.648 19.098 o
4 9 4 476.653 479.228 5.516 1.354 o
4 9 5 390.679 407.488 9.023 1.058 o
4 9 6 6.379 6.041 0.909 165.061 o
4 9 7 87.067 90.515 2.541 15.542 o
4 9 8 0.901 0.127 0.820 205.828 o
4 9 9 11.500 12.412 1.822 41.132 o
4 9 10 31.234 35.293 2.707 18.058 o
4 9 11 0.096 -1.817 1.186 98.330 o
4 10 4 121.674 119.036 2.139 15.094 o
4 10 5 1.258 1.176 0.649 328.086 o
4 10 6 43.869 39.785 1.769 37.435 o
4 10 7 3.513 2.161 0.945 154.325 o
4 10 8 1.800 0.795 0.920 163.273 o
4 10 9 57.727 66.336 3.259 11.751 o
4 10 10 40.739 45.162 2.968 14.772 o
4 11 4 23.884 22.520 1.148 92.892 o
4 11 5 3.903 3.953 0.961 149.081 o
4 11 6 1.338 0.267 0.799 216.453 o
4 11 7 7.700 8.040 1.277 83.824 o
4 11 8 30.043 30.726 2.087 29.795 o
4 11 9 40.360 40.867 2.328 23.305 o
4 11 10 8.536 8.042 2.199 28.491 o
4 12 4 12.468 11.820 1.100 110.087 o
4 12 5 9.511 8.702 1.242 88.165 o
4 12 6 2.874 2.638 0.999 138.332 o
4 12 7 6.189 5.939 1.246 88.444 o
4 12 8 1.139 1.236 1.038 128.408 o
4 12 9 1.188 0.711 1.071 120.533 o
4 13 4 83.895 76.974 2.594 15.686 o
4 13 5 35.357 37.242 2.022 30.786 o
4 13 6 11.568 9.730 1.367 72.633 o
4 13 7 11.039 10.283 1.495 60.945 o
4 13 8 2.050 1.384 1.119 110.404 o
4 13 9 14.484 14.751 1.784 42.606 o
4 14 4 22.364 20.944 1.686 46.244 o
4 14 5 3.665 2.993 1.072 120.000 o
4 14 6 8.723 8.436 1.473 63.078 o
4 14 7 72.684 71.528 4.088 7.539 o
4 14 8 17.619 18.239 1.904 37.150 o
4 15 4 32.998 36.312 2.485 21.156 o
4 15 5 88.813 92.840 3.127 11.219 o
4 15 6 44.259 45.156 2.625 18.408 o
4 15 7 0.687 -0.507 1.030 130.412 o
4 16 4 30.051 31.405 2.530 20.676 o
4 16 5 111.261 125.625 4.382 5.904 o
4 16 6 49.579 56.534 3.190 12.556 o
4 17 4 7.597 7.177 1.649 50.594 o
4 17 5 19.474 17.348 2.186 28.315 o
4 18 4 24.062 23.860 2.498 21.545 o
5 0 5 32.450 31.974 2.318 24.274 o
5 0 7 75.765 78.916 3.521 9.709 o
5 0 9 32.964 30.273 2.753 17.515 o
5 0 11 0.195 0.369 1.405 70.134 o
5 1 5 50.799 46.549 2.109 26.540 o
5 1 6 6.746 6.166 0.586 387.305 o
5 1 7 33.490 35.556 1.812 37.913 o
5 1 8 5.347 5.626 1.079 117.867 o
5 1 9 0.072 0.018 0.838 197.217 o
5 1 10 0.009 -0.889 0.844 194.287 o
5 1 11 33.322 34.937 2.371 23.136 o
5 2 5 36.481 36.327 1.095 85.571 o
5 2 6 2.462 2.042 0.528 492.690 o
5 2 7 2.150 1.801 0.791 220.526 o
5 2 8 61.231 58.839 2.362 20.568 o
5 2 9 149.022 157.166 5.428 3.769 o
5 2 10 0.828 0.729 0.973 146.184 o
5 2 11 28.801 30.113 2.246 26.045 o
5 3 5 90.456 85.653 2.155 19.410 o
5 3 6 0.053 -0.011 0.458 659.392 o
5 3 7 286.881 288.459 7.810 1.591 o
5 3 8 34.021 33.636 1.935 33.707 o
5 3 9 7.574 7.891 1.304 80.461 o
5 3 10 1.639 1.139 1.007 136.386 o
5 3 11 5.669 4.857 1.339 76.831 o
5 4 5 47.350 42.198 3.824 9.060 o
5 4 6 50.781 47.053 2.259 23.544 o
5 4 7 174.530 166.841 5.255 3.748 o
5 4 8 307.744 319.270 10.274 1.017 o
5 4 9 27.001 28.381 1.979 33.310 o
5 4 10 6.097 4.679 1.247 88.386 o
5 4 11 3.487 1.171 1.165 101.717 o
5 5 5 56.161 53.637 1.695 36.077 o
5 5 6 155.608 139.590 15.902 0.532 o
5 5 7 523.400 532.715 13.498 0.514 o
5 5 8 248.304 248.757 4.575 3.429 o
5 5 9 9.345 9.781 1.404 69.192 o
5 5 10 65.489 74.455 2.954 13.567 o
5 5 11 10.207 10.218 1.639 50.888 o
5 6 5 36.606 37.727 1.836 36.421 o
5 6 6 0.019 -0.124 0.596 389.437 o
5 6 7 270.656 281.394 4.835 2.941 o
5 6 8 41.444 42.637 2.354 22.721 o
5 6 9 60.989 60.770 3.460 10.534 o
5 6 10 17.255 18.710 1.837 39.838 o
5 6 11 31.087 34.712 2.898 15.860 o
5 7 5 0.853 0.904 0.641 336.113 o
5 7 6 19.106 18.715 1.309 75.760 o
5 7 7 15.521 14.362 1.244 85.425 o
5 7 8 243.676 254.698 6.999 2.028 o
5 7 9 3.006 3.374 1.155 103.583 o
5 7 10 103.709 108.754 6.127 3.372 o
5 8 5 60.843 62.624 2.044 25.796 o
5 8 6 185.918 188.338 4.268 4.741 o
5 8 7 28.082 27.343 1.598 49.458 o
5 8 8 14.990 15.804 1.364 71.519 o
5 8 9 26.629 29.302 2.101 29.731 o
5 8 10 0.446 -0.221 1.245 89.268 o
5 9 5 194.403 203.504 4.201 4.625 o
5 9 6 96.417 98.608 3.246 10.247 o
5 9 7 0.119 -0.849 0.671 307.279 o
5 9 8 0.007 -0.407 0.842 195.181 o
5 9 9 19.211 21.611 2.767 17.776 o
5 9 10 153.907 179.718 5.782 3.315 o
5 10 5 0.016 0.274 0.749 246.747 o
5 10 6 1.591 0.561 0.746 248.561 o
5 10 7 12.109 11.502 1.433 65.978 o
5 10 8 20.593 20.646 1.849 38.968 o
5 10 9 0.597 -0.073 1.174 100.473 o
5 11 5 8.333 7.297 1.194 95.705 o
5 11 6 2.176 1.054 0.910 166.749 o
5 11 7 17.574 16.636 1.663 48.398 o
5 11 8 0.442 0.342 0.996 139.413 o
5 11 9 16.926 15.603 2.123 30.128 o
5 12 5 20.317 18.870 1.657 48.251 o
5 12 6 145.743 146.868 4.234 5.615 o
5 12 7 3.274 0.825 1.029 130.427 o
5 12 8 17.034 15.095 1.756 43.669 o
5 13 5 39.169 43.511 2.239 25.022 o
5 13 6 1.563 1.773 1.063 122.437 o
5 13 7 2.310 0.253 1.049 125.730 o
5 13 8 53.312 55.188 2.730 16.535 o
5 14 5 39.459 39.705 2.296 24.007 o
5 14 6 42.026 42.553 2.370 22.400 o
5 14 7 121.197 122.646 4.831 4.943 o
5 15 5 1.996 1.193 1.296 82.314 o
5 15 6 12.002 10.475 1.612 52.387 o
5 16 5 32.309 33.227 2.757 17.434 o
6 0 6 3.479 3.657 1.252 88.065 o
6 0 8 182.127 183.943 5.736 3.188 o
6 0 10 25.071 27.248 3.024 14.791 o
6 1 6 68.915 70.033 1.980 25.474 o
6 1 7 0.005 -0.864 0.636 342.406 o
6 1 8 24.322 24.578 1.852 38.270 o
6 1 9 12.482 11.608 1.501 60.179 o
6 1 10 27.619 29.571 2.199 27.200 o
6 2 6 4.406 4.338 0.699 279.608 o
6 2 7 28.274 27.070 1.790 40.119 o
6 2 8 63.944 62.797 2.557 17.717 o
6 2 9 11.273 10.949 1.608 52.723 o
6 2 10 49.825 54.778 2.694 17.101 o
6 3 6 4.445 3.394 0.744 247.806 o
6 3 7 0.985 0.189 0.797 218.019 o
6 3 8 210.322 222.381 4.497 3.990 o
6 3 9 2.697 2.582 1.093 115.543 o
6 3 10 4.975 3.096 1.218 92.881 o
6 4 6 7.330 6.869 0.902 166.585 o
6 4 7 372.451 413.599 14.741 0.524 o
6 4 8 11.358 10.272 1.423 67.062 o
6 4 9 1.371 0.299 0.986 142.303 o
6 4 10 16.146 18.600 1.907 37.134 o
6 5 6 13.233 8.434 2.773 17.903 o
6 5 7 77.885 83.736 3.252 11.000 o
6 5 8 0.086 -0.049 0.870 182.958 o
6 5 9 2.387 2.666 1.112 111.677 o
6 5 10 4.574 3.964 1.298 81.849 o
6 6 6 101.993 100.249 5.405 4.264 o
6 6 7 77.694 79.882 2.399 17.995 o
6 6 8 33.263 35.383 2.185 26.937 o
6 6 9 0.936 -0.135 1.011 135.425 o
6 6 10 11.083 9.823 1.618 52.169 o
6 7 6 3.578 3.179 0.762 236.644 o
6 7 7 42.766 43.138 2.744 17.061 o
6 7 8 0.192 -0.223 0.867 184.060 o
6 7 9 13.273 13.068 1.666 48.912 o
6 8 6 0.016 0.156 0.613 368.253 o
6 8 7 68.582 66.209 2.048 24.535 o
6 8 8 16.459 19.284 2.802 17.419 o
6 8 9 26.984 27.712 2.566 20.303 o
6 9 6 7.051 5.590 1.015 132.662 o
6 9 7 9.757 7.938 1.175 98.281 o
6 9 8 0.133 -0.194 1.138 106.819 o
6 9 9 17.209 18.762 2.242 27.010 o
6 10 6 24.471 26.244 1.915 35.789 o
6 10 7 5.801 3.939 1.174 99.738 o
6 10 8 1.827 1.059 1.238 90.207 o
6 11 6 4.641 2.676 1.064 121.629 o
6 11 7 7.998 8.004 1.407 69.228 o
6 11 8 4.336 2.848 1.421 68.405 o
6 12 6 0.588 -0.631 0.933 158.914 o
6 12 7 0.111 -0.845 0.950 153.316 o
6 13 6 1.440 0.773 1.093 115.749 o
7 0 7 96.551 92.542 4.176 6.818 o
7 0 9 6.811 5.940 1.971 35.482 o
7 1 7 9.874 8.932 1.282 82.688 o
7 1 8 2.017 1.076 0.959 150.220 o
7 1 9 4.003 2.199 1.172 100.505 o
7 2 7 7.835 6.231 1.184 97.601 o
7 2 8 54.955 55.228 2.539 18.700 o
7 2 9 14.274 13.044 1.657 49.341 o
7 3 7 50.695 50.722 2.632 17.882 o
7 3 8 12.256 11.928 1.540 57.224 o
7 3 9 12.542 10.885 1.593 53.572 o
7 4 7 23.065 22.281 1.790 41.070 o
7 4 8 0.001 -0.194 0.918 164.337 o
7 4 9 8.791 8.631 1.516 59.618 o
7 5 7 47.188 44.029 2.276 23.655 o
7 5 8 58.944 53.598 2.840 15.214 o
7 5 9 5.936 4.012 1.299 81.597 o
7 6 7 263.595 283.968 9.105 1.306 o
7 6 8 5.483 3.888 1.243 89.126 o
7 7 7 127.908 132.453 5.057 4.487 o
7 7 8 88.741 91.945 3.295 10.330 o
7 8 7 8.605 7.539 1.394 70.468 o
7 8 8 99.499 107.430 4.110 6.859 o
7 9 7 0.501 -0.313 1.144 105.664 o
7 10 7 2.222 0.313 1.637 51.654 o
8 0 8 107.326 106.054 7.571 2.272 o
8 1 8 4.601 4.088 1.985 35.060 o
;
_iucr_refine_instructions_details
;
TITL thpp_a.res in P2(1)/n
REM Old TITL thpp_a.res in P2(1)/n
REM SHELXT solution in P2(1)/n
REM R1 0.125, Rweak 0.002, Alpha 0.014, Orientation as input
REM Formula found by SHELXT: C11 F2 N3
CELL 0.71073 6.9196 14.5749 9.7248 90 90.637 90
ZERR 4 0.0001 0.0002 0.0001 0 0.001 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H F N
DISP C 0.0021 0.0016 11.5003
DISP F 0.0136 0.0103 51.4857
DISP H 0 0 0.624
DISP N 0.0041 0.0033 19.5955
UNIT 40 40 8 16
L.S. 10
PLAN 20
CONF
BOND $H
FMAP 2
MORE -1
ACTA
LIST -3
WGHT 0.017742 0
FVAR 0.571182 0.88161
REM
REM
REM
F001 3 0.16752 0.57360 0.26258 11.00000 0.03339 0.02795 0.01982 =
0.00687 -0.00249 -0.00015
F002 3 0.13120 0.68497 0.48746 11.00000 0.03833 0.01738 0.03124 =
0.00264 -0.00486 0.00218
N003 4 0.22200 0.56957 0.62956 11.00000 0.02354 0.01732 0.01936 =
-0.00071 -0.00134 0.00034
N004 4 0.36182 0.33061 0.57637 11.00000 0.02505 0.01706 0.01835 =
0.00095 0.00149 0.00116
N005 4 0.30290 0.45756 0.78542 11.00000 0.03445 0.02171 0.01560 =
-0.00015 -0.00098 0.00328
N006 4 0.25111 0.36110 0.18032 11.00000 0.05610 0.03486 0.01844 =
-0.00617 -0.00201 0.00389
C007 1 0.30117 0.41737 0.54235 11.00000 0.01760 0.01663 0.01567 =
0.00054 0.00092 -0.00141
C008 1 0.26225 0.45015 0.40935 11.00000 0.01961 0.01886 0.01533 =
0.00040 0.00112 -0.00208
C009 1 0.18832 0.59752 0.50240 11.00000 0.02255 0.01644 0.02092 =
0.00160 -0.00185 -0.00085
C00A 1 0.20611 0.54280 0.39025 11.00000 0.02165 0.01921 0.01742 =
0.00268 -0.00075 -0.00188
C00B 1 0.27489 0.48319 0.65269 11.00000 0.02000 0.01763 0.01582 =
-0.00034 0.00033 -0.00071
C00C 1 0.26097 0.39696 0.28619 11.00000 0.03183 0.02519 0.01594 =
-0.00114 0.00068 -0.00003
C00D 1 0.39577 0.26085 0.47323 11.00000 0.03666 0.02000 0.02408 =
-0.00292 0.00112 0.00376
H00a 2 0.26144 0.23540 0.42715 11.00000 0.05743 0.05335 0.04690 =
-0.02042 -0.00194 -0.01004
H00b 2 0.48388 0.28919 0.39120 11.00000 0.05621 0.03859 0.03109 =
-0.00195 0.01439 0.00370
H00c 2 0.47308 0.20602 0.52061 11.00000 0.08656 0.03391 0.04749 =
0.00701 -0.00454 0.02490
C00E 1 0.26827 0.52381 0.89396 11.00000 0.03908 0.02801 0.01745 =
-0.00329 -0.00078 0.00378
H00d 2 0.36353 0.58280 0.88594 11.00000 0.08202 0.03077 0.06575 =
-0.01710 0.01316 -0.02467
H00e 2 0.12441 0.55148 0.88561 11.00000 0.05122 0.06756 0.05867 =
-0.00973 0.00444 0.01894
H00f 2 0.29116 0.49180 0.99138 11.00000 0.12641 0.05033 0.02781 =
-0.00410 -0.00672 0.02724
PART 1
C00F 1 0.36801 0.36581 0.82064 21.00000 0.03147 0.02330 0.01752 =
0.00374 -0.00007 0.00353
H00g 2 0.52600 0.36519 0.82995 21.00000 0.03518 0.05166 0.05273 =
0.00058 -0.00999 0.00449
H00h 2 0.31320 0.34697 0.92044 21.00000 0.09345 0.02935 0.01338 =
0.00986 0.00167 0.00983
C00G 1 0.30554 0.29777 0.71192 21.00000 0.03247 0.01976 0.02002 =
0.00394 0.00293 0.00023
H00i 2 0.14564 0.28748 0.71562 21.00000 0.03921 0.04803 0.04087 =
0.00336 0.01179 -0.01125
H00j 2 0.37851 0.23221 0.73054 21.00000 0.07599 0.01291 0.03693 =
0.00039 0.00071 0.00106
PART 2
C1 1 0.29182 0.36521 0.81857 -21.00000 0.03294 0.02416 0.01991 =
0.00471 0.00625 0.00682
AFIX 22
H1b 2 0.34312 0.35590 0.91075 -21.00000 0.12335
H1a 2 0.15743 0.34627 0.81782 -21.00000 0.05324
AFIX 0
C00h 1 0.40497 0.30566 0.71726 -21.00000 0.01632 0.01899 0.02214 =
0.00074 0.00011 -0.00132
AFIX 22
H00k 2 0.37239 0.24166 0.73150 -21.00000 0.06128
H00l 2 0.54238 0.31292 0.73484 -21.00000 0.03050
AFIX 0
HKLF 4
END
Q1 1 -0.04 0.388889 0.916667 11 0.05 0.16
Q2 1 0.52 0.5 0.861111 11 0.05 0.16
Q3 1 0 0.185185 0.694444 11 0.05 0.16
Q4 1 0 0.462963 0.305556 11 0.05 0.15
Q5 1 0.02 0.5 0.583333 11 0.05 0.15
REM The information below was added by Olex2.
REM
REM R1 = 0.0214 for 2456 Fo > 4sig(Fo) and 0.0288 for all 2975 data
REM 258 parameters refined using 0 restraints
REM Highest difference peak 0.1588, deepest hole -0.2130
REM Mean Shift 0.0000, Max Shift 0.0003.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0288
REM R1_gt = 0.0214
REM wR_ref = 0.0483
REM GOOF = 1.0794
REM Shift_max = 0.0003
REM Shift_mean = 0.0000
REM Reflections_all = 2975
REM Reflections_gt = 2456
REM Parameters = 258
REM Hole = -0.2130
REM Peak = 0.1588
REM Flack = n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_Os_PBE
_database_code_depnum_ccdc_archive 'CCDC 2034388'
loop_
_audit_author_name
_audit_author_address
'Florian Kleemiss'
;University of Bern
Switzerland
;
_audit_update_record
;
2020-09-28 deposited with the CCDC. 2020-11-09 downloaded from the CCDC.
;
_audit_creation_date 2020-03-12
_audit_creation_method
;
Olex2 1.3-dev
(compiled 2020.03.04 svn.rc2590c38 for OlexSys, GUI svn.r6014)
;
_chemical_formula_moiety 'C24 H44 Os P2'
_chemical_formula_sum 'C24 H44 Os P2'
_chemical_formula_weight 584.789
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
_atom_type_scat_dispersion_source
H 0.00000 0.00000 NoSpherA2
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
C 0.00347 0.00161 NoSpherA2
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
Os -1.02940 7.59418 NoSpherA2
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
P 0.10434 0.09671 NoSpherA2
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
_vrf_PLAT974_Os_PBE
;
PROBLEM: Check Calcd Negative Resid. Density on Os -5.13 eA-3
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_vrf_PLAT910_Os_PBE
;
PROBLEM: Missing # of FCF Reflection(s) Below Theta(Min). 11 Note
RESPONSE: Reflections were affected by the Beamstop
;
_vrf_PLAT926_Os_PBE
;
PROBLEM: Reported and Calculated R1 Differ by ......... -0.0056 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_vrf_PLAT927_Os_PBE
;
PROBLEM: Reported and Calculated wR2 Differ by ......... -0.0105 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_vrf_PLAT928_Os_PBE
;
PROBLEM: Reported and Calculated S value Differ by . -0.380 Check
RESPONSE: Non-spherical refienment, therefore sattistics of ChecCIF are unreliable
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/n 1'
_space_group_name_Hall '-P 2ybc (x-z,y,z)'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x+1/2,y+1/2,-z+1/2
3 -x,-y,-z
4 x-1/2,-y-1/2,z-1/2
_symmetry_Int_Tables_number 14
_cell_length_a 10.8918(1)
_cell_length_b 13.7619(1)
_cell_length_c 17.0714(2)
_cell_angle_alpha 90
_cell_angle_beta 98.563(1)
_cell_angle_gamma 90
_cell_volume 2530.34(4)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 63613
_cell_measurement_temperature 120.00(10)
_cell_measurement_theta_max 36.3840
_cell_measurement_theta_min 3.5970
_exptl_absorpt_correction_T_max 1.000
_exptl_absorpt_correction_T_min 0.262
_exptl_absorpt_correction_type gaussian
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.7c (Rigaku Oxford Diffraction, 2015)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_coefficient_mu 5.176
_exptl_crystal_density_diffrn 1.535
_exptl_crystal_colour 'clear colourless'
_exptl_crystal_colour_lustre clear
_exptl_crystal_colour_modifier .
_exptl_crystal_colour_primary colourless
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_description block
_exptl_crystal_F_000 1176
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-3 -5 -2 0.1060
3 5 4 0.1078
-1 -1 5 0.0665
-3 -5 -4 0.1078
1 1 -5 0.0435
5 0 1 0.1557
-5 0 -1 0.1557
2 -5 -2 0.1561
-2 5 2 0.1561
3 5 2 0.1060
_exptl_crystal_size_max 0.39
_exptl_crystal_size_mid 0.212
_exptl_crystal_size_min 0.11
loop_
_exptl_oxdiff_crystal_face_indexfrac_h
_exptl_oxdiff_crystal_face_indexfrac_k
_exptl_oxdiff_crystal_face_indexfrac_l
_exptl_oxdiff_crystal_face_x
_exptl_oxdiff_crystal_face_y
_exptl_oxdiff_crystal_face_z
-3.0094 -5.0063 -1.9870 -0.3272 -0.0417 -0.0951
3.0116 5.0110 3.9860 0.3427 0.1235 0.1067
-0.9962 -0.9887 5.0010 -0.0336 0.2137 -0.0122
-3.0116 -5.0110 -3.9860 -0.3427 -0.1235 -0.1067
0.9962 0.9887 -5.0010 0.0336 -0.2137 0.0122
5.0045 0.0045 0.9853 0.1335 0.0246 0.3098
-5.0045 -0.0045 -0.9853 -0.1335 -0.0246 -0.3098
1.9940 -5.0041 -2.0012 -0.2015 -0.0580 0.2090
-1.9940 5.0041 2.0012 0.2015 0.0580 -0.2090
3.0094 5.0063 1.9870 0.3272 0.0417 0.0951
_diffrn_reflns_av_R_equivalents 0.0582
_diffrn_reflns_av_unetI/netI 0.0248
_diffrn_reflns_Laue_measured_fraction_full 0.9976
_diffrn_reflns_Laue_measured_fraction_max 0.9986
_diffrn_reflns_limit_h_max 18
_diffrn_reflns_limit_h_min -18
_diffrn_reflns_limit_k_max 23
_diffrn_reflns_limit_k_min -23
_diffrn_reflns_limit_l_max 29
_diffrn_reflns_limit_l_min -29
_diffrn_reflns_number 196209
_diffrn_reflns_point_group_measured_fraction_full 0.9976
_diffrn_reflns_point_group_measured_fraction_max 0.9986
_diffrn_reflns_theta_full 25.2417
_diffrn_reflns_theta_max 30.51
_diffrn_reflns_theta_min 3.51
_diffrn_measured_fraction_theta_full 0.9976
_diffrn_measured_fraction_theta_max 0.9986
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.71073
_reflns_Friedel_coverage 0.0
_reflns_limit_h_max 12
_reflns_limit_h_min -15
_reflns_limit_k_max 19
_reflns_limit_k_min 0
_reflns_limit_l_max 24
_reflns_limit_l_min -11
_reflns_number_gt 7199
_reflns_number_total 7723
_diffrn_ambient_environment N~2~
_diffrn_ambient_temperature 120.00(10)
_diffrn_detector 'CCD plate'
_diffrn_detector_area_resol_mean 8.0856
_diffrn_detector_type EosS2
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):
# Type Start End Width t~exp~ \w \q \k \f Frames
#--------------------------------------------------------------------------
1 \w 50.00 105.00 1.00 3.65 -- 36.08 159.00 95.00 55
2 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00 0.00 95
3 \w 19.00 103.00 1.00 3.65 -- 36.08 57.00-180.00 84
4 \w 35.00 108.00 1.00 3.65 -- 36.08 178.00 150.00 73
5 \w 35.00 108.00 1.00 3.65 -- 36.08 178.00 30.00 73
6 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00 60.00 95
7 \w -33.00 105.00 1.00 3.65 -- 36.08 0.00-180.00 138
8 \w -33.00 105.00 1.00 3.65 -- 36.08 0.00 60.00 138
9 \w -4.00 86.00 1.00 3.65 -- 36.08-118.00-143.00 90
10 \w 35.00 108.00 1.00 3.65 -- 36.08 178.00-150.00 73
11 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00-180.00 95
12 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00 -90.00 95
13 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00 120.00 95
14 \w 19.00 103.00 1.00 3.65 -- 36.08 57.00 -90.00 84
15 \w -99.00 -11.00 1.00 3.65 -- -30.00 -38.00 -30.00 88
16 \w -99.00 -11.00 1.00 3.65 -- -30.00 -38.00 150.00 88
17 \w -31.00 63.00 1.00 3.65 -- 36.08 -77.00 60.00 94
18 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00 -30.00 95
19 \w 35.00 108.00 1.00 3.65 -- 36.08 178.00 -30.00 73
20 \w 20.00 109.00 1.00 3.65 -- 36.08-159.00 63.00 89
21 \w -98.00 -3.00 1.00 3.65 -- -30.00 -77.00 150.00 95
22 \w -98.00 -3.00 1.00 3.65 -- -30.00 -77.00 30.00 95
23 \w -97.00 -13.00 1.00 3.65 -- -30.00 -57.00-150.00 84
24 \w -49.00 39.00 1.00 3.65 -- -30.00 38.00-120.00 88
25 \w -97.00 -19.00 1.00 3.65 -- -30.00 -57.00 30.00 78
26 \w 9.00 104.00 1.00 3.65 -- 36.08 77.00-150.00 95
;
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, EosS2'
_diffrn_measurement_method '\w scans'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11 0.0251251000
_diffrn_orient_matrix_UB_12 0.0472240000
_diffrn_orient_matrix_UB_13 0.0076280000
_diffrn_orient_matrix_UB_21 -0.0031394000
_diffrn_orient_matrix_UB_22 -0.0060278000
_diffrn_orient_matrix_UB_23 0.0409225000
_diffrn_orient_matrix_UB_31 0.0607998000
_diffrn_orient_matrix_UB_32 -0.0198267000
_diffrn_orient_matrix_UB_33 0.0057471000
_diffrn_radiation_monochromator mirror
_diffrn_radiation_probe x-ray
_diffrn_source 'micro-focus sealed X-ray tube'
_diffrn_source_type 'SuperNova (Mo) X-ray Source'
_reflns_Friedel_fraction_full .
_reflns_Friedel_fraction_max .
_reflns_special_details
;
Refinement using NoSpherA2, an implementation of
NOn-SPHERical Atom-form-factors in Olex2.
Please cite:
F. Kleemiss, H. Puschmann, O. Dolomanov, S.Grabowsky - to be publsihed - 2020
NoSpherA2 makes use of tailor-made aspherical atomic form factors calculated
on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from
spherical-atom form factors.
The ED is calculated from a gaussian basis set single determinant SCF
wavefunction - either Hartree-Fock or DFT
- for a fragment of the crystal embedded in
an electrostatic crystal field.
The following options were used:
SOFTWARE: ORCA
PARTITIONING: NoSpherA2
METHOD: PBE
INT ACCURACY: High
BASIS SET: x2c-TZVPP
CHARGE: 0
MULTIPLICITY: 1
DATE: 2020-03-13_12-39-10
;
_computing_cell_refinement 'CrysAlisPro 1.171.39.7c (Rigaku OD, 2015)'
_computing_data_collection 'CrysAlisPro 1.171.39.7c (Rigaku OD, 2015)'
_computing_data_reduction 'CrysAlisPro 1.171.39.7c (Rigaku OD, 2015)'
_computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)'
_computing_structure_solution 'olex2.solve (Bourhis et al., 2015)'
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_reflns_threshold_expression I>=2u(I)
_refine_diff_density_max 0.5047
_refine_diff_density_min -0.5003
_refine_diff_density_rms 0.0793
_refine_ls_d_res_high 0.7000
_refine_ls_d_res_low 5.7986
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_goodness_of_fit_ref 1.0722
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 636
_refine_ls_number_reflns 7723
_refine_ls_number_restraints 6
_refine_ls_R_factor_all 0.0143
_refine_ls_R_factor_gt 0.0119
_refine_ls_restrained_S_all 1.0717
_refine_ls_shift/su_max 0.0003
_refine_ls_shift/su_mean 0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0005P)^2^+0.2531P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0185
_refine_ls_wR_factor_ref 0.0189
_olex2_refinement_description
;
1. Rigid body (RIGU) restrains
H8, Os
with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
H7, Os
with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
;
_atom_sites_solution_primary dual
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
P002 P 0.64836(2) 0.598594(18) 0.200797(15) 0.01276(5) Uani 1.000000 . .
P003 P 0.33818(2) 0.406082(18) 0.268430(15) 0.01251(5) Uani 1.000000 . .
C004 C 0.37841(9) 0.32778(7) 0.35559(6) 0.0159(2) Uani 1.000000 . .
C005 C 0.30571(10) 0.31745(8) 0.18632(6) 0.0181(2) Uani 1.000000 . .
C006 C 0.76659(10) 0.65205(8) 0.27749(7) 0.0186(2) Uani 1.000000 . .
C007 C 0.61739(9) 0.69827(7) 0.12930(6) 0.0156(2) Uani 1.000000 . .
C008 C 0.73932(10) 0.51139(7) 0.14854(7) 0.0186(2) Uani 1.000000 . .
C009 C 0.33192(11) 0.23311(8) 0.35882(7) 0.0198(2) Uani 1.000000 . .
C00A C 0.25019(15) 0.36648(10) 0.10853(8) 0.0298(3) Uani 1.000000 . .
C00B C 0.50071(11) 0.70520(8) 0.08316(6) 0.0194(2) Uani 1.000000 . .
C00C C 0.18089(10) 0.45036(8) 0.28141(7) 0.0202(2) Uani 1.000000 . .
C00D C 0.82254(14) 0.57581(10) 0.33744(9) 0.0291(3) Uani 1.000000 . .
C00E C 0.70657(12) 0.76883(8) 0.11930(7) 0.0219(2) Uani 1.000000 . .
C00F C 0.45240(11) 0.36467(9) 0.42293(7) 0.0247(2) Uani 1.000000 . .
C00G C 0.66231(13) 0.47373(10) 0.07233(7) 0.0251(2) Uani 1.000000 . .
C00H C 0.67815(12) 0.84544(8) 0.06641(7) 0.0261(3) Uani 1.000000 . .
C00I C 0.71497(13) 0.73711(9) 0.32002(8) 0.0247(3) Uani 1.000000 . .
C00J C 0.56035(13) 0.85269(8) 0.02266(7) 0.0269(3) Uani 1.000000 . .
C00K C 0.07854(12) 0.37350(9) 0.26791(10) 0.0260(3) Uani 1.000000 . .
C00L C 0.35925(11) 0.17718(9) 0.42723(7) 0.0245(2) Uani 1.000000 . .
C00M C 0.42150(13) 0.25935(10) 0.17563(9) 0.0278(3) Uani 1.000000 . .
C00N C 0.18281(14) 0.49646(11) 0.36308(10) 0.0317(3) Uani 1.000000 . .
C00O C 0.47182(12) 0.78187(9) 0.03019(7) 0.0257(3) Uani 1.000000 . .
C00P C 0.43237(12) 0.21515(9) 0.49388(8) 0.0286(3) Uani 1.000000 . .
C00Q C 0.47864(13) 0.30928(10) 0.49169(8) 0.0321(3) Uani 1.000000 . .
C00R C 0.86358(13) 0.55063(10) 0.13037(10) 0.0305(3) Uani 1.000000 . .
H00i H 0.7977(13) 0.7668(10) 0.1537(10) 0.051(5) Uani 1.000000 . .
H00n H 0.7477(14) 0.8991(11) 0.0601(9) 0.055(5) Uani 1.000000 . .
H00r H 0.5389(15) 0.9150(11) -0.0163(9) 0.060(5) Uani 1.000000 . .
H00 H 0.3792(13) 0.7860(10) -0.0042(8) 0.043(4) Uani 1.000000 . .
H00d H 0.4313(12) 0.6524(10) 0.0907(8) 0.034(4) Uani 1.000000 . .
H00j H 0.4913(14) 0.4360(11) 0.4183(8) 0.047(4) Uani 1.000000 . .
H2 H 0.5331(15) 0.3405(12) 0.5426(9) 0.066(6) Uani 1.000000 . .
H1 H 0.4534(14) 0.1722(11) 0.5471(9) 0.055(5) Uani 1.000000 . .
H00v H 0.3237(14) 0.1037(11) 0.4283(9) 0.057(5) Uani 1.000000 . .
H009 H 0.2738(14) 0.2029(11) 0.3081(8) 0.051(5) Uani 1.000000 . .
H005 H 0.2356(11) 0.2665(9) 0.2034(8) 0.029(4) Uani 1.000000 . .
H006 H 0.8423(13) 0.6807(10) 0.2457(8) 0.037(4) Uani 1.000000 . .
H008 H 0.7590(13) 0.4513(9) 0.1912(8) 0.033(4) Uani 1.000000 . .
H00a H 0.1678(15) 0.4073(13) 0.1152(9) 0.058(5) Uani 1.000000 . .
H00b H 0.3184(16) 0.4138(13) 0.0868(9) 0.062(5) Uani 1.000000 . .
H00c H 0.2247(17) 0.3095(13) 0.0634(9) 0.071(6) Uani 1.000000 . .
H00e H 0.1614(12) 0.5072(10) 0.2369(9) 0.036(4) Uani 1.000000 . .
H00f H 0.7525(15) 0.5517(13) 0.3716(10) 0.063(6) Uani 1.000000 . .
H00g H 0.8557(16) 0.5129(11) 0.3095(11) 0.067(6) Uani 1.000000 . .
H00h H 0.8993(13) 0.6072(11) 0.3776(9) 0.052(5) Uani 1.000000 . .
H00k H 0.5767(15) 0.4401(11) 0.0827(9) 0.056(5) Uani 1.000000 . .
H00l H 0.6390(15) 0.5324(11) 0.0304(9) 0.050(5) Uani 1.000000 . .
H00m H 0.7176(14) 0.4190(11) 0.0458(9) 0.051(5) Uani 1.000000 . .
H00o H 0.6698(13) 0.7927(9) 0.2795(8) 0.039(4) Uani 1.000000 . .
H00p H 0.6476(14) 0.7139(11) 0.3562(10) 0.055(5) Uani 1.000000 . .
H00q H 0.7895(14) 0.7706(11) 0.3605(9) 0.051(5) Uani 1.000000 . .
H00s H 0.0615(14) 0.3480(13) 0.2074(10) 0.059(5) Uani 1.000000 . .
H00t H 0.1013(14) 0.3126(11) 0.3045(10) 0.052(5) Uani 1.000000 . .
H00u H -0.0087(14) 0.4036(12) 0.2813(11) 0.060(5) Uani 1.000000 . .
H00w H 0.4919(15) 0.3054(12) 0.1618(10) 0.062(5) Uani 1.000000 . .
H00x H 0.4586(15) 0.2209(12) 0.2296(9) 0.057(5) Uani 1.000000 . .
H00y H 0.3978(15) 0.2068(11) 0.1270(9) 0.058(5) Uani 1.000000 . .
H00z H 0.1983(16) 0.4412(13) 0.4095(10) 0.065(6) Uani 1.000000 . .
H H 0.2543(15) 0.5513(12) 0.3755(9) 0.052(5) Uani 1.000000 . .
Ha H 0.0915(15) 0.5301(12) 0.3639(10) 0.063(5) Uani 1.000000 . .
H3 H 0.8496(14) 0.6137(11) 0.0899(10) 0.055(5) Uani 1.000000 . .
Hb H 0.9257(13) 0.5718(12) 0.1823(10) 0.049(5) Uani 1.000000 . .
Hc H 0.9123(14) 0.4952(11) 0.1021(10) 0.056(5) Uani 1.000000 . .
Os Os 0.478328(4) 0.530020(3) 0.249003(2) 0.015000(14) Uani 1.000000 . U
H5 H 0.3928(18) 0.5758(15) 0.3067(12) 0.096(7) Uani 1.000000 . .
H9 H 0.5503(14) 0.5299(13) 0.3320(11) 0.077(6) Uani 1.000000 . .
H4 H 0.4857(12) 0.6435(10) 0.2649(8) 0.031(4) Uiso 1.000000 . .
H7 H 0.4600(14) 0.4824(10) 0.1673(8) 0.048(5) Uani 1.000000 . U
H8 H 0.5685(13) 0.4421(10) 0.2606(10) 0.053(5) Uani 1.000000 . U
H6 H 0.3709(12) 0.5782(11) 0.1905(9) 0.051(5) Uani 1.000000 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
P002 0.01163(12) 0.01058(11) 0.01601(13) -0.00101(9) 0.00192(10) 0.00060(9)
P003 0.01181(12) 0.01112(11) 0.01491(12) -0.00065(9) 0.00306(10) 0.00021(9)
C004 0.0152(5) 0.0151(5) 0.0175(5) -0.0017(4) 0.0032(4) 0.0024(4)
C005 0.0210(6) 0.0163(5) 0.0173(5) -0.0033(4) 0.0039(4) -0.0021(4)
C006 0.0159(5) 0.0156(5) 0.0228(6) -0.0000(4) -0.0018(4) -0.0008(4)
C007 0.0162(5) 0.0131(4) 0.0177(5) -0.0010(4) 0.0030(4) 0.0013(4)
C008 0.0198(6) 0.0144(5) 0.0228(6) 0.0009(4) 0.0068(4) -0.0003(4)
C009 0.0221(6) 0.0167(5) 0.0208(6) -0.0018(4) 0.0036(5) 0.0044(4)
C00A 0.0370(8) 0.0325(7) 0.0180(6) -0.0110(6) -0.0023(6) 0.0015(5)
C00B 0.0206(6) 0.0195(5) 0.0173(5) 0.0001(4) 0.0000(4) 0.0028(4)
C00C 0.0140(5) 0.0158(5) 0.0318(7) 0.0014(4) 0.0064(5) 0.0007(4)
C00D 0.0274(7) 0.0248(7) 0.0308(7) 0.0045(5) -0.0093(6) 0.0009(5)
C00E 0.0233(6) 0.0162(5) 0.0264(6) -0.0050(4) 0.0043(5) 0.0042(4)
C00F 0.0290(7) 0.0244(6) 0.0188(6) -0.0079(5) -0.0020(5) 0.0028(5)
C00G 0.0309(7) 0.0241(6) 0.0222(6) -0.0010(5) 0.0096(5) -0.0056(5)
C00H 0.0377(7) 0.0157(5) 0.0262(6) -0.0049(5) 0.0091(5) 0.0049(5)
C00I 0.0260(7) 0.0192(6) 0.0270(7) 0.0000(5) -0.0022(5) -0.0074(5)
C00J 0.0445(8) 0.0180(5) 0.0181(6) 0.0020(5) 0.0043(5) 0.0042(4)
C00K 0.0149(6) 0.0212(6) 0.0427(8) -0.0022(5) 0.0071(6) 0.0004(6)
C00L 0.0266(6) 0.0210(6) 0.0267(6) 0.0014(5) 0.0066(5) 0.0099(5)
C00M 0.0307(7) 0.0226(6) 0.0332(7) 0.0001(5) 0.0149(6) -0.0074(5)
C00N 0.0257(7) 0.0288(7) 0.0447(9) -0.0016(6) 0.0188(6) -0.0121(6)
C00O 0.0327(7) 0.0250(6) 0.0180(6) 0.0027(5) -0.0010(5) 0.0053(5)
C00P 0.0299(7) 0.0329(7) 0.0228(6) 0.0011(5) 0.0037(5) 0.0127(5)
C00Q 0.0373(8) 0.0363(7) 0.0198(6) -0.0070(6) -0.0053(5) 0.0077(5)
C00R 0.0211(7) 0.0262(7) 0.0473(9) 0.0007(5) 0.0155(6) -0.0032(6)
H00i 0.036(10) 0.033(10) 0.080(13) -0.010(8) -0.002(9) 0.013(9)
H00n 0.060(12) 0.040(10) 0.062(12) -0.025(9) 0.005(9) 0.011(9)
H00r 0.098(14) 0.040(11) 0.042(11) 0.008(10) 0.006(10) 0.016(9)
H00 0.030(9) 0.051(11) 0.042(10) 0.018(8) -0.014(8) 0.001(8)
H00d 0.022(8) 0.030(9) 0.049(10) -0.007(7) 0.010(7) -0.005(8)
H00j 0.066(12) 0.035(10) 0.031(10) -0.009(9) -0.018(8) -0.001(8)
H2 0.080(14) 0.064(12) 0.042(11) -0.021(10) -0.030(10) 0.009(10)
H1 0.056(11) 0.066(12) 0.045(11) 0.017(9) 0.013(9) 0.042(10)
H00v 0.061(12) 0.039(11) 0.067(13) -0.008(9) -0.002(9) 0.009(10)
H009 0.072(12) 0.053(11) 0.026(10) -0.022(9) 0.001(9) -0.009(8)
H005 0.025(9) 0.021(8) 0.041(10) -0.001(7) 0.009(7) -0.018(7)
H006 0.040(10) 0.036(10) 0.036(10) 0.015(8) 0.009(8) -0.004(8)
H008 0.051(10) 0.017(8) 0.036(9) 0.015(7) 0.021(8) 0.012(7)
H00a 0.053(12) 0.073(14) 0.048(12) 0.007(11) 0.006(9) -0.004(10)
H00b 0.072(13) 0.072(13) 0.040(11) -0.033(11) 0.003(10) 0.023(10)
H00c 0.099(15) 0.083(14) 0.026(10) -0.029(12) -0.004(10) -0.027(10)
H00e 0.026(9) 0.032(9) 0.049(11) -0.004(7) 0.003(7) 0.015(8)
H00f 0.042(11) 0.078(14) 0.068(14) -0.016(10) 0.006(10) 0.042(11)
H00g 0.075(14) 0.033(11) 0.085(15) 0.018(10) -0.012(11) -0.017(10)
H00h 0.035(10) 0.064(12) 0.046(11) -0.005(9) -0.026(8) 0.002(9)
H00k 0.061(12) 0.059(12) 0.049(12) -0.036(10) 0.009(10) -0.010(9)
H00l 0.071(13) 0.040(10) 0.038(11) -0.000(9) 0.001(9) 0.003(9)
H00m 0.064(12) 0.042(10) 0.051(11) 0.012(9) 0.023(9) -0.015(9)
H00o 0.059(11) 0.015(8) 0.039(10) 0.014(8) -0.006(8) -0.003(7)
H00p 0.048(11) 0.058(12) 0.067(13) -0.009(9) 0.037(10) -0.023(10)
H00q 0.053(11) 0.043(11) 0.053(12) -0.013(9) -0.006(9) -0.020(9)
H00s 0.035(11) 0.081(14) 0.058(13) -0.008(9) 0.000(9) -0.019(11)
H00t 0.048(11) 0.033(10) 0.076(14) -0.018(8) 0.008(9) 0.002(10)
H00u 0.026(10) 0.051(12) 0.104(16) -0.006(9) 0.015(10) -0.009(11)
H00w 0.057(12) 0.047(11) 0.092(15) -0.001(9) 0.048(11) -0.002(10)
H00x 0.067(13) 0.065(13) 0.039(11) 0.043(10) 0.007(9) 0.016(10)
H00y 0.079(13) 0.047(11) 0.054(12) -0.024(10) 0.031(10) -0.039(10)
H00z 0.085(15) 0.066(14) 0.046(12) 0.008(11) 0.021(10) 0.014(11)
H 0.048(11) 0.070(13) 0.045(11) -0.018(10) 0.027(9) -0.024(10)
Ha 0.055(12) 0.059(12) 0.088(15) 0.019(10) 0.051(11) -0.001(11)
H3 0.052(12) 0.037(11) 0.087(14) 0.011(9) 0.048(10) 0.022(10)
Hb 0.017(9) 0.076(13) 0.057(12) -0.013(8) 0.018(8) -0.029(10)
Hc 0.045(11) 0.048(11) 0.081(14) 0.010(9) 0.032(10) -0.018(10)
Os 0.01480(2) 0.01244(2) 0.01854(2) -0.002938(15) 0.005066(15) 0.000255(16)
H5 0.091(16) 0.098(17) 0.118(19) -0.010(13) 0.075(15) -0.035(15)
H9 0.033(11) 0.109(17) 0.086(15) -0.035(11) -0.005(10) 0.006(13)
H7 0.070(12) 0.037(9) 0.040(6) -0.043(8) 0.019(5) -0.011(4)
H8 0.045(9) 0.038(8) 0.084(14) 0.012(4) 0.038(8) 0.030(7)
H6 0.034(10) 0.050(11) 0.071(13) 0.004(8) 0.014(9) 0.025(10)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P002 C006 1.8470(11) . ?
P002 C007 1.8337(10) . ?
P002 C008 1.8657(11) . ?
P002 Os 2.3348(3) . ?
P003 C004 1.8366(10) . ?
P003 C005 1.8520(11) . ?
P003 C00C 1.8624(11) . ?
P003 Os 2.3452(3) . ?
C004 C009 1.4019(14) . ?
C004 C00F 1.3973(15) . ?
C005 C00A 1.5315(17) . ?
C005 C00M 1.5270(17) . ?
C005 H005 1.108(13) . ?
C006 C00D 1.5277(16) . ?
C006 C00I 1.5281(16) . ?
C006 H006 1.123(14) . ?
C007 C00B 1.3952(15) . ?
C007 C00E 1.4018(14) . ?
C008 C00G 1.5297(16) . ?
C008 C00R 1.5311(17) . ?
C008 H008 1.101(12) . ?
C009 C00L 1.3934(15) . ?
C009 H009 1.077(14) . ?
C00A H00a 1.079(17) . ?
C00A H00b 1.094(15) . ?
C00A H00c 1.105(15) . ?
C00B C00O 1.3947(15) . ?
C00B H00d 1.070(13) . ?
C00C C00K 1.5290(16) . ?
C00C C00N 1.5291(18) . ?
C00C H00e 1.089(13) . ?
C00D H00f 1.080(16) . ?
C00D H00g 1.076(16) . ?
C00D H00h 1.089(14) . ?
C00E C00H 1.3925(16) . ?
C00E H00i 1.076(14) . ?
C00F C00Q 1.3931(16) . ?
C00F H00j 1.077(14) . ?
C00G H00k 1.078(15) . ?
C00G H00l 1.083(15) . ?
C00G H00m 1.103(14) . ?
C00H C00J 1.3888(18) . ?
C00H H00n 1.075(14) . ?
C00I H00o 1.098(13) . ?
C00I H00p 1.076(15) . ?
C00I H00q 1.088(14) . ?
C00J C00O 1.3903(17) . ?
C00J H00r 1.089(14) . ?
C00K H00s 1.081(17) . ?
C00K H00t 1.054(16) . ?
C00K H00u 1.092(16) . ?
C00L C00P 1.3901(18) . ?
C00L H00v 1.084(15) . ?
C00M H00w 1.048(16) . ?
C00M H00x 1.088(15) . ?
C00M H00y 1.102(14) . ?
C00N H00z 1.093(17) . ?
C00N H 1.083(16) . ?
C00N Ha 1.099(15) . ?
C00O H00 1.090(13) . ?
C00P C00Q 1.3925(18) . ?
C00P H1 1.079(13) . ?
C00Q H2 1.067(15) . ?
C00R H3 1.106(16) . ?
C00R Hb 1.072(15) . ?
C00R Hc 1.083(15) . ?
Os H5 1.584(16) . ?
Os H9 1.513(17) . ?
Os H4 1.585(14) . ?
Os H7 1.527(14) . ?
Os H8 1.553(14) . ?
Os H6 1.568(14) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C007 P002 C006 102.34(5) . . ?
C008 P002 C006 103.37(5) . . ?
C008 P002 C007 102.77(5) . . ?
Os P002 C006 114.65(4) . . ?
Os P002 C007 117.39(3) . . ?
Os P002 C008 114.46(3) . . ?
C005 P003 C004 102.85(5) . . ?
C00C P003 C004 102.02(5) . . ?
C00C P003 C005 103.31(5) . . ?
Os P003 C004 117.35(3) . . ?
Os P003 C005 115.27(4) . . ?
Os P003 C00C 114.11(3) . . ?
C009 C004 P003 122.21(8) . . ?
C00F C004 P003 119.48(8) . . ?
C00F C004 C009 118.22(10) . . ?
C00A C005 P003 111.87(8) . . ?
C00M C005 P003 111.55(8) . . ?
C00M C005 C00A 110.70(11) . . ?
H005 C005 P003 106.2(6) . . ?
H005 C005 C00A 108.0(7) . . ?
H005 C005 C00M 108.3(6) . . ?
C00D C006 P002 111.58(8) . . ?
C00I C006 P002 112.02(8) . . ?
C00I C006 C00D 110.25(11) . . ?
H006 C006 P002 106.3(7) . . ?
H006 C006 C00D 108.4(7) . . ?
H006 C006 C00I 108.0(7) . . ?
C00B C007 P002 119.26(8) . . ?
C00E C007 P002 122.49(8) . . ?
C00E C007 C00B 118.25(10) . . ?
C00G C008 P002 111.20(8) . . ?
C00R C008 P002 114.73(8) . . ?
C00R C008 C00G 109.67(11) . . ?
H008 C008 P002 103.4(7) . . ?
H008 C008 C00G 109.6(7) . . ?
H008 C008 C00R 108.0(7) . . ?
C00L C009 C004 120.86(11) . . ?
H009 C009 C004 120.0(8) . . ?
H009 C009 C00L 119.2(8) . . ?
H00a C00A C005 111.4(9) . . ?
H00b C00A C005 110.8(8) . . ?
H00b C00A H00a 110.1(13) . . ?
H00c C00A C005 108.5(9) . . ?
H00c C00A H00a 108.5(12) . . ?
H00c C00A H00b 107.4(12) . . ?
C00O C00B C007 121.09(11) . . ?
H00d C00B C007 119.1(7) . . ?
H00d C00B C00O 119.7(7) . . ?
C00K C00C P003 114.75(8) . . ?
C00N C00C P003 110.88(9) . . ?
C00N C00C C00K 109.58(11) . . ?
H00e C00C P003 103.8(7) . . ?
H00e C00C C00K 109.2(7) . . ?
H00e C00C C00N 108.3(8) . . ?
H00f C00D C006 109.3(9) . . ?
H00g C00D C006 112.5(9) . . ?
H00g C00D H00f 107.6(13) . . ?
H00h C00D C006 110.0(8) . . ?
H00h C00D H00f 108.7(12) . . ?
H00h C00D H00g 108.7(12) . . ?
C00H C00E C007 120.82(11) . . ?
H00i C00E C007 121.0(8) . . ?
H00i C00E C00H 118.2(8) . . ?
C00Q C00F C004 121.01(11) . . ?
H00j C00F C004 117.1(7) . . ?
H00j C00F C00Q 121.8(7) . . ?
H00k C00G C008 112.5(8) . . ?
H00l C00G C008 110.7(8) . . ?
H00l C00G H00k 107.7(12) . . ?
H00m C00G C008 108.5(8) . . ?
H00m C00G H00k 108.3(11) . . ?
H00m C00G H00l 109.0(11) . . ?
C00J C00H C00E 120.09(11) . . ?
H00n C00H C00E 119.6(8) . . ?
H00n C00H C00J 120.4(8) . . ?
H00o C00I C006 113.4(7) . . ?
H00p C00I C006 112.1(8) . . ?
H00p C00I H00o 106.8(11) . . ?
H00q C00I C006 109.5(8) . . ?
H00q C00I H00o 109.1(11) . . ?
H00q C00I H00p 105.6(12) . . ?
C00O C00J C00H 119.86(11) . . ?
H00r C00J C00H 118.8(9) . . ?
H00r C00J C00O 121.3(9) . . ?
H00s C00K C00C 112.7(9) . . ?
H00t C00K C00C 111.1(8) . . ?
H00t C00K H00s 107.5(12) . . ?
H00u C00K C00C 110.1(8) . . ?
H00u C00K H00s 107.0(12) . . ?
H00u C00K H00t 108.2(12) . . ?
C00P C00L C009 120.22(11) . . ?
H00v C00L C009 119.8(8) . . ?
H00v C00L C00P 120.0(8) . . ?
H00w C00M C005 110.8(9) . . ?
H00x C00M C005 111.3(8) . . ?
H00x C00M H00w 107.0(13) . . ?
H00y C00M C005 109.2(9) . . ?
H00y C00M H00w 108.9(12) . . ?
H00y C00M H00x 109.6(12) . . ?
H00z C00N C00C 110.6(9) . . ?
H C00N C00C 112.3(8) . . ?
H C00N H00z 108.3(13) . . ?
Ha C00N C00C 107.3(10) . . ?
Ha C00N H00z 109.0(12) . . ?
Ha C00N H 109.2(12) . . ?
C00J C00O C00B 119.84(12) . . ?
H00 C00O C00B 119.3(8) . . ?
H00 C00O C00J 120.8(8) . . ?
C00Q C00P C00L 119.56(11) . . ?
H1 C00P C00L 120.4(9) . . ?
H1 C00P C00Q 120.0(9) . . ?
C00P C00Q C00F 120.13(12) . . ?
H2 C00Q C00F 119.1(9) . . ?
H2 C00Q C00P 120.8(9) . . ?
H3 C00R C008 111.1(8) . . ?
Hb C00R C008 113.4(8) . . ?
Hb C00R H3 108.3(12) . . ?
Hc C00R C008 110.4(8) . . ?
Hc C00R H3 107.8(12) . . ?
Hc C00R Hb 105.6(12) . . ?
P003 Os P002 155.635(9) . . ?
H5 Os P002 129.0(7) . . ?
H5 Os P003 75.3(7) . . ?
H9 Os P002 90.2(6) . . ?
H9 Os P003 97.1(6) . . ?
H9 Os H5 71.9(10) . . ?
H4 Os P002 68.9(5) . . ?
H4 Os P003 135.2(5) . . ?
H4 Os H5 61.4(8) . . ?
H4 Os H9 80.5(8) . . ?
H7 Os P002 81.6(5) . . ?
H7 Os P003 79.5(5) . . ?
H7 Os H5 136.9(10) . . ?
H7 Os H9 146.4(10) . . ?
H7 Os H4 125.2(7) . . ?
H8 Os P002 80.8(5) . . ?
H8 Os P003 80.1(5) . . ?
H8 Os H5 130.6(10) . . ?
H8 Os H9 69.5(9) . . ?
H8 Os H4 137.0(8) . . ?
H8 Os H7 77.0(9) . . ?
H6 Os P002 99.2(5) . . ?
H6 Os P003 87.6(5) . . ?
H6 Os H5 77.1(9) . . ?
H6 Os H9 146.1(10) . . ?
H6 Os H4 73.0(7) . . ?
H6 Os H7 67.4(8) . . ?
H6 Os H8 144.0(9) . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P002 C007 C00B C00O 177.61(9) . . . . ?
P002 C007 C00E C00H -177.68(9) . . . . ?
P003 C004 C009 C00L -176.83(9) . . . . ?
P003 C004 C00F C00Q 176.17(10) . . . . ?
C004 C009 C00L C00P 0.69(13) . . . . ?
C004 C00F C00Q C00P 0.83(15) . . . . ?
C007 C00B C00O C00J 0.24(13) . . . . ?
C007 C00E C00H C00J -0.07(13) . . . . ?
C009 C00L C00P C00Q -0.32(14) . . . . ?
C00B C00O C00J C00H 1.64(14) . . . . ?
C00E C00H C00J C00O -1.72(14) . . . . ?
C00F C00Q C00P C00L -0.43(16) . . . . ?
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
0 -23 0 12.79 10.55
0 -23 -1 -5.38 10.19
0 -23 1 -7.16 9.79
0 -23 -2 5.57 8.85
0 -23 2 21.89 11.24
0 -23 3 36.5 13.54
0 -23 -3 20.93 11.45
0 -23 -4 3.74 8.99
0 -23 4 11.7 8.86
0 -23 -5 -0.85 8.19
0 -22 0 3.62 11.39
0 -22 0 27.85 11.16
0 -22 -1 201.31 36.54
0 -22 1 130.21 30.31
0 -22 1 136.19 23.75
0 -22 -1 131.79 23.45
0 -22 2 26.62 17.91
0 -22 -2 49.27 19.88
0 -22 2 43.02 14.99
0 -22 -2 18.82 11.1
0 -22 -3 212.38 36.48
0 -22 3 196.41 33.8
0 -22 -3 214.38 29.49
0 -22 3 191.5 27.77
0 -22 -4 47.62 20.51
0 -22 4 83.58 22.72
0 -22 -4 54.76 15.27
0 -22 4 37.18 14.07
0 -22 -5 289.6 41.01
0 -22 5 250.69 36.34
0 -22 -5 269.71 33.83
0 -22 5 271.11 32.53
0 -22 6 97.45 23.37
0 -22 -6 55.2 20.28
0 -22 6 82.88 19.55
0 -22 -6 65.49 18.65
0 -22 -7 268.77 38.42
0 -22 7 260.84 36.91
0 -22 7 206.56 28.71
0 -22 -7 241.34 32.77
0 -22 -8 76.1 20.61
0 -22 8 73.39 20.3
0 -22 -8 52.64 17.22
0 -22 8 69.94 17.67
0 -22 9 187.98 32.22
0 -22 9 174.29 26.12
0 -22 -9 215.99 31.71
0 -21 0 -1.58 10.46
0 -21 0 -0.66 9
0 -21 0 -0.09 8.18
0 -21 -1 -6.48 8.8
0 -21 1 -4.52 11.29
0 -21 1 -7.88 9.07
0 -21 -1 6.55 9.31
0 -21 2 19.57 11.21
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-1 11 8 243.69 20.75
1 11 -8 268.74 23.56
-1 11 8 253.51 23.11
1 11 -8 273.75 21.18
1 11 -8 237.48 21.54
1 11 -8 238.12 19.95
-1 11 8 234.65 21.58
1 11 -7 1345.55 52.07
-1 11 7 1300.56 51.14
1 11 -7 1317.54 51.26
1 11 -7 1311.23 50.08
-1 11 7 1112.93 48.66
-1 11 7 1164.58 52.66
-1 11 7 1262.83 50.02
1 11 -7 1399.7 55.74
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1 11 -7 1286.81 52.78
1 11 -7 1307.32 50.45
-1 11 7 1256.74 52.87
1 11 -6 496.85 29.81
1 11 -6 542.34 30.8
-1 11 6 531.47 30.2
1 11 -6 554.02 30.32
-1 11 6 533.72 30.3
-1 11 6 462.48 30.83
-1 11 6 573.59 31.48
1 11 -6 555.2 32.71
-1 11 6 541.42 33.1
1 11 -6 501.15 22.84
1 11 -6 548.37 31.47
1 11 -6 564.27 30.7
-1 11 6 532.09 31.82
1 11 -5 864.17 39.63
-1 11 5 844.87 39.13
1 11 -5 876.89 39.71
1 11 -5 892.73 39.17
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1 11 -5 813.47 39.95
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1 11 -5 886.28 31.74
1 11 -5 891.09 40.23
1 11 -5 820.67 38.18
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1 11 -4 407.04 25.85
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1 11 -4 438.08 27.04
-1 11 4 443.01 26.41
1 11 -4 413.83 25.58
-1 11 4 400.58 27.41
1 11 -4 472.02 28.56
-1 11 4 448.89 26.6
1 11 -4 398.11 20.83
-1 11 4 406.37 26.72
1 11 -4 398.87 25.44
1 11 -4 414.74 26.03
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1 11 -3 854.75 38.44
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1 11 -3 890.14 40.13
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1 11 -3 828.54 32.98
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1 11 -3 898.17 38.44
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1 11 -3 875.65 39.93
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1 11 -3 845.62 38.93
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1 11 -3 841.4 38.86
1 11 -2 552.73 29.5
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1 11 -2 575.72 30.96
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1 11 -2 551.17 26.39
1 11 -2 536.46 28.4
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1 11 -2 528.84 30.07
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1 11 -2 565.35 30.8
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1 11 -2 587.44 31.13
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1 11 -1 1747.93 58.74
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1 11 -1 1797.99 60.07
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1 11 -1 1611.39 53.85
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1 11 -1 1767.23 56.35
1 11 -1 1776.99 61.08
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1 11 -1 1814.71 61.31
1 11 -1 1776.03 60.64
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1 11 0 79.52 11.11
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1 11 0 84.9 11.41
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1 11 0 86.56 11.61
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1 11 0 84.62 10.69
1 11 0 90.83 10.49
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1 11 0 93.51 12.78
-1 11 0 88.77 12
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1 11 0 73.45 10.87
1 11 0 90.11 12.55
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1 11 1 1906.55 61.07
1 11 1 1727.97 59.04
1 11 1 1801.13 60.22
-1 11 -1 1822.53 61
-1 11 -1 1762.36 57.23
1 11 1 1717.71 58.15
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1 11 1 1830.99 55.18
1 11 1 1740.09 61.68
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1 11 1 1900.7 63.63
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1 11 1 1817.79 62.09
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-1 11 -2 61.29 10.79
1 11 2 67.47 11.13
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1 11 2 47.27 8.98
1 11 2 59.76 9.73
1 11 2 45.73 8.45
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1 11 2 52.61 9.41
1 11 2 48.78 7.37
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1 11 2 68.37 11.13
-1 11 -3 1871.33 60.66
1 11 3 1870.73 65.06
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1 11 3 2021.38 63.56
1 11 3 1727.02 61.03
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1 11 3 1929.52 61.55
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1 11 3 1695.26 62.04
-1 11 -3 1912.13 62.69
1 11 3 1889.28 54.69
-1 11 -3 1952.55 64.15
1 11 3 1877.04 65.67
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1 11 4 36.62 8.51
-1 11 -4 26.89 7.89
1 11 4 47.33 9.27
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1 11 4 34.91 8.28
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1 11 4 38.13 8.27
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1 11 4 20.32 5.99
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1 11 4 39.17 9.66
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1 11 5 1207.38 50.69
1 11 5 1247.87 48.25
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1 11 5 1225.71 49.13
1 11 5 1190.03 46.34
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1 11 5 1139.96 50.02
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1 11 5 1307.1 52.97
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1 11 6 381.96 26.97
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1 11 6 351.15 24.61
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1 11 6 317.24 24.13
1 11 6 384.97 24.59
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1 11 6 369.62 27.1
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1 11 6 402.1 28.29
-1 11 -7 1001.66 43.49
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1 11 7 1002.78 46.87
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1 11 7 981.07 45.72
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1 11 7 1030.04 48.96
1 11 8 81.5 13.39
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1 11 8 79.57 9.11
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1 11 8 88.5 13.07
1 11 8 89.44 12.12
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1 11 8 66.15 11.82
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1 11 8 79.79 12.77
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1 11 10 96.53 11.19
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1 11 10 102.87 13.86
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1 11 10 116.77 16.9
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1 11 12 248.34 24.98
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1 11 12 268.37 25.15
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1 11 12 250.44 19.18
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1 11 13 427.59 33.1
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1 11 13 457.73 27.61
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1 11 14 220.41 23.85
1 11 14 172.32 17.66
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1 11 15 337.73 25.89
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1 13 -20 224.27 29.59
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1 15 -11 48.23 13.97
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1 15 -11 63.58 13.7
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1 15 -11 68.95 14.3
1 15 -11 42.02 11.58
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1 15 -10 545.46 35.83
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1 15 -10 549 41.17
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1 15 -10 491.86 36.12
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1 15 -10 536.22 37.67
1 15 -10 531.19 36.21
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1 15 -9 140.3 18.02
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1 15 -9 132.21 19.76
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1 15 -9 98.89 15.76
1 15 -9 123.93 18.68
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1 15 -8 418.36 30.87
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1 15 -8 376.26 32.31
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1 15 -8 403.76 31.59
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1 15 -8 419.99 32.49
1 15 -8 418.22 31.65
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1 15 -7 43.92 11.91
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1 15 -6 344.67 30.53
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1 15 -6 400.32 30.82
1 15 -6 426.11 31.62
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1 15 -5 104 15.99
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2 14 13 2.32 6
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2 14 14 259.74 27.54
2 14 14 198.41 26.21
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2 14 14 234.94 27.88
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2 14 16 161.32 22.36
2 14 16 161.94 24.9
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2 14 16 154.24 23.33
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2 14 17 23.52 11.73
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2 14 17 22.09 10.42
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2 14 18 67.49 14.77
2 14 18 95.86 20.27
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2 14 18 98.64 19.46
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3 5 -5 1972.31 50.6
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3 5 -5 2075.18 41.1
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3 5 -5 1995.31 53.16
3 5 -5 2010.51 56.01
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3 5 -4 2017.45 51.5
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3 5 6 993.64 31.15
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3 10 16 98.61 16
3 10 16 116.71 18.48
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3 10 16 122.17 19.17
3 10 16 104.1 15.03
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3 10 17 4.1 5.96
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3 10 18 70.56 14.57
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3 10 20 134.57 21.17
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3 10 20 140.37 20.46
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3 10 24 20.92 11
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3 11 -25 64 16.07
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3 11 -24 13.78 11.14
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3 11 -23 179.66 25.97
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3 11 -22 60.74 13.8
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3 11 -20 81.92 16.52
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3 11 -20 79.91 17.16
3 11 -20 93.31 16.07
3 11 -20 84.04 18.81
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3 11 -19 267.67 28.97
3 11 -19 241.43 27.54
3 11 -19 212.84 23.3
3 11 -19 243.18 24.14
3 11 -19 298.76 32.95
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3 11 -18 94.77 19.25
3 11 -18 104.39 18.15
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3 11 -18 89.13 15.12
3 11 -18 135.65 18.4
3 11 -18 120.78 19.73
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3 11 -17 405.89 38.43
3 11 -17 403.5 34.03
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3 11 -17 438.42 35.27
3 11 -17 361.12 28.46
3 11 -17 387.16 29.98
3 11 -17 442.32 38.06
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3 11 -16 83.68 17.58
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3 11 -16 110.29 17.53
3 11 -16 116.94 17.21
3 11 -16 105.55 15.8
3 11 -16 82.14 12.93
3 11 -16 92.42 17.56
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3 11 -15 746.94 49.1
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3 11 -15 595.94 39.86
3 11 -15 638.59 40.77
3 11 -15 691.22 39.11
3 11 -15 653.35 38.33
3 11 -15 675.99 45.28
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3 11 -14 84.47 15.75
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3 11 -14 74.36 16.13
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3 11 -14 119.32 17.19
3 11 -14 69.68 13.18
3 11 -14 81.08 12.6
3 11 -14 73.43 12.84
3 11 -14 60.96 11.32
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3 11 -13 879.01 49.49
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3 11 -12 45.45 11.85
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3 11 -12 42.04 10.67
3 11 -12 51.8 12.36
3 11 -12 43.71 9.26
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3 11 -12 39.5 9.67
3 11 -12 42.58 9.31
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3 11 -11 1013.03 52.56
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3 11 -10 134.4 18.01
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3 11 -10 147.53 17.3
3 11 -10 148.56 16.42
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3 11 -10 166.94 16.68
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3 11 -6 630.03 35.75
3 11 -6 629.04 23.37
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3 11 -6 629.68 33.83
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3 11 -6 610.57 31.8
3 11 -6 635.09 34.68
3 11 -6 619.21 34.67
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-3 11 5 1885.67 69.68
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3 11 -5 1857.7 51.23
3 11 -5 1870.5 65.53
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3 11 -5 1824.37 63.83
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3 11 -5 1923.59 62.96
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3 11 -5 1946.83 65.22
3 11 -5 1872.96 65.73
3 11 -4 573.69 32.98
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3 11 -4 619.56 33.91
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3 11 -4 559.8 25.03
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3 11 -4 603.99 33.19
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3 11 -4 579.93 31.34
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3 11 -3 926.29 41.99
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3 11 -3 958.43 42.2
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3 11 -3 912.81 42.13
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3 11 -3 930.93 40.42
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3 11 10 124.09 16.21
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3 11 14 74.82 15.56
3 11 14 71.45 11.91
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3 11 15 244.06 25.05
3 11 15 229.98 26.49
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3 11 15 222.47 25.5
3 11 15 242.72 21.76
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3 11 16 125.48 19.38
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3 11 17 160.95 20.84
3 11 17 174.9 24.72
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3 11 18 107.06 17.8
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3 11 19 108.13 19.56
3 11 19 91.31 18.57
3 11 19 151.58 22.28
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3 11 20 53.04 14.59
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3 11 20 45.81 13.17
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3 11 21 86.48 18.86
3 11 21 84.98 17.91
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3 11 21 86.88 17.14
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3 11 22 10.23 11.1
3 11 22 5.28 6.44
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3 11 23 82.34 18.08
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3 12 -24 6.22 7.58
3 12 -24 5.69 7.68
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3 12 -23 12.09 9.69
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3 12 -22 14.65 8.52
3 12 -22 54.66 16.46
3 12 -22 24.62 11.8
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3 12 -21 32.93 14.25
3 12 -21 10.63 8.32
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3 12 -21 21.87 8.28
3 12 -21 27.34 11.16
3 12 -21 28.61 10.43
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3 12 -20 13.86 7.48
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3 12 -20 21.99 9.58
3 12 -20 22.18 10.87
3 12 -20 36.19 13.28
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3 12 -19 58.71 16.18
3 12 -19 50.56 14.38
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3 12 -19 32.63 10.53
3 12 -19 52.86 12.35
3 12 -19 56.19 14.54
3 12 -19 58.49 14.51
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3 12 -18 12.7 9.48
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3 12 -18 11.91 6.65
3 12 -18 9.48 6.3
3 12 -18 19.03 10.79
3 12 -18 22.73 10.53
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3 12 -17 84.83 19.35
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3 12 -17 60.51 14.08
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3 12 -17 99.26 15.49
3 12 -17 77.37 14.76
3 12 -17 79.68 17.43
3 12 -17 88.42 16.79
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4 12 -19 136.14 19.76
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4 13 -14 23 9.77
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4 13 -14 20.07 9.41
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4 13 -5 305.23 25.86
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4 13 -5 306.46 26.67
-4 13 5 324.06 25.74
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4 13 -5 260.2 23.7
4 13 -5 316.26 26.8
-4 13 5 297.74 19.94
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4 13 -4 343.71 25.34
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4 13 -4 339.37 27.16
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4 13 -4 355.59 28.37
4 13 -4 305.74 25.85
-4 13 4 349.57 25.38
-4 13 4 340.6 21.15
4 13 -4 367.01 28.6
4 13 -4 315.57 25.13
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-4 13 3 187.16 21.23
4 13 -3 208.01 20.7
-4 13 3 215.62 21.22
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4 13 -3 234.96 22.49
4 13 -3 171.48 19.36
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4 13 -3 230.8 21.17
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4 13 -2 324.52 26.43
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4 13 -2 367.1 28.61
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4 13 -1 242.78 23.73
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4 13 0 376.2 26.66
-4 13 0 474.67 30.6
4 13 0 371.95 25.59
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4 13 2 187.33 19.49
4 13 2 177.31 20.25
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4 13 2 178.65 14.78
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4 13 5 334.52 24.54
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4 13 5 321.58 27.54
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4 14 -17 13.13 5.54
4 14 -17 21 10.38
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4 14 -16 242.56 32
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4 14 -16 263.23 26.07
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4 14 -16 252.99 27.93
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4 14 -15 53.08 11.23
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4 14 -10 512.01 39.9
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4 14 0 225.88 21.36
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4 14 4 541.25 37.72
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4 14 5 150.68 17.1
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4 14 5 129.57 18.89
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4 14 7 333.79 25.81
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4 14 7 290.68 28
4 14 7 300.47 29.54
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4 14 10 280.25 26.61
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4 14 11 158.58 23.69
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4 14 12 308.15 31.57
4 14 12 316.28 34.31
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4 14 12 234.89 29.23
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4 14 13 129.99 19.37
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4 14 13 117.32 21.66
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4 14 14 249.92 26.82
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4 14 14 217.1 27.38
4 14 14 199.4 28.1
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8 12 -5 79.37 13.73
8 12 -5 81.89 12.34
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-8 12 5 87.59 14.34
-8 12 5 94.03 16.72
8 12 -5 69.5 13.02
8 12 -5 78.27 14.49
-8 12 5 105.79 14.5
-8 12 5 89.75 13.29
8 12 -4 61.5 10.96
-8 12 4 45.99 11.86
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8 12 -4 67.2 12.1
8 12 -4 77.68 11.98
-8 12 4 64 13.08
8 12 -4 83.75 15.92
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8 12 -4 77.27 13.87
8 12 -4 58.32 13.64
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8 12 -3 131.63 15.91
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8 12 -3 142.21 18.67
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8 12 -2 106.98 14.66
8 12 -2 99.1 13.46
8 12 -2 81.18 13.26
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8 12 -2 117.7 17.29
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8 12 -2 103.41 16.53
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8 12 -1 266.08 26.07
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8 12 -1 238.51 21.08
8 12 -1 237.8 22.16
8 12 -1 186.35 19.79
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8 12 -1 261.86 25.71
8 12 -1 193.04 23.04
8 12 -1 269.23 20.53
8 12 0 67.28 13.46
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8 12 0 69.98 10.99
8 12 0 70.8 13.1
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8 12 0 88.33 13.92
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8 12 0 66.88 12.99
8 12 1 203.4 22.11
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8 12 1 207.79 18.64
8 12 1 200.04 21.9
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8 12 1 161.76 19.26
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8 12 1 166.94 21
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8 12 2 15.85 6.85
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8 12 2 17.12 8.26
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8 12 3 155.02 20.46
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8 12 3 155.97 20.11
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8 12 3 123.4 19.73
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8 12 5 63.4 14.84
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8 12 5 60.39 12.86
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8 12 5 75.75 16.67
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8 12 6 -3.8 8.76
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8 12 6 9.99 6.92
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8 12 7 145.06 21.93
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8 12 7 165.34 19.73
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8 12 8 21.11 10.13
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8 12 11 33.15 9.43
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8 12 13 11.84 8.48
8 12 13 16.14 10.24
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8 12 15 -7.41 11.51
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8 12 18 9.71 12.58
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8 13 -22 14.99 9.19
-8 13 22 27.22 11.05
-8 13 21 100.53 19.34
8 13 -21 126.13 23.54
8 13 -21 70.41 16.33
8 13 -21 82.41 18.56
-8 13 21 104.3 20.42
-8 13 21 74.75 20.04
-8 13 20 55.53 16.12
8 13 -20 84.19 19.71
8 13 -20 56.56 14.08
8 13 -20 87.67 18.53
-8 13 20 48.97 13.96
-8 13 20 71.92 19.53
-8 13 19 127.4 22.27
8 13 -19 113.49 21.55
8 13 -19 105.02 19.42
8 13 -19 120.47 20.6
-8 13 19 130.94 21.32
-8 13 19 114.19 23.65
-8 13 18 117.53 21.4
8 13 -18 87.82 19.14
8 13 -18 97.9 18.9
8 13 -18 91.11 19.09
-8 13 18 84 18.37
-8 13 18 113.35 22.72
-8 13 17 148.84 27.06
8 13 -17 187.14 29.33
-8 13 17 151.51 22.97
8 13 -17 173.67 25.77
8 13 -17 172.46 23.63
8 13 -17 118.78 20.07
-8 13 17 152.54 22.45
8 13 -17 179.19 27.24
8 13 -16 167.78 25.89
-8 13 16 190.43 26.39
-8 13 16 117.76 23.76
8 13 -16 185.97 29.37
-8 13 16 169.76 24.67
8 13 -16 152.22 22.78
8 13 -16 184.89 24.06
-8 13 16 122.55 20.09
8 13 -16 93.62 17.6
8 13 -15 268.79 31.97
-8 13 15 256.45 30.51
-8 13 15 227.42 23.85
-8 13 15 194.88 28.51
8 13 -15 265.99 33.06
-8 13 15 244.26 29.7
8 13 -15 202.43 26.77
-8 13 15 219.86 23.58
8 13 -15 252.18 28.26
-8 13 15 163.61 22.38
8 13 -15 211.72 25.88
8 13 -14 126.41 22.34
-8 13 14 130.96 18.55
-8 13 14 160.24 23.89
-8 13 14 141.12 24.65
8 13 -14 168.67 26.77
-8 13 14 122.25 20.89
8 13 -14 187.43 24.5
-8 13 14 149.92 19.84
8 13 -14 149.43 18.64
8 13 -14 174.64 23.83
-8 13 14 159.58 22.17
8 13 -14 156.04 21.99
8 13 -13 179.5 25.86
-8 13 13 211.47 23.09
-8 13 13 209.63 26.82
-8 13 13 239.58 30.81
8 13 -13 219.92 29.54
-8 13 13 197.3 25.24
8 13 -13 221.44 27.11
-8 13 13 262.86 25.91
8 13 -13 232.91 26.85
8 13 -13 179.8 20.45
-8 13 13 190.54 23.38
8 13 -13 242.8 26.64
8 13 -12 313.27 33.47
-8 13 12 336.98 29.37
-8 13 12 258.08 28.8
-8 13 12 268.38 31.8
8 13 -12 266.23 31.18
-8 13 12 328.93 34.08
8 13 -12 317.63 31.26
-8 13 12 281.45 26.91
8 13 -12 280.7 25.59
8 13 -12 271.85 28.8
-8 13 12 263.72 27.23
8 13 -12 308.92 29.52
8 13 -11 170.78 23.76
-8 13 11 154.89 21.81
-8 13 11 181.51 22.11
-8 13 11 190.37 26.22
8 13 -11 183.22 25.07
-8 13 11 193.99 26.84
8 13 -11 174.72 23.54
-8 13 11 202.58 22.77
8 13 -11 178.42 20.18
-8 13 11 188.01 22.14
8 13 -11 185.78 23.25
8 13 -10 291.05 29.92
-8 13 10 272.94 26.78
-8 13 10 281.41 28.51
-8 13 10 261.91 29.82
8 13 -10 249.17 28.68
-8 13 10 239.32 28.81
-8 13 10 296.07 27.8
8 13 -10 255.57 24.77
-8 13 10 235.51 24.51
8 13 -10 250.93 26.72
8 13 -9 457.2 36.44
-8 13 9 366.41 31.5
-8 13 9 347.05 31.34
-8 13 9 389.03 36.59
8 13 -9 350.57 33.06
-8 13 9 378.06 35.02
-8 13 9 372.64 31.44
8 13 -9 347.68 28.66
-8 13 9 385.58 31.29
8 13 -9 378.3 32.18
8 13 -8 171.44 21.36
-8 13 8 152.79 20.88
-8 13 8 175.34 22.13
-8 13 8 176.65 24.61
8 13 -8 166.36 22.74
-8 13 8 172.66 24.09
-8 13 8 155.68 20.36
8 13 -8 133.5 17.82
-8 13 8 151.98 19.16
-8 13 8 166.05 18.98
8 13 -8 148.65 16.94
8 13 -8 132.98 19.7
8 13 -7 398.26 32.03
-8 13 7 356.2 31.24
-8 13 7 388.47 32.19
-8 13 7 342.59 33.25
8 13 -7 388.23 32.49
-8 13 7 401.81 33.09
-8 13 7 350.28 33.69
8 13 -7 361.22 29.56
8 13 -7 341.62 30.67
-8 13 7 395.07 32.89
-8 13 7 363.72 29.62
-8 13 7 389.1 29.06
8 13 -7 339.13 25.1
8 13 -6 134.6 18.29
-8 13 6 106.62 18.86
-8 13 6 114.1 17.88
8 13 -6 101.21 16.33
-8 13 6 112.15 18.24
8 13 -6 86.48 16.51
-8 13 6 109.65 17.06
-8 13 6 88.51 16.06
8 13 -6 102.17 15.46
8 13 -6 129.01 18.92
-8 13 6 92.69 13.65
8 13 -6 118.57 15.09
-8 13 6 105.24 15.17
8 13 -5 334.36 27.17
-8 13 5 318.95 31.45
-8 13 5 334.43 29.04
8 13 -5 340.53 28.95
-8 13 5 300.91 28.37
-8 13 5 308.41 29.31
8 13 -5 334.81 31.67
-8 13 5 368.21 29.93
8 13 -5 323.62 28.1
8 13 -5 330.81 29.95
-8 13 5 305.54 25.93
-8 13 5 292.12 24.42
8 13 -5 305.26 24.72
8 13 -4 43.62 9.51
-8 13 4 61.26 13.28
-8 13 4 73.49 14.41
8 13 -4 56.86 12.45
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8 13 -4 52.79 10.82
8 13 -4 60.33 13.96
-8 13 4 35.51 10.15
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8 13 -4 43.67 11.12
8 13 -4 20.96 7.83
-8 13 4 44.84 8.87
-8 13 4 39.48 10.77
8 13 -3 320.47 24.78
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-8 13 3 338.44 29.03
8 13 -3 319.86 26.55
-8 13 3 314.24 29.12
-8 13 3 298.64 28.9
-8 13 3 261 24.08
8 13 -3 340.7 30.87
8 13 -3 322.62 28.63
-8 13 3 337.06 25.85
8 13 -3 353.12 30.98
-8 13 3 258.42 24.09
8 13 -3 252.39 23.26
8 13 -2 39.02 8.81
8 13 -2 44.55 12.01
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8 13 -2 36.33 8.91
8 13 -2 46.6 11.04
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8 13 -2 56.75 13.6
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8 13 -2 30.06 10.24
-8 13 2 31.28 9.49
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-8 13 1 413.32 31.1
8 13 -1 436.39 30.32
8 13 -1 394.14 28.54
8 13 -1 386.36 29.79
-8 13 1 416.48 34.75
-8 13 1 385.88 29.46
8 13 -1 390.14 33.05
-8 13 1 438 35.63
8 13 -1 517.48 37.29
8 13 -1 387.88 33.61
-8 13 0 68.25 13.16
-8 13 0 60.37 12.47
8 13 0 59.09 10.65
8 13 0 44.29 10.46
8 13 0 43.75 11
-8 13 0 71.25 14.07
8 13 0 72.14 14.96
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8 13 0 77.68 15.48
-8 13 0 59.25 13.74
8 13 0 65.17 15.11
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8 13 1 363.08 26
8 13 1 329.2 28.91
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8 13 1 309.59 27.83
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8 13 1 327.54 29.56
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8 13 1 311.84 30.09
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8 13 2 145.04 15.93
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8 13 2 133.87 19.29
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8 13 2 148.09 19.37
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8 13 2 160.63 22.56
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8 13 3 351.78 30.39
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8 13 3 318.16 29.84
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8 13 3 341.12 29.41
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8 13 3 313.68 31.62
8 13 4 111.02 17.1
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8 13 4 126.75 19.31
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8 13 4 119.33 18.78
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8 13 4 106.28 19.05
8 13 5 336.45 29.13
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8 13 5 306.08 30.04
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8 13 5 272.45 28.73
8 13 5 266.84 30.22
-8 13 -5 331.79 30.07
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8 13 6 169.86 23.87
8 13 6 180.7 25.83
8 13 6 182.49 24.67
-8 13 -6 184.66 23.4
-8 13 -6 153.28 21.49
8 13 6 238.76 25.05
-8 13 -6 211.98 25.43
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8 13 7 370.97 34.33
8 13 7 391.2 31.47
-8 13 -7 395.45 34.56
-8 13 -7 391.22 33.76
8 13 7 403.53 37.09
-8 13 -7 325.08 31.67
8 13 7 448.96 40.76
8 13 8 115.92 17.56
-8 13 -8 99.56 17.17
-8 13 -8 93.57 17.45
8 13 8 141.58 22.49
-8 13 -8 123.91 17.45
8 13 8 137.98 22.46
-8 13 -8 116.96 19.31
-8 13 -8 93.66 17.48
8 13 8 144.13 24.82
-8 13 -9 394.4 31.18
8 13 9 341.3 33.85
-8 13 -9 325.56 34.57
8 13 9 404.58 39.23
-8 13 -9 421.52 34.19
-8 13 -9 358.97 34.15
-8 13 -9 377.38 33.22
8 13 9 445.41 33.71
-8 13 -10 169.56 21.04
-8 13 -10 108.87 21.1
-8 13 -10 151.89 21.03
8 13 10 115.15 21.16
8 13 10 139.51 19.21
-8 13 -10 96.86 16.64
8 13 10 132.94 22.61
-8 13 -11 180.3 22.26
-8 13 -11 173.27 26.09
8 13 11 183.23 27.79
-8 13 -11 175.28 22.2
8 13 11 212.18 27.94
8 13 11 205.66 23.54
-8 13 -11 187.3 23.11
8 13 12 108.1 20.29
-8 13 -12 128.21 23.02
-8 13 -12 163.35 22.39
8 13 12 180.4 22.11
8 13 13 157.19 24.4
-8 13 -13 157.65 26.65
-8 13 -13 180.36 24.06
8 13 13 160.01 21.53
8 13 14 61.44 17.58
-8 13 -14 77.98 20.48
-8 13 -14 67.51 15.29
8 13 14 64.97 14.24
8 13 15 113.96 22.3
-8 13 -15 84.51 20.2
-8 13 -15 86.89 18.23
8 13 16 34.24 13.01
-8 13 -16 44.84 16.56
-8 13 -16 49.82 15.19
8 13 17 77.36 19.81
-8 13 -17 89.97 19.22
-8 13 -17 107.55 22.26
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-8 14 20 41.89 14.68
8 14 -20 89.68 18.39
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8 14 -20 38.86 13.31
-8 14 20 62.27 18.95
8 14 -20 59.01 16.47
-8 14 19 35.32 13.34
8 14 -19 33.87 13.61
-8 14 19 53.03 15.75
8 14 -19 25.99 11.62
-8 14 19 28.44 13.98
8 14 -19 31.15 12.42
-8 14 18 45.54 13.84
-8 14 18 87 17.93
8 14 -18 42.74 15.11
8 14 -18 63.52 15.68
-8 14 18 94.91 22.99
8 14 -18 72.17 17.06
-8 14 17 57.65 15.01
-8 14 17 73.58 17.08
8 14 -17 60.58 15.86
-8 14 17 77.09 18.13
8 14 -17 62.03 16.31
8 14 -17 68.11 15.65
-8 14 17 53.37 16.55
8 14 -16 94.95 21.12
-8 14 16 81.25 18.48
-8 14 16 130.86 25.72
8 14 -16 87.77 20.73
-8 14 16 109.92 21.05
8 14 -16 76.81 16.36
8 14 -16 93.44 18.48
-8 14 16 107.07 18.93
8 14 -16 112.78 20.49
8 14 -15 164.49 25.66
-8 14 15 177.92 21.91
-8 14 15 144.59 23.18
-8 14 15 100.87 21.46
8 14 -15 136.37 25.06
-8 14 15 115.78 21.2
8 14 -15 129.2 21.86
-8 14 15 161.33 20.97
8 14 -15 118.17 20.66
-8 14 15 130.01 20.39
8 14 -15 128.38 21.09
8 14 -14 50.6 16.33
-8 14 14 54.58 12.79
-8 14 14 68.22 16.15
-8 14 14 69.57 18.38
8 14 -14 89 20.08
-8 14 14 48.07 14.84
8 14 -14 38.44 12.77
-8 14 14 60.57 13.06
8 14 -14 55.73 12.71
8 14 -14 73.73 15.88
-8 14 14 44.02 11.6
8 14 -14 55.76 15.14
8 14 -13 177.98 26.21
-8 14 13 226.29 24.95
-8 14 13 199.94 26.15
-8 14 13 224.48 30.49
8 14 -13 222.01 30.2
-8 14 13 215.61 28.93
8 14 -13 167.91 24.27
-8 14 13 178.53 21.88
8 14 -13 172.25 24.51
8 14 -13 192.11 22.17
-8 14 13 174.02 22.7
8 14 -13 214.37 25.6
8 14 -12 90.05 17.3
-8 14 12 65.62 15.45
-8 14 12 83.3 15.55
-8 14 12 106.65 20.81
8 14 -12 112.1 20.87
-8 14 12 65.31 16.76
8 14 -12 79.87 18.02
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8 14 -12 75.33 15.2
8 14 -12 92.49 15.39
-8 14 12 62.89 13.09
8 14 -12 117.23 18.87
8 14 -11 74.23 15.81
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8 14 -11 103.28 20.01
-8 14 11 96.76 19.82
8 14 -11 79.06 17.78
-8 14 11 106.45 17.04
8 14 -11 100.46 16.2
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8 14 -11 115.7 19.09
8 14 -10 75.87 15.08
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8 14 -10 87.39 14.64
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8 14 -10 81.94 16.04
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8 14 -9 86.21 17.18
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-8 14 9 72.33 15.1
8 14 -9 47.03 11.65
-8 14 9 41.59 11.46
8 14 -9 50.83 13.5
8 14 -8 52.43 12.35
8 14 -8 75.32 16.54
-8 14 8 90.32 16.81
-8 14 8 77.53 15.7
-8 14 8 88.55 19.29
8 14 -8 63.47 14.52
-8 14 8 61.43 14.74
-8 14 8 55.94 13.59
8 14 -8 71.81 14.44
-8 14 8 83.78 14.06
-8 14 8 93.08 15.59
8 14 -8 88.78 16.2
8 14 -7 102.31 16.21
8 14 -7 97.75 18.23
-8 14 7 83.2 15.95
-8 14 7 86.86 15.5
-8 14 7 93.84 19.34
-8 14 7 94.86 17.23
8 14 -7 107.66 16.9
-8 14 7 115.71 20.17
8 14 -7 93.41 15.42
8 14 -7 123.91 19.46
-8 14 7 105.03 17.78
-8 14 7 114.05 16.69
-8 14 7 91.8 15.67
8 14 -7 76.68 13.01
8 14 -6 10.7 5.89
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10 -17 -14 6.67 7.45
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10 -17 -10 63.21 18.29
10 -17 -10 27.67 13.26
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10 -17 -9 166.36 27.63
10 -17 -9 180.69 29.23
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10 -17 -8 35.15 14.8
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10 -17 -7 269.83 34.55
10 -17 -7 305.83 38.26
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10 -17 -6 15.92 9.47
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10 1 -3 1463.41 47.46
10 1 -3 1519.03 47.65
10 1 -3 1557.32 43.78
10 1 -3 1538.31 46.94
10 1 -3 1499.9 53.13
-10 1 3 1593.14 44.86
-10 1 3 1513.53 58.79
10 1 -2 93.44 9.62
10 1 -2 79.08 10.49
10 1 -2 93.7 11.54
-10 1 2 96.26 16.19
10 1 -2 93.5 13.79
-10 1 2 82.6 9.93
10 1 -2 81.8 9.92
10 1 -2 96.29 9.66
-10 1 2 81.35 12.4
-10 1 2 79.97 14.71
10 1 -1 1433.43 46.95
10 1 -1 1404.92 49.62
-10 1 1 1426.91 55.26
-10 1 1 1510.72 66.9
-10 1 1 1501.87 49.51
10 1 -1 1408.49 56.6
10 1 -1 1466.79 48.72
10 1 -1 1460.9 42.87
-10 1 1 1348.76 63.14
-10 1 1 1445.71 56.25
10 1 -1 1495.29 53.52
10 1 0 70.82 11.47
-10 1 0 60 12.33
10 1 0 78.09 12.19
-10 1 0 62.73 9.56
10 1 0 64.65 9.49
10 1 0 68.01 9.28
10 1 0 74.28 9.82
-10 1 0 69.13 10.97
-10 1 0 81.9 13.29
-10 1 0 59.5 13.14
10 1 0 78.24 11.77
10 1 1 951.94 43.44
-10 1 -1 892.19 49.27
-10 1 -1 1015.23 43.08
10 1 1 983.78 43.11
10 1 1 869.7 38.36
-10 1 -1 892.33 41.12
10 1 1 915.85 39.22
10 1 1 901.58 36.47
-10 1 -1 910.45 44.05
10 1 1 924.95 40.71
-10 1 -1 898.13 49.01
10 1 2 25.75 7.71
-10 1 -2 19.43 8.23
10 1 2 23.36 7.14
-10 1 -2 9.53 5.93
10 1 2 25.88 7.47
-10 1 -2 30.05 7.74
10 1 2 19.38 5.63
-10 1 -2 14.03 6.07
10 1 2 12.25 4.96
10 1 2 11.13 5.1
-10 1 -2 21.76 8.17
10 1 3 740.36 39.75
10 1 3 670.55 33.56
-10 1 -3 745.42 39.83
10 1 3 731.23 36.42
10 1 3 725.22 37.27
10 1 3 679.4 29.78
-10 1 -3 646.57 40.84
10 1 3 755.91 35.11
-10 1 -3 670.46 41.07
-10 1 -3 674.03 39.2
-10 1 -4 18.47 6.18
10 1 4 43 6.91
10 1 4 43.28 8.16
10 1 4 33.54 8.35
-10 1 -4 25.76 7.89
10 1 4 40.17 11.47
10 1 4 32.71 8.79
-10 1 -4 21.99 7.9
10 1 4 36.61 8.24
-10 1 -4 49.95 11.96
-10 1 -5 798.34 45.38
10 1 5 836.03 35.74
-10 1 -5 761.7 45.32
10 1 5 795.41 41.25
10 1 5 839.61 42.96
10 1 5 905.26 46.6
10 1 5 796.18 42.65
-10 1 -5 869.15 46.36
10 1 5 867.78 37.8
-10 1 -5 778.17 44.54
-10 1 -6 -2.34 5.43
10 1 6 6.71 4.3
-10 1 -6 2.15 5.79
10 1 6 9.01 6.03
10 1 6 15.72 7.75
10 1 6 14 9.41
10 1 6 10.13 4.79
-10 1 -6 1.99 6.42
10 1 6 8.78 5.78
-10 1 -6 4.65 4.47
-10 1 -7 856.96 46.54
-10 1 -7 815.3 51.52
10 1 7 853.92 46.13
10 1 7 876.63 44.6
10 1 7 901.1 49.03
10 1 7 938.22 49.05
10 1 7 898.51 38.43
-10 1 -7 833.93 47.99
-10 1 -8 17.79 8.36
-10 1 -8 42.71 12.26
10 1 8 35.27 10.26
10 1 8 38.22 9.78
10 1 8 20.63 9.33
10 1 8 27.22 9.76
10 1 8 18.82 6.67
-10 1 -8 17.41 6.8
-10 1 -9 671.4 40.16
-10 1 -9 683.02 50.7
10 1 9 702.23 44.41
10 1 9 707.33 41
10 1 9 785.97 46.74
10 1 9 724.21 45.35
10 1 9 655.75 32.88
-10 1 -9 714.03 46.13
-10 1 -10 63.03 14.82
-10 1 -10 42.93 15.86
10 1 10 47.74 11.22
10 1 10 40.53 13.04
10 1 10 34.61 12.01
10 1 10 41.96 8.78
-10 1 -10 43.39 10.82
-10 1 -11 530.5 34.89
-10 1 -11 595.02 49.38
10 1 11 576.62 42.37
10 1 11 545.59 36.79
-10 1 -11 549.56 40.18
10 1 11 552.68 41.64
-10 1 -11 542.27 42.5
10 1 11 595.54 30.7
-10 1 -12 21.33 10.66
10 1 12 21.12 10.54
10 1 12 31.07 11.36
-10 1 -12 35.95 11.28
-10 1 -12 29.69 12.5
10 1 12 20.8 10.4
10 1 13 501.76 41.94
10 1 13 558.98 38.55
-10 1 -13 460.7 44.42
-10 1 -13 505.98 39.89
-10 1 -13 504.98 42.91
10 1 13 535.79 42.29
-10 1 -14 25.14 15.28
10 1 14 26.28 10.45
10 1 14 44.03 14.3
-10 1 -14 18.94 8.9
-10 1 -14 11.38 9.01
10 1 14 21.95 11.55
10 1 15 502.22 44.11
10 1 15 520.72 39.23
-10 1 -15 524.58 48.49
-10 1 -15 474.26 40.21
-10 1 -15 483.6 44.79
10 1 15 516.51 43.65
-10 1 -16 -0.13 9.32
-10 1 -16 -8.59 10.25
10 1 16 26.2 10.93
10 1 16 -2.61 7.26
-10 1 -16 4.44 9.11
10 1 16 17.88 11.56
-10 1 -17 344.64 35.22
10 1 17 335.61 35.53
10 1 17 413.33 36.45
-10 1 -17 344.65 40.66
10 1 17 307.06 33.48
-10 1 -17 450.13 46.16
10 1 17 415.76 41.95
10 1 18 -3.9 11.25
-10 1 -18 9.02 12.76
10 1 18 -4.14 7.2
10 1 18 8.04 9.13
-10 1 -18 -6.47 12.19
10 1 18 -0.46 8.16
10 1 19 247.77 29.87
10 1 19 254.57 29.75
-10 1 -19 218.89 34.47
-10 1 -19 279.85 37.27
10 1 20 11.77 9.85
10 1 20 7.67 8.5
-10 1 -20 -0.37 10.45
-10 1 -20 -2.84 10.03
10 1 21 142.75 23.42
10 1 21 75.55 17.62
-10 1 -21 142.16 29.22
-10 1 -21 124.4 25.24
-10 2 26 58.75 15.58
10 2 -26 54.61 16.23
10 2 -25 -4.15 9.62
-10 2 25 1.92 8.45
10 2 -25 10.62 10.7
10 2 -25 -6.45 7.14
-10 2 25 1.52 7.9
10 2 -24 9.72 6.98
10 2 -24 26.34 12.74
-10 2 24 31.6 10.35
10 2 -24 48.06 15.64
-10 2 24 39.08 15.48
10 2 -23 -0.81 6.21
10 2 -23 -2.29 8.09
10 2 -23 -4.65 8.86
10 2 -23 -8.76 11.22
-10 2 23 -3.02 7.86
10 2 -23 11.43 9.92
-10 2 23 3.76 8.96
10 2 -22 21.94 9.3
10 2 -22 9.66 7.21
10 2 -22 28.11 12.71
10 2 -22 22.63 11.65
-10 2 22 18.81 8.1
10 2 -22 38.24 12.83
-10 2 22 27.91 12.5
10 2 -21 5.74 7.1
10 2 -21 -12.08 8.18
10 2 -21 9.01 11.15
10 2 -21 -5.08 7.79
-10 2 21 -6.84 7.62
-10 2 21 23.08 13.54
10 2 -21 18.12 10
10 2 -20 46.94 12.8
10 2 -20 76.42 16.38
10 2 -20 60.67 16.22
-10 2 20 85.78 16.81
-10 2 20 77.3 18.2
10 2 -20 58.39 16.81
10 2 -19 20.13 8.86
10 2 -19 21.31 10.98
10 2 -19 12.09 7.3
-10 2 19 8.6 5.48
-10 2 19 18.55 10.74
10 2 -19 6.13 7.73
10 2 -18 59.17 12.88
10 2 -18 78.73 16.24
10 2 -18 93.94 18.73
-10 2 18 83.91 15.43
-10 2 18 117.48 22.79
10 2 -18 66.47 16.56
10 2 -17 3.39 5.24
10 2 -17 3.23 7.06
10 2 -17 -2.58 6.79
-10 2 17 -1.46 5.93
-10 2 17 1.83 8.78
10 2 -17 1.9 6.6
10 2 -16 54.75 11.87
10 2 -16 73.19 14.89
-10 2 16 61.19 11.65
-10 2 16 54.78 12.53
-10 2 16 85.77 18.95
10 2 -16 86.26 15.91
10 2 -15 1.26 3.78
10 2 -15 3 8.1
-10 2 15 -0.09 3.92
-10 2 15 0.57 5.3
-10 2 15 -4.51 8.62
10 2 -15 -3.59 5.67
-10 2 14 61.54 11.56
10 2 -14 61.24 11.85
10 2 -14 76.9 13.84
-10 2 14 63.94 11.38
10 2 -14 56.35 12.32
-10 2 14 42.38 13.39
-10 2 13 59.24 12.37
-10 2 13 45.73 10.37
10 2 -13 33.45 8.11
10 2 -13 40.58 10.59
-10 2 13 35.19 8.34
-10 2 13 35.1 9.52
10 2 -13 30.83 8.7
-10 2 13 44.13 13.92
-10 2 12 78.65 13.48
-10 2 12 113.02 14.08
-10 2 12 92.98 18.27
10 2 -12 90.7 13.9
-10 2 12 79.87 13.28
10 2 -12 97.48 15.73
-10 2 12 90.18 13.17
10 2 -12 98.03 13.07
10 2 -11 28.07 6.85
-10 2 11 30.53 7.79
-10 2 11 18.71 8.32
10 2 -11 26 7.44
-10 2 11 34.57 10.16
10 2 -11 25.33 7.98
-10 2 11 27.27 8.26
-10 2 11 37 8.33
10 2 -11 39.67 7.13
-10 2 10 76.9 11.57
-10 2 10 84.65 15.21
10 2 -10 74.4 11.85
-10 2 10 79.44 13.71
10 2 -10 85.59 13.36
-10 2 10 73.6 13.62
-10 2 10 88.74 11.55
10 2 -10 88.61 10.01
-10 2 9 54.4 9.71
-10 2 9 46.7 11.89
10 2 -9 71.63 11.95
-10 2 9 43.78 11.34
10 2 -9 52.49 10.61
-10 2 9 37 8.09
-10 2 9 47.59 11.11
10 2 -9 58.43 7.89
-10 2 8 159 15.18
-10 2 8 146.57 19.81
10 2 -8 142.47 15.86
-10 2 8 140.79 18.64
10 2 -8 166.51 18.19
-10 2 8 161.59 15.2
-10 2 8 129.07 18.14
10 2 -8 157.08 12.76
-10 2 7 11.37 3.79
-10 2 7 5.56 5.58
10 2 -7 14.87 5.84
-10 2 7 22.27 8.65
10 2 -7 8.98 5.53
10 2 -7 9.66 3.51
-10 2 7 10.43 4.27
-10 2 7 8.76 5.95
10 2 -6 57.52 7.62
-10 2 6 57.12 12.75
-10 2 6 56.18 8.74
-10 2 6 83.86 13.58
10 2 -6 65.98 10.14
-10 2 6 50.93 12.1
10 2 -6 69.64 11.55
10 2 -6 62.16 8.08
10 2 -6 56.15 7.32
-10 2 5 34.15 11.83
-10 2 5 38 6.78
-10 2 5 22.98 8.93
10 2 -5 30.56 6.73
10 2 -5 29.19 5.62
10 2 -5 47.06 9.42
10 2 -5 39.17 7.08
-10 2 5 25.8 7.22
10 2 -4 77.18 9.8
-10 2 4 98.63 16.66
-10 2 4 104.89 10.37
10 2 -4 99.6 9.29
10 2 -4 81.82 10.41
10 2 -4 88.66 9.95
10 2 -4 72.76 11.17
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10 2 -3 6.39 3.49
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10 2 -3 2.69 2.34
10 2 -3 0.88 2.93
10 2 -3 4.26 3.35
10 2 -3 1.3 2.44
10 2 -3 -0.22 3.65
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10 2 -2 31.5 5.93
10 2 -2 27.69 5.68
10 2 -2 27.74 6.52
10 2 -2 21.35 6.33
10 2 -2 23.23 4.83
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10 2 -1 1.6 3.31
10 2 -1 -0.52 3.62
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10 2 -1 -3.78 6.3
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10 2 -1 0.24 2.86
10 2 -1 0.28 3.01
10 2 -1 -3.04 4.6
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10 2 0 4.16 3.12
10 2 0 8.03 4.58
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10 2 0 2.87 2.54
10 2 0 -0.48 2.88
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10 2 0 3.36 3.75
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10 2 1 3.7 3.96
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10 2 1 2.94 3.12
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10 2 1 -2.47 3.99
10 2 1 -1.92 4.38
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-10 2 -1 1.79 5.83
10 2 1 0.48 3.54
10 2 2 11.06 6.42
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10 2 2 3.59 2.83
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10 2 2 4.62 4.69
10 2 2 8.65 4.15
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10 2 2 2.77 2.86
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10 2 3 1.46 3.59
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10 2 3 0.67 2.41
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10 2 3 -0.86 4.88
10 2 3 1.59 3.47
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10 2 3 -3.83 4.16
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10 2 4 47.73 8.56
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10 2 4 49.15 9.39
10 2 4 37.48 7.02
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10 2 4 57.61 12.29
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10 2 4 37.86 7.77
10 2 5 42.28 9.97
10 2 5 19.35 5.68
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10 2 5 30.12 7.74
10 2 5 33.05 9.1
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10 2 5 29.23 7.95
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10 2 5 37.82 7.45
10 2 6 24.37 8.05
10 2 6 28.29 6.22
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10 2 6 37.24 9.68
10 2 6 31.79 9.28
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10 2 6 21.32 5.64
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10 2 6 29.05 9.78
10 2 7 143.46 19.31
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10 2 7 138.19 17.71
10 2 7 137.22 16.51
10 2 7 153.39 14.65
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-10 2 -7 159.94 19.3
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10 2 7 127.23 17.76
10 2 8 3.25 6.38
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10 2 8 15.33 7.39
10 2 8 14.6 5.6
-10 2 -8 20.24 8.01
-10 2 -8 11.07 6.33
-10 2 -8 23.34 9.14
10 2 8 19.34 7.63
10 2 9 99.15 17.2
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10 2 9 69.36 12.51
10 2 9 56.7 8.83
-10 2 -9 57.11 11.55
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10 2 9 92.96 17.38
10 2 10 37.73 11.97
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10 2 10 26.76 8.61
10 2 10 18.5 6.28
10 2 10 26.69 9.82
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10 2 11 82.02 16.19
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10 2 11 59.73 14.63
10 2 11 47.57 11.11
10 2 12 1.46 7.35
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10 2 12 -1.61 8.15
10 2 12 -4.14 6.17
10 2 13 16.94 8.56
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-10 2 -13 30.83 13.43
10 2 13 23.03 11.03
10 2 13 20.43 8.2
10 2 14 -5.44 9.07
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-10 2 -14 7.71 8.11
10 2 14 12.62 10.08
10 2 14 -1.97 5.46
10 2 15 0.09 7.19
10 2 15 4.9 5.57
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-10 2 -15 13.78 10.37
10 2 15 5.5 9.6
10 2 16 -6.36 7.08
10 2 16 -6.98 6.56
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10 2 16 5.8 8.93
-10 2 -16 -5.54 10.52
10 2 16 -6.12 9.2
10 2 17 2.65 9.22
10 2 17 4.36 10.32
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10 2 17 -5.78 7.07
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10 2 17 9.15 8.66
10 2 18 5.88 8.23
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10 2 18 -3.57 7.89
10 2 18 -7.92 9.07
-10 2 -18 -5.78 8.98
10 2 19 17.02 8.34
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10 2 19 7.59 9.49
10 2 20 -9.83 9.04
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10 2 20 -6.98 7.97
10 2 21 7.97 6.98
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10 2 21 1.44 7.76
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10 3 -25 117.54 20.86
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10 3 -25 136.77 22.43
10 3 -24 106.09 19.71
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10 3 -24 101.04 19.99
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10 3 -24 125.99 20.06
10 3 -23 171.34 24.24
10 3 -23 186.75 25.59
10 3 -23 176.29 24.99
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-10 3 23 239.32 29.36
10 3 -23 218.64 27.96
10 3 -23 207.16 28.42
10 3 -22 103.96 19.02
10 3 -22 103.35 19.27
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10 3 -22 83.2 18.04
10 3 -22 94.83 20.25
10 3 -21 189.73 24.06
10 3 -21 220.03 27.25
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-10 3 21 202.99 25.89
10 3 -21 228.63 28.01
10 3 -21 225.42 29.02
10 3 -20 116.99 19.17
10 3 -20 144.09 22.84
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10 3 -20 126.97 21.69
10 3 -20 112.35 21
10 3 -19 358.41 31.65
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10 3 -19 385.04 34.94
-10 3 19 336.89 36.55
10 3 -19 359.11 34.04
10 3 -19 433.29 39.39
10 3 -18 131.7 18.84
10 3 -18 157.26 22.46
-10 3 18 123.78 22.77
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10 3 -18 156.9 21.89
10 3 -18 123.32 20.42
10 3 -17 501.9 38.01
10 3 -17 507.5 40.92
10 3 -17 499.72 38.15
-10 3 17 410.62 39.94
10 3 -17 430.56 33.22
-10 3 17 445.75 35.42
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10 3 -16 140.97 18.2
10 3 -16 171.88 22.39
-10 3 16 161.37 18.69
10 3 -16 168.13 21.32
-10 3 16 138.89 23.13
10 3 -16 166.75 23.53
-10 3 15 558.39 35.8
-10 3 15 531.62 34.94
10 3 -15 624.92 37.75
-10 3 15 589.73 39.39
10 3 -15 662.14 41.78
10 3 -15 688.02 42.67
10 3 -15 630.01 44.15
-10 3 15 578.54 47.1
-10 3 14 184.03 20.27
-10 3 14 218.88 22.69
10 3 -14 232.72 21.43
10 3 -14 194.67 21.94
10 3 -14 211.6 18.17
10 3 -14 211.25 23.26
-10 3 14 200.95 21.11
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-10 3 13 633.05 38.22
-10 3 13 625.25 38.57
10 3 -13 611.42 38.42
10 3 -13 625.56 31.51
10 3 -13 684.96 41.24
-10 3 13 614.47 37.7
-10 3 13 616.65 45.52
-10 3 12 287.97 25.62
-10 3 12 293.11 24.65
10 3 -12 257.81 23.97
10 3 -12 274.84 19.69
10 3 -12 299.63 26.35
-10 3 12 254.31 24.07
-10 3 12 226.51 27.04
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-10 3 11 790.13 40.26
10 3 -11 783.35 41.5
10 3 -11 727.6 32.63
10 3 -11 755.42 41.84
-10 3 11 718.01 41.95
-10 3 11 717.88 47.48
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-10 3 10 539.51 31.83
10 3 -10 507.37 32.46
10 3 -10 494.99 25.86
10 3 -10 540.25 34.06
-10 3 10 458.36 33.3
-10 3 10 489.05 26.89
-10 3 10 504.1 37.84
-10 3 9 590.34 38.38
-10 3 9 680.89 35.1
10 3 -9 607.31 34.87
10 3 -9 648.58 29.54
10 3 -9 625.17 36.56
-10 3 9 548.72 37.46
-10 3 9 646.95 30.56
-10 3 9 600.7 39.94
-10 3 8 719.21 43.27
-10 3 8 860.95 38.62
10 3 -8 723.92 37.54
10 3 -8 790.58 33.26
10 3 -8 783 40.59
-10 3 8 858.23 35.22
-10 3 8 724.52 43.84
-10 3 8 737.55 43.66
-10 3 7 725.04 43.85
-10 3 7 760.19 35.66
10 3 -7 736.27 36.74
10 3 -7 827.31 33.55
10 3 -7 844.85 41.13
-10 3 7 790.01 43.69
-10 3 7 680.64 42.6
-10 3 6 771.14 46.06
-10 3 6 789.57 46.35
-10 3 6 839 36.47
10 3 -6 801.4 36.89
10 3 -6 807.72 33.98
10 3 -6 820.99 31.01
10 3 -6 790.52 39.62
10 3 -6 774.78 30.69
-10 3 6 798.4 43.04
-10 3 5 949.53 52.36
-10 3 5 931.54 51.65
-10 3 5 1036.61 39.94
10 3 -5 1020.96 41.37
10 3 -5 977.94 38.41
10 3 -5 989.2 36.3
10 3 -5 903.21 42.48
10 3 -5 912.42 35.92
-10 3 5 991.59 47.1
-10 3 4 602.48 41.77
-10 3 4 664.08 43.69
-10 3 4 668.55 30.49
10 3 -4 641.28 31.12
10 3 -4 641.33 30.32
10 3 -4 598.62 33.16
-10 3 4 699.56 37.38
10 3 -4 624.01 29.87
-10 3 3 813.42 49.28
-10 3 3 812.2 49.05
-10 3 3 818.65 33.53
10 3 -3 760.01 33.83
10 3 -3 781.72 35.34
10 3 -3 729.07 36.61
-10 3 3 867.85 41.39
10 3 -2 678.17 28.84
10 3 -2 659.55 33.97
-10 3 2 699.03 45.69
-10 3 2 666.61 28.46
10 3 -2 661.72 26.32
10 3 -2 675.03 30.13
10 3 -2 700.68 34.39
-10 3 2 687.41 44.8
-10 3 2 742.29 37.29
-10 3 2 744.77 36.73
10 3 -1 1005.69 38.93
-10 3 1 1059.16 45.11
-10 3 1 1058.56 56.43
-10 3 1 1073.26 40.22
10 3 -1 1016.55 36.14
10 3 -1 1058.36 38.34
10 3 -1 1062.31 44.96
-10 3 1 1035.01 55.52
-10 3 1 1088.54 46.54
10 3 0 335.34 22.3
-10 3 0 354.53 24.01
-10 3 0 347.54 31.01
-10 3 0 382.17 23.99
10 3 0 339.24 20.43
10 3 0 348.52 19.77
10 3 0 358.61 25.48
-10 3 0 352.26 30.56
-10 3 0 361.04 25.68
10 3 1 772.92 36.67
-10 3 -1 765.25 36.16
-10 3 -1 793.95 47.17
10 3 1 809.97 39.48
-10 3 -1 729.01 36.74
10 3 1 751.22 32.71
10 3 1 687.15 29
10 3 1 767 39.77
-10 3 -1 862.14 41.4
-10 3 -1 753.47 45.92
10 3 2 249.96 20.45
10 3 2 225.21 19.41
10 3 2 216.48 17.59
-10 3 -2 229.11 20.76
-10 3 -2 222.91 18.36
-10 3 -2 226.59 24.89
10 3 2 191.77 20
-10 3 -2 246.72 22.19
10 3 2 222.3 18.1
-10 3 -2 235.28 24.74
10 3 3 609.15 34.83
10 3 3 601.14 32.08
10 3 3 584.36 31.07
-10 3 -3 579.45 35.85
-10 3 -3 614.98 31.07
-10 3 -3 578.13 39.35
10 3 3 574.01 36.06
10 3 3 605.45 29.75
-10 3 -3 537.18 34.5
10 3 3 598.17 30.61
-10 3 -3 638.29 41.01
10 3 4 200.77 20.5
10 3 4 193.84 16.93
-10 3 -4 201.18 21.53
10 3 4 208.51 18.73
-10 3 -4 188.41 22.03
10 3 4 209.56 16.56
10 3 4 230.69 23.39
-10 3 -4 236.61 22.82
10 3 4 208.15 17.4
-10 3 -4 190.57 21.67
10 3 5 786.43 42.97
10 3 5 777.43 34.51
-10 3 -5 683.79 44.12
10 3 5 776.68 39.47
10 3 5 765.45 40.16
10 3 5 818.22 33.38
-10 3 -5 779.83 45.6
10 3 5 824.28 44.86
-10 3 -5 787.17 43.57
10 3 5 763.18 34.45
-10 3 -5 703.79 43.24
10 3 6 246.53 23.68
10 3 6 219.52 16.65
-10 3 -6 213.19 25.02
10 3 6 217.34 21.36
10 3 6 221.63 21.17
-10 3 -6 223.61 23.59
-10 3 -6 216.59 22.43
10 3 6 230.48 17.42
-10 3 -6 213.95 22.65
10 3 6 223.82 23.93
10 3 7 575.08 39.39
-10 3 -7 549.12 42.5
10 3 7 568.88 34.78
-10 3 -7 565.2 38.05
-10 3 -7 521.98 36.05
10 3 7 562.82 28.24
-10 3 -7 536.71 36.37
10 3 7 566.71 38.28
10 3 8 128.01 19.32
-10 3 -8 154.02 23.52
10 3 8 150.74 18.29
-10 3 -8 159.69 20.89
-10 3 -8 135.91 18.07
-10 3 -8 115.41 16.72
10 3 8 153.93 13.97
10 3 8 132.11 18.92
10 3 9 505.94 38.61
-10 3 -9 432.3 40.71
10 3 9 459.69 32.56
-10 3 -9 437.32 35.07
-10 3 -9 429.52 31.96
-10 3 -9 420.34 31.29
10 3 9 398.68 33.88
10 3 10 109.77 18.71
-10 3 -10 114.86 22.26
10 3 10 108.54 15.97
-10 3 -10 87.23 17.95
-10 3 -10 121.17 16.81
-10 3 -10 95.36 15.17
10 3 10 118.93 19.8
-10 3 -11 306.37 26.95
-10 3 -11 316.92 32.26
-10 3 -11 251.69 31.53
10 3 11 337.35 32.97
10 3 11 388.52 35.06
10 3 11 303.71 27.06
-10 3 -12 120.87 20.23
-10 3 -12 100.58 20.04
10 3 12 83.33 17.54
10 3 12 122.76 19.89
10 3 12 118.2 18.07
-10 3 -13 240.99 29.57
-10 3 -13 239.57 31.91
10 3 13 223.56 27.49
10 3 13 216.03 27.98
10 3 13 263.77 26.13
-10 3 -14 155.33 24.63
10 3 14 150.48 20.74
-10 3 -14 106.8 24.34
10 3 14 136.87 22.31
10 3 14 119.02 21.7
-10 3 -15 246.47 32.01
10 3 15 244.98 26.66
-10 3 -15 249.64 32.49
10 3 15 231 27.74
10 3 15 323.58 33.86
10 3 15 313.58 35.48
-10 3 -16 125.95 22.93
10 3 16 180.68 23.35
-10 3 -16 159.49 27.35
10 3 16 134.2 21.44
10 3 16 159.42 25.07
10 3 16 158.74 25.88
-10 3 -17 177.5 28.56
-10 3 -17 235.26 32.89
10 3 17 181.31 23.68
10 3 17 144.57 23.78
10 3 17 206.61 28.5
10 3 17 232.67 31.33
-10 3 -18 38.78 16.06
-10 3 -18 64.62 18.45
10 3 18 58.76 15.63
10 3 18 42.35 14.3
10 3 18 55.21 14.47
10 3 19 48.1 13.66
10 3 19 61.46 14.98
-10 3 -19 73.14 20.12
-10 3 -19 86.77 22.25
10 3 20 23.28 10.64
10 3 20 22.03 11.75
-10 3 -20 0.88 10.99
-10 3 -20 1.25 12.01
10 3 21 41.78 13.56
10 3 21 39.85 13.53
10 4 -25 -7.73 8.52
-10 4 25 -1.74 6.45
10 4 -25 11.74 7.59
-10 4 25 -9.8 10.54
-10 4 24 10.94 9.31
-10 4 24 36.02 12.8
10 4 -24 24.29 10.37
10 4 -24 33.76 12.32
-10 4 23 10.55 8.22
-10 4 23 -10.79 10.31
10 4 -23 -13.91 8.46
10 4 -23 -4.39 8.59
10 4 -22 56.14 15.51
10 4 -22 8.9 7.88
-10 4 22 37.73 13.36
10 4 -22 50.87 15.65
-10 4 22 63.85 17.24
-10 4 21 -5.22 8.15
-10 4 21 2.02 7.2
10 4 -21 15.01 11.62
10 4 -21 17.27 11.28
10 4 -21 -13.3 11.29
-10 4 20 30.15 12.35
-10 4 20 35.4 11.85
10 4 -20 0.11 7.51
10 4 -20 13.97 10
10 4 -20 33.42 12.06
-10 4 19 -4.39 8.98
-10 4 19 9.06 6.19
10 4 -19 -13.97 11.2
10 4 -19 18.02 10.29
10 4 -19 -3.18 7.05
-10 4 18 23.6 9.85
-10 4 18 22.63 7.88
10 4 -18 27.94 12.26
10 4 -18 33.89 11.06
10 4 -18 7.87 7.97
-10 4 17 6.24 6.6
-10 4 17 0.98 6.36
10 4 -17 11.8 6.11
10 4 -17 0.75 7.07
10 4 -17 -7.48 9.8
-10 4 16 18.32 4.78
-10 4 16 25.84 11.4
-10 4 16 37.92 10.7
10 4 -16 37.19 10.95
-10 4 16 9.14 5.31
10 4 -16 20.88 9.04
10 4 -16 17.14 6.07
10 4 -16 17.23 9.1
-10 4 15 12.68 5.8
-10 4 15 9.94 8.69
-10 4 15 24.99 9.4
10 4 -15 10.74 6.52
-10 4 15 17.16 6.45
10 4 -15 32.46 10.41
10 4 -15 12.83 5.88
10 4 -15 12.8 8.16
-10 4 14 51.9 11.35
-10 4 14 24.47 11.24
-10 4 14 22.55 8.4
10 4 -14 26.13 10.32
-10 4 14 22.63 6.41
10 4 -14 37.15 10.82
10 4 -14 33.62 8.03
10 4 -14 30.76 11.46
-10 4 13 11.89 6.71
-10 4 13 22.61 10.23
-10 4 13 20 7.52
10 4 -13 18.65 8.38
-10 4 13 24.78 8.45
10 4 -13 21.21 8.7
10 4 -13 19.71 5.89
10 4 -13 19.37 10.04
-10 4 12 -2.82 8.95
-10 4 12 10.37 6.39
10 4 -12 22.9 8.67
-10 4 12 16.96 7.36
10 4 -12 -0.09 6.9
-10 4 12 5.41 4.39
10 4 -12 7.23 5.2
-10 4 11 129.63 19.53
-10 4 11 129.42 16.24
10 4 -11 119.8 15.75
-10 4 11 121.52 16.89
10 4 -11 116.27 15.95
-10 4 11 114.39 16.38
10 4 -11 113.84 12.78
-10 4 10 4.59 5.87
-10 4 10 7.67 4.57
10 4 -10 6.13 6.46
-10 4 10 -0.83 4.78
10 4 -10 -2.93 6.14
-10 4 10 2.29 4.68
10 4 -10 0.55 3.8
-10 4 9 33.59 10.15
-10 4 9 58.22 10.85
10 4 -9 51.53 10.52
-10 4 9 43.34 10.47
10 4 -9 39.81 9.47
-10 4 9 50.06 11.86
10 4 -9 46.15 8.69
-10 4 8 25.19 8.13
-10 4 8 35.97 8.58
10 4 -8 23.33 7.63
-10 4 8 21.42 7.33
10 4 -8 25.33 7.95
-10 4 8 29.24 10.48
10 4 -8 38.64 7.3
-10 4 7 67.28 12.55
-10 4 7 58.78 10.09
10 4 -7 66.69 11.14
-10 4 7 62.87 13.02
10 4 -7 64.94 8.25
10 4 -7 63.42 11.37
10 4 -7 67.54 9.55
-10 4 7 56.72 12.87
-10 4 6 85.82 14.37
-10 4 6 75.97 12.91
-10 4 6 120.29 13.72
10 4 -6 128.25 14.4
-10 4 6 147.37 19.97
10 4 -6 104.99 14
10 4 -6 131.43 12.04
10 4 -6 118.71 13.04
10 4 -6 111.89 11.33
10 4 -5 26.78 6.02
-10 4 5 7.08 4.94
-10 4 5 32.89 9.38
-10 4 5 26.88 6.53
10 4 -5 27.04 7.55
-10 4 5 20.93 7.53
10 4 -5 21.94 6.57
10 4 -5 22.83 6.71
10 4 -5 26.61 6.06
-10 4 4 85.66 15.97
-10 4 4 76.71 14.65
-10 4 4 73.68 10.24
10 4 -4 76.49 10.82
10 4 -4 64.59 9.69
10 4 -4 85.47 12.53
10 4 -4 82.24 10.61
-10 4 4 61.57 10.63
-10 4 3 54.21 13.13
-10 4 3 41.27 7.77
10 4 -3 52.33 8.91
10 4 -3 43.4 8.21
10 4 -3 51.65 9.36
-10 4 3 63.97 10.62
-10 4 3 42.83 11.37
-10 4 2 120.51 19.28
-10 4 2 125.01 11.52
-10 4 2 128.95 19
10 4 -2 109.88 12.43
-10 4 2 123.3 14.71
-10 4 2 128.97 14.72
10 4 -2 113.96 11.63
10 4 -2 121.9 14.13
-10 4 2 148.4 13.88
-10 4 1 29.64 11.32
-10 4 1 20.08 10.27
-10 4 1 28.31 6.14
10 4 -1 27.14 6.52
10 4 -1 15.77 5.33
-10 4 1 19.23 6.01
-10 4 1 39.35 8.69
10 4 -1 25.35 6.1
-10 4 0 264.95 20.75
-10 4 0 295.33 28.98
-10 4 0 247.94 19.38
-10 4 0 224.87 25.01
-10 4 0 304.99 23.57
-10 4 -1 20.34 9.04
-10 4 -1 15.85 5.96
-10 4 -1 15.19 6.52
10 4 1 11.18 3.91
-10 4 -1 13.21 4.72
-10 4 -1 5.39 6.74
-10 4 -2 130.49 15.91
10 4 2 107.64 12.12
-10 4 -2 147.07 14.48
-10 4 -2 118.46 17.31
10 4 2 169.21 18.85
-10 4 -2 138.51 16.41
-10 4 -2 150.87 20.35
10 4 3 33.94 7.81
-10 4 -3 28.17 9.29
10 4 3 26.51 6.69
-10 4 -3 20.95 5.65
10 4 3 36.02 7.84
-10 4 -3 13.93 8.69
10 4 3 20.8 6.98
-10 4 -3 23.25 7.55
-10 4 -3 35.16 10.98
10 4 3 13.25 4.71
10 4 4 58.96 9.72
-10 4 -4 65.08 12.56
10 4 4 59.38 10.11
10 4 4 58.49 10.53
10 4 4 64.55 9.46
-10 4 -4 77.17 14.48
10 4 4 79.5 14.3
-10 4 -4 62.14 11.55
-10 4 -4 56.65 12.47
10 4 4 81.94 10.32
10 4 5 67.78 12.64
10 4 5 67.08 9.79
-10 4 -5 35.79 10.46
10 4 5 51.56 10.23
10 4 5 49.42 10.78
-10 4 -5 48.74 12.02
10 4 5 52.49 8.25
10 4 5 53.48 8.71
-10 4 -5 40.62 10.95
-10 4 -5 57.02 12.36
10 4 5 76.52 14.01
10 4 6 49.04 12.9
-10 4 -6 43.97 12.97
10 4 6 57.08 10.5
-10 4 -6 27.08 9.03
10 4 6 43.03 7.43
10 4 6 46.24 7.9
-10 4 -6 23.46 7.89
-10 4 -6 31 10.5
10 4 6 47.19 11.3
10 4 7 14.42 8.47
-10 4 -7 7.48 6.31
10 4 7 10.15 5.35
-10 4 -7 22.67 8.48
10 4 7 7.78 3.91
-10 4 -7 10.78 7
-10 4 -7 7.7 5.59
10 4 7 14.37 7.63
10 4 8 12.95 6.21
-10 4 -8 5.07 6.38
10 4 8 5.53 5.75
-10 4 -8 13.71 8.33
-10 4 -8 0.97 5.6
-10 4 -8 1.17 5.83
10 4 8 8.11 7.63
10 4 9 25.67 9.19
-10 4 -9 40 14.36
10 4 9 48.05 10.82
-10 4 -9 55.26 12.32
-10 4 -9 52.99 11.95
-10 4 -9 41.06 10.72
10 4 9 49.71 13.75
10 4 10 2.84 7.08
-10 4 -10 3.69 7.15
10 4 10 0.15 5.62
-10 4 -10 1.79 4.99
-10 4 -10 -0.93 4.53
-10 4 -10 3.3 6.17
10 4 10 9.81 7.57
10 4 11 7.84 9.51
-10 4 -11 11.89 7.27
10 4 11 10.3 6.85
-10 4 -11 28.64 8.92
10 4 11 30.44 12.4
-10 4 -11 2.51 5.33
-10 4 -11 8.96 6.81
10 4 12 -3.21 7.26
10 4 12 -1.33 6.23
-10 4 -12 11.22 10.2
10 4 12 -6.34 8.33
-10 4 -12 22.2 9.87
10 4 13 22.18 8.9
10 4 13 36.44 12.58
10 4 13 28.7 10.16
-10 4 -13 15.42 9.16
10 4 13 32.07 12.14
-10 4 -13 26.69 12.5
10 4 14 35.56 14.2
10 4 14 16.88 10.08
10 4 14 21.41 8.11
-10 4 -14 25.82 13.46
10 4 14 4.77 10.34
-10 4 -14 6.1 7.86
10 4 15 8.33 8.18
10 4 15 -1.52 6.52
10 4 15 -10.8 9.3
-10 4 -15 -0.41 11.82
10 4 15 4.86 7.28
-10 4 -15 18.85 12.44
10 4 16 13.01 10.81
10 4 16 -1.67 7.54
-10 4 -16 9.84 11.29
10 4 16 7.26 6.28
10 4 16 20.05 9.27
-10 4 -16 12.35 10.29
-10 4 -17 -8.36 12.63
10 4 17 13.07 11.62
10 4 17 -8.79 7.95
10 4 17 -1.71 7.88
10 4 17 -7.54 11.2
-10 4 -17 -0.21 8.55
10 4 18 3.82 7.92
10 4 18 -1.98 8
-10 4 -18 -2.61 8.83
-10 4 -18 11.15 13.88
10 4 19 1.26 6.39
10 4 19 4.89 9.12
-10 4 -19 21.73 14.82
-10 4 -19 -11.97 12.51
10 4 20 5.03 8.68
-10 4 -20 -12.45 11.02
-10 4 -20 -4.7 9.31
10 4 20 -3.76 6.46
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-10 5 25 37.35 14.68
10 5 -24 121.87 22.67
-10 5 24 125.52 22.16
-10 5 24 93.41 20.16
10 5 -24 147.15 23.22
10 5 -23 59.51 16.65
10 5 -23 38.68 14.58
-10 5 23 35.85 13.35
-10 5 23 74.72 19.33
10 5 -22 174.33 25.54
10 5 -22 173.9 26
10 5 -22 155.28 24.48
-10 5 22 123.65 21.59
-10 5 22 161.95 25.72
10 5 -21 119.57 21.35
10 5 -21 91.18 18.6
10 5 -21 125.65 22.13
-10 5 21 121.54 20.68
-10 5 21 73.59 17.79
10 5 -20 309.5 32.8
10 5 -20 284.3 33.05
10 5 -20 292.63 31.49
-10 5 20 274.42 30.75
-10 5 20 250.9 31.71
10 5 -19 210.93 26.46
10 5 -19 194.36 27.51
10 5 -19 182.87 24.44
-10 5 19 143.66 22.06
-10 5 19 151.18 24.38
10 5 -18 361.09 33.3
10 5 -18 307.31 31.25
10 5 -18 353.1 35.64
-10 5 18 332.34 32.24
-10 5 18 356.61 36.7
10 5 -17 341.18 26.78
10 5 -17 356.9 32.9
10 5 -17 287.14 29.44
10 5 -17 396.1 37.42
-10 5 17 277.3 31.42
-10 5 17 301.37 30.52
-10 5 16 513.82 34
-10 5 16 508.48 38.96
-10 5 16 448.04 31.55
10 5 -16 443.41 35.8
10 5 -16 472.35 40.65
10 5 -16 449.81 36.2
10 5 -16 483.14 31.25
-10 5 16 486.82 42
-10 5 15 287.54 25.4
-10 5 15 264.61 27.3
-10 5 15 249.65 23.42
10 5 -15 279.78 27.89
10 5 -15 342.44 33.75
10 5 -15 293.44 28.39
10 5 -15 283.46 23.6
-10 5 15 257.18 30.35
-10 5 14 432.36 31.6
-10 5 14 486.5 36.34
-10 5 14 453.5 32.31
10 5 -14 450 34.09
10 5 -14 535.8 41.7
10 5 -14 462.05 34.53
10 5 -14 460.31 29.47
-10 5 14 466.4 41.08
-10 5 13 549.13 36.32
-10 5 13 602.61 39.05
-10 5 13 524.11 35.27
10 5 -13 591.1 38.45
10 5 -13 594.66 43.67
10 5 -13 594.58 39.01
10 5 -13 562.33 32.17
-10 5 13 595.08 44.87
-10 5 12 617.95 38.86
-10 5 12 704.3 41.52
-10 5 12 655.78 39.73
10 5 -12 623.24 39.37
10 5 -12 681.9 46.11
10 5 -12 622.52 39.03
10 5 -12 605.29 32.85
-10 5 12 735.65 48.6
-10 5 11 546.5 36.46
-10 5 11 591.24 37.14
-10 5 11 527.1 35.71
10 5 -11 561.75 36.01
10 5 -11 622.83 42.95
10 5 -11 558.52 36.62
10 5 -11 561.97 30.88
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-10 5 10 906.14 45.42
-10 5 10 883.53 47.05
10 5 -10 883.21 44.84
10 5 -10 909.32 52.24
10 5 -10 888.49 46.05
10 5 -10 822.93 38.02
-10 5 10 895.48 51.45
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-10 5 9 453.89 30.68
-10 5 9 429.32 32.83
10 5 -9 476.29 31.24
10 5 -9 468.48 36.08
10 5 -9 445.32 31.65
10 5 -9 484.93 27.97
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-10 5 8 784.57 45.65
10 5 -8 798.51 41.05
-10 5 8 867.5 47.77
10 5 -8 788.75 42.54
10 5 -8 884.37 38.71
-10 5 8 816.39 46.35
-10 5 7 353.38 25.55
-10 5 7 317.83 28.62
10 5 -7 294.13 23.82
-10 5 7 316.32 28.41
10 5 -7 301.89 19.76
10 5 -7 317.8 25.42
10 5 -7 354.37 23.34
-10 5 7 361.22 28.63
-10 5 6 577.27 32.64
-10 5 6 573.69 38.85
10 5 -6 606.94 33.13
-10 5 6 571.78 38.95
10 5 -6 547.17 27.95
10 5 -6 542.16 33.46
10 5 -6 614.55 31.85
-10 5 6 586.63 36.15
-10 5 5 300.52 22.52
-10 5 5 263.44 26.88
10 5 -5 275.1 21.75
-10 5 5 319.68 29.14
10 5 -5 316.15 24.91
10 5 -5 284.46 19.82
10 5 -5 306.47 22
-10 5 5 254.49 23.28
-10 5 4 905.69 40.28
-10 5 4 784.81 47.47
10 5 -4 821.33 38.43
-10 5 4 824.78 49.28
10 5 -4 810.76 36.42
10 5 -4 842.04 38.57
-10 5 4 840.73 41.75
-10 5 3 338.95 31.5
10 5 -3 395.88 22.65
10 5 -3 336.09 23.33
10 5 -3 357.38 24.42
-10 5 3 390.05 26.88
-10 5 3 411.79 25.77
-10 5 3 357.78 31.98
10 5 -2 769.27 31.26
-10 5 2 808.29 38
-10 5 2 804.76 38.65
-10 5 2 785.8 49.25
-10 5 2 745.52 35.84
-10 5 2 775.9 48.97
10 5 -2 750.3 31.12
-10 5 1 600.26 43
-10 5 1 597.84 29.57
-10 5 1 598.63 42.37
-10 5 1 532.42 30.34
-10 5 1 561.5 31.67
-10 5 0 767.12 48.75
-10 5 0 787.22 38.81
-10 5 0 828.07 37.49
-10 5 0 819.43 37.81
-10 5 0 788.2 48.95
-10 5 -1 493.69 27.56
-10 5 -1 530.6 39.74
-10 5 -1 484.52 30.36
-10 5 -1 448.69 29.05
-10 5 -1 505.15 38.44
-10 5 -2 623.73 36.62
-10 5 -2 627.02 31.09
-10 5 -2 656.4 44.1
10 5 2 591.58 32.82
-10 5 -2 631.41 42.66
-10 5 -2 691.09 37.75
-10 5 -3 615.7 29.61
-10 5 -3 538.1 39.44
10 5 3 585.22 31.65
-10 5 -3 618.77 35.82
10 5 3 582.16 29.91
-10 5 -3 531.56 38.91
-10 5 -3 636.14 39.19
10 5 3 581.09 29.35
10 5 4 462.35 29.63
-10 5 -4 460.76 35.99
10 5 4 448.4 26.75
-10 5 -4 412.7 30.04
10 5 4 461.92 25.72
-10 5 -4 404.16 33.44
-10 5 -4 387.93 32.06
10 5 4 391.45 25.6
-10 5 -5 393 33.6
10 5 5 424.83 28.97
10 5 5 437.91 26.45
-10 5 -5 513.71 38.02
-10 5 -5 478.28 33.46
10 5 5 435.14 25.73
10 5 5 488.47 26.15
-10 5 -5 491.07 36.41
10 5 6 496.49 31.8
-10 5 -6 503.02 35.2
10 5 6 488.22 27.65
-10 5 -6 494.53 36.89
-10 5 -6 482.67 39.04
10 5 6 581.34 27.87
-10 5 -6 538.57 37.84
10 5 7 422.54 29.31
-10 5 -7 386.7 31.79
10 5 7 413.7 24.64
-10 5 -7 406.54 33.29
-10 5 -7 410.55 32.63
-10 5 -7 435.14 38.69
-10 5 -8 609 48.57
10 5 8 672.64 37.95
-10 5 -8 656.1 42.48
-10 5 -8 638.44 40.88
-10 5 -8 562.21 38.32
10 5 8 636.93 43.94
-10 5 -9 196.28 27.32
10 5 9 263.97 23.85
-10 5 -9 313.98 30.07
-10 5 -9 236.17 24.74
-10 5 -9 221.04 23.76
10 5 9 250.19 28.4
10 5 10 376.72 35.17
-10 5 -10 327.61 31.82
-10 5 -10 328.79 35.84
10 5 10 309.73 26.74
-10 5 -10 340.47 28.93
-10 5 -10 303.57 27.28
10 5 10 328.55 32.43
10 5 11 86.14 18.07
-10 5 -11 105.47 18.85
-10 5 -11 93.61 19.76
10 5 11 93.62 15.71
-10 5 -11 94.69 15.32
10 5 11 85.07 17.85
-10 5 -11 81.53 14.27
10 5 11 106.5 20.35
-10 5 -12 266.37 30.76
10 5 12 291.67 26.87
-10 5 -12 245.91 31.58
10 5 12 247.34 28.43
10 5 12 278.63 30.96
10 5 12 289.78 32.17
-10 5 -13 36.47 12.86
10 5 13 38.84 11.89
-10 5 -13 41.47 16.84
10 5 13 14.19 8.78
10 5 13 26.19 10.89
10 5 13 35.34 13.97
-10 5 -14 234.96 29.33
-10 5 -14 211.14 30.94
10 5 14 214.33 24.3
10 5 14 218.97 27.8
10 5 14 227.27 29.03
10 5 14 246.77 31.33
-10 5 -15 20.07 12.47
10 5 15 5.41 10.18
-10 5 -15 23.92 13.25
10 5 15 18.43 7.65
10 5 15 21.96 9.84
10 5 15 18.3 10.51
-10 5 -16 172.35 27.26
10 5 16 177.78 25.7
-10 5 -16 175.39 28.63
10 5 16 177.38 22.87
10 5 16 127.98 22.2
10 5 16 169.01 26.59
-10 5 -17 34.56 15.62
10 5 17 31.54 13.2
-10 5 -17 27.54 15.04
10 5 17 9.89 6.86
10 5 17 11.78 11.77
10 5 17 5.28 7.79
10 5 18 213.45 28.58
10 5 18 149.54 22.58
-10 5 -18 171.74 28.85
-10 5 -18 161.8 27.5
10 5 19 35.62 13.59
10 5 19 32 11.56
-10 5 -19 5.11 8.1
-10 5 -19 27.56 15.07
10 5 20 100.97 20.87
-10 5 -20 107.91 24.1
10 5 20 108.96 20.27
-10 5 -20 111.41 23.07
10 6 -24 17.1 10.97
10 6 -24 3.98 8.16
-10 6 24 -6.79 9.4
-10 6 24 12.78 7.42
10 6 -23 44.76 15.43
10 6 -23 42.63 14.16
-10 6 23 34.69 14.27
-10 6 23 47.13 15.59
10 6 -22 4.53 10.37
10 6 -22 5.17 9.59
-10 6 22 1.36 6.47
-10 6 22 8.04 9.11
-10 6 21 74.29 17.4
10 6 -21 54.59 15.57
10 6 -21 51.36 15.83
-10 6 21 34.04 13.12
10 6 -21 21.1 10.49
-10 6 20 5.57 8.46
10 6 -20 1.84 7.79
10 6 -20 -4.38 8.11
-10 6 20 8.35 8.54
10 6 -20 6.6 9.88
-10 6 19 53.81 15.64
10 6 -19 30.47 11.66
10 6 -19 67.7 13.68
10 6 -19 76.26 16.19
-10 6 19 46.92 13.98
10 6 -19 76.89 18.72
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10 6 -18 25.55 10.6
10 6 -18 23.04 9.57
10 6 -18 26.53 11.54
-10 6 18 21.63 9.29
10 6 -18 44.29 13.84
-10 6 17 65.65 16.74
10 6 -17 77.22 15.86
10 6 -17 72.65 13.61
10 6 -17 79.87 16.45
10 6 -17 95.28 19.76
-10 6 17 79.18 17.21
-10 6 16 42.56 10.49
-10 6 16 35.71 10.93
-10 6 16 38.45 13.79
10 6 -16 16.07 8.41
10 6 -16 27.05 8.29
10 6 -16 23.72 11.67
-10 6 16 45.14 10.17
10 6 -16 29.12 12.41
-10 6 15 27.38 7.65
-10 6 15 28.42 10.05
-10 6 15 34.09 12.21
10 6 -15 26.29 9.57
10 6 -15 31.39 8.98
10 6 -15 52.9 13.48
-10 6 15 30.8 9.99
10 6 -15 18.04 8.65
-10 6 14 5.56 6.47
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-10 6 14 1.41 6.99
10 6 -14 5.16 7
10 6 -14 8.7 5.66
10 6 -14 -0.7 6.93
-10 6 14 0.82 5.11
10 6 -14 -14.23 10.81
-10 6 13 59.55 11.76
-10 6 13 58.49 13.03
-10 6 13 54.95 14.59
10 6 -13 51.97 12.32
10 6 -13 43.98 9.61
10 6 -13 78.52 15.2
-10 6 13 65.43 12.55
10 6 -13 53.17 14.94
-10 6 12 15.92 8.28
-10 6 12 19.69 7.95
-10 6 12 18.1 9.21
10 6 -12 32.14 9.86
10 6 -12 22.73 6.84
10 6 -12 32.85 9.26
-10 6 12 25.66 8.57
10 6 -12 42.35 12.85
-10 6 11 33.15 10.06
-10 6 11 54.35 12.33
-10 6 11 34.78 11.41
10 6 -11 55.66 12.67
10 6 -11 32.69 8.33
10 6 -11 39.44 11.41
-10 6 11 37.37 10.56
10 6 -11 57.02 15.66
-10 6 10 -0.01 4.93
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10 6 -10 15.35 7.06
10 6 -10 12.67 5.34
10 6 -10 -4.51 6.34
-10 6 10 15.6 8.25
10 6 -10 14.11 9.46
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10 6 -9 14.75 5.86
10 6 -9 19.69 6.73
10 6 -9 17.9 6.8
-10 6 9 15.3 6.62
10 6 -9 33.44 10.92
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-10 6 8 30.19 8.5
-10 6 8 40.01 10.76
10 6 -8 31.97 8.28
10 6 -8 14.41 5.09
10 6 -8 37.54 10
10 6 -8 22.08 5.57
-10 6 8 49.14 11.92
10 6 -8 26.93 8.58
-10 6 7 6.47 5.14
-10 6 7 6.12 4.41
-10 6 7 22.94 9.17
10 6 -7 7.36 4.68
10 6 -7 10.43 4.24
10 6 -7 9.07 6.19
10 6 -7 14.06 4.1
10 6 -7 16.87 7.35
-10 6 6 39.54 11.55
-10 6 6 33.61 8.8
-10 6 6 22.85 7.55
10 6 -6 36.35 8.95
10 6 -6 16.02 5.37
10 6 -6 28.22 8.11
10 6 -6 27.01 6.02
10 6 -6 43.57 10.63
-10 6 6 7.69 5.57
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-10 6 5 108.41 14.31
-10 6 5 78.09 12.93
10 6 -5 80.52 12.39
10 6 -5 127.69 16.72
10 6 -5 114.62 14.25
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10 6 -5 99.04 12.24
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-10 6 4 33.32 10.96
-10 6 4 35.14 8.06
10 6 -4 31.27 6.83
10 6 -4 37.65 8.89
10 6 -4 19.49 7.6
10 6 -4 33.1 7.33
10 6 -4 31.22 8.82
-10 6 4 35.69 8.22
-10 6 3 89.25 17
-10 6 3 86.09 12.24
10 6 -3 91 10.84
10 6 -3 103.16 14.18
10 6 -3 96.8 13.25
10 6 -3 102.27 13.19
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10 6 -2 56.11 8.15
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10 6 -2 42.85 7.14
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10 6 -2 55.84 9.66
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10 6 -1 54.76 9.96
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10 6 0 112.04 12.99
-10 6 -1 8.43 4.08
-10 6 -1 14.98 5.7
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10 6 1 5.01 4.85
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10 6 1 14.68 5.04
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-10 6 -2 255.2 22.08
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10 6 2 272.03 22.15
-10 6 -2 263.45 28
-10 6 -2 231.69 22.27
10 6 3 23.27 7.19
-10 6 -3 9.02 5.93
-10 6 -3 26.55 7.84
10 6 3 23.11 6.6
-10 6 -3 25.09 10.57
-10 6 -3 43.43 11.89
10 6 4 177.77 17.71
-10 6 -4 161.99 18.71
10 6 4 145.99 15.82
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10 6 4 137.82 13.43
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10 6 5 0.04 4.75
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10 6 5 7.66 5.19
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10 6 5 1.96 3.07
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10 6 6 8.72 4.42
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10 6 6 2.08 3.61
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10 6 7 5.15 5.18
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10 6 7 -0.41 3.34
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10 6 8 1.97 5.46
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10 6 9 0.91 4.38
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-10 6 -9 5.24 6.37
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10 6 9 3.95 6.45
10 6 10 30.53 13.22
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10 6 10 9.48 5.2
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-10 6 -10 23.32 8.57
-10 6 -10 17.72 8.34
10 6 10 11.32 7.8
10 6 11 14.65 9.62
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10 6 11 -2.35 5.19
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10 6 11 -2.55 8.56
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10 6 12 10.25 6.37
10 6 12 16.84 10.36
10 6 12 31.66 13.62
10 6 12 17.08 7.97
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10 6 13 23.44 10.87
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10 6 13 -9.29 7.24
10 6 13 1.32 6.9
10 6 13 15.49 9.93
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10 6 14 6.25 7.23
-10 6 -14 10.55 8.04
10 6 14 9.16 6.71
10 6 14 -8.73 11.77
10 6 14 26.77 11.27
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10 6 15 -14.92 11.19
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10 6 15 4.53 6.8
10 6 15 -1.58 8.79
10 6 15 -12.92 8.19
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10 6 16 4.01 8.32
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10 6 16 12.21 8.14
10 6 16 19.57 11.31
10 6 16 14.9 11.73
-10 6 -17 3.88 10.57
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10 6 17 4.47 9.63
10 6 17 15.64 11.8
10 6 17 -8.23 7.67
10 6 18 17.98 10.97
10 6 18 7.37 6.93
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-10 6 -18 18.24 13.08
10 6 19 24 11.63
-10 6 -19 13.57 12.8
10 6 19 17.08 9.27
-10 6 -19 40.75 18.17
10 6 20 44.34 14.27
10 7 -24 216.64 29.32
10 7 -24 200.03 28.96
-10 7 24 154.1 25.31
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10 7 -23 0.41 8.42
10 7 -23 8.67 9.68
-10 7 23 10.6 10.34
-10 7 23 11.56 6.91
10 7 -22 287.62 32.06
10 7 -22 266.93 33.01
-10 7 22 272.37 33.53
-10 7 22 263.57 32.37
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10 7 -21 11.67 10.27
10 7 -21 -3.32 8.13
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10 7 -21 7.71 7.37
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10 7 -20 245.33 30.16
10 7 -20 327.61 29.78
10 7 -20 358.05 35.82
-10 7 20 333.84 35.27
10 7 -20 337.35 37.32
-10 7 19 24.97 11.47
10 7 -19 35.14 12.71
10 7 -19 47.8 12.4
10 7 -19 45 13.53
-10 7 19 27.62 11.78
10 7 -19 37.11 13.91
-10 7 18 387.52 37.48
10 7 -18 375.33 34.84
10 7 -18 438.08 33.32
10 7 -18 410.8 35.82
-10 7 18 363.67 36.13
10 7 -18 435.93 41.21
-10 7 17 38.18 13.04
10 7 -17 21.77 10.19
10 7 -17 21.24 7.6
10 7 -17 14.85 9.49
10 7 -17 42.88 15.87
-10 7 17 22.71 10.3
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-10 7 16 635.21 46.68
-10 7 16 619.96 46.53
10 7 -16 606.19 43.14
10 7 -16 608.51 37.93
10 7 -16 604.2 42.44
10 7 -16 640.36 49.16
-10 7 16 579.37 36.92
-10 7 15 74.93 13.63
-10 7 15 110.55 18.56
-10 7 15 62.03 14.92
10 7 -15 76.29 15.8
10 7 -15 77.57 12.87
10 7 -15 96.5 17.76
10 7 -15 85.39 18.54
-10 7 15 79.39 14.82
-10 7 14 744.09 43.19
-10 7 14 781.06 49.11
-10 7 14 703.52 48.56
10 7 -14 748.85 46.05
10 7 -14 736.16 40.13
10 7 -14 737.13 45.6
10 7 -14 706.84 50.49
-10 7 14 733.59 42.39
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-10 7 13 85.75 15.9
-10 7 13 70.8 16.27
10 7 -13 95.83 16.19
10 7 -13 83.48 13.43
10 7 -13 55.08 13.23
10 7 -13 109.9 19.08
-10 7 13 84.87 14.76
-10 7 12 512.81 35.89
-10 7 12 508.47 37.6
-10 7 12 558.17 42.82
10 7 -12 496 35.57
10 7 -12 553.89 33.47
10 7 -12 528.14 36.98
10 7 -12 593.34 44.43
-10 7 12 514.15 35.71
-10 7 11 99.37 16.01
-10 7 11 81.03 14.81
-10 7 11 119.4 19.18
10 7 -11 91.9 15.34
10 7 -11 91.66 13.1
10 7 -11 102.73 16.34
10 7 -11 134.11 21.28
-10 7 11 91.02 15.27
-10 7 10 564.24 38.31
-10 7 10 544.43 37.04
-10 7 10 592.43 42
10 7 -10 570.88 37.41
10 7 -10 542.14 32.67
10 7 -10 597.43 38.22
10 7 -10 520.58 39.49
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10 7 -9 59.43 11.73
10 7 -9 62.91 11.37
10 7 -9 65.73 12.8
10 7 -9 46.04 11.5
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-10 7 8 419.99 32.51
10 7 -8 433.66 31
10 7 -8 459.12 29.41
10 7 -8 437.88 25.45
10 7 -8 456.11 32.66
10 7 -8 512.09 37.47
-10 7 8 464.21 34.71
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10 7 -7 75.22 13.23
10 7 -7 59.04 10.74
10 7 -7 76.73 12.91
10 7 -7 63.19 9.81
10 7 -7 76.51 13.84
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10 7 -6 458.59 30.71
10 7 -6 471.71 30.07
10 7 -6 507.67 28.93
10 7 -6 491.24 34.61
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10 7 -5 31.53 8.65
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10 7 -5 25.81 7.58
10 7 -5 31.45 9.16
10 7 -5 30.23 8.33
10 7 -5 41.78 8
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10 7 -4 671.18 33.52
10 7 -4 589.91 34.7
10 7 -4 653.46 34.58
10 7 -4 659.5 37.81
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10 7 -3 120.28 12.03
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10 7 -3 118.5 12.89
10 7 -3 128.37 15.92
10 7 -3 121.55 15.81
10 7 -3 131.43 15.31
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10 7 -2 721.51 37.14
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10 7 -2 724.27 38.4
10 7 -2 682.29 31.83
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-10 7 1 116.25 14.25
10 7 -1 143.37 15.58
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10 7 -1 121.58 13.39
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10 7 0 660.26 32.6
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10 7 1 142.31 17.46
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10 7 2 1059.82 44.99
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10 7 2 949.73 45.67
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10 7 3 79.92 12.04
10 7 3 108.21 14.52
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10 7 4 1115.28 48.23
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10 7 4 1011.89 46.49
10 7 4 1140.13 41.98
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10 7 5 99.72 13.7
10 7 5 102.52 13.91
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10 7 5 110.84 17.51
-10 7 -6 991.96 50.73
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10 7 6 930.59 52.77
10 7 6 1035.17 46.63
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10 7 6 1042.97 45.11
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-10 7 -7 45.31 13.23
10 7 7 59.38 11.03
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10 7 7 41.03 9.7
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10 7 7 48.41 13.19
-10 7 -8 711.6 44.13
-10 7 -8 626.24 48.79
10 7 8 683.79 44.87
10 7 8 653.19 37.19
-10 7 -8 608.9 41.39
10 7 8 668.37 34.95
-10 7 -8 649.92 42.79
-10 7 -9 52.99 12.65
-10 7 -9 50.47 13.95
-10 7 -9 41.5 11.23
10 7 9 44.67 9.9
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10 7 9 5.86 7.91
-10 7 -10 383.13 38.58
10 7 10 503.63 40.19
-10 7 -10 434.71 36.15
-10 7 -10 480.28 35.71
-10 7 -10 429.29 33.68
10 7 10 457.83 32.51
-10 7 -11 8.27 7.73
10 7 11 22.32 9.58
-10 7 -11 22.3 10.19
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-10 7 -11 21.18 8.53
10 7 11 35.74 9.71
-10 7 -12 381.09 35.79
-10 7 -12 363.94 39.09
10 7 12 429.83 39.36
10 7 12 425.61 32.4
10 7 12 368.82 35.57
-10 7 -13 11.55 9.98
10 7 13 16.41 9.55
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10 7 13 -4.87 9.66
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10 10 -13 90.5 16.36
10 10 -13 65.52 15.76
10 10 -13 79.62 14.93
10 10 -12 5.2 7.37
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10 10 -12 2.51 6.51
10 10 -12 15.01 9.62
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10 10 -12 25.02 12.03
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10 10 -12 14.05 8.62
10 10 -11 103.17 19.42
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10 10 -11 82.7 16.83
10 10 -11 59.98 14.22
-10 10 11 88.97 15.42
10 10 -11 54.62 12.61
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10 10 -11 78.98 14.38
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10 10 -10 3.85 7.41
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10 10 -10 24.14 9.66
10 10 -10 14.51 6.66
10 10 -10 16.16 8.57
10 10 -10 7.6 6.12
10 10 -9 41.62 12.22
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10 10 -9 21.85 8.92
10 10 -9 23.16 10.16
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10 10 -9 42.97 12.63
10 10 -9 30.08 8.08
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10 10 -9 18.47 7.94
10 10 -8 44.57 12.15
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10 10 -8 39.89 10.45
10 10 -8 48.04 12.35
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10 10 -8 23.11 5.31
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10 10 -8 51.73 12.24
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10 10 -7 64.74 12.99
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10 10 -7 63.08 13.86
10 10 -7 53.4 11.03
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10 10 -7 47.33 11.34
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10 10 -6 21.99 8.73
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10 10 -6 33.98 9.91
10 10 -6 20.89 7.3
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10 10 -6 17.72 7.62
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10 10 -5 88.52 13.9
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10 10 -5 83.77 13.72
10 10 -5 81.73 13.18
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10 10 -5 83.86 14.67
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10 10 -4 11.61 6.37
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10 10 -4 4.44 4.87
10 10 -4 16.44 8.95
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10 10 -4 6.3 5.08
10 10 -3 23.33 7.85
10 10 -3 25.37 7.11
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10 10 -3 23.81 7.17
10 10 -3 12.3 6.1
10 10 -3 25.87 7.55
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10 10 -2 97.07 13.53
10 10 -2 112.97 15.78
10 10 -2 102.46 16.04
10 10 -2 98.79 13.58
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10 10 -1 35.48 10.52
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10 10 -1 43.84 9.46
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10 10 0 23.04 9.58
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10 10 0 39.68 9.84
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10 10 1 37.42 10.1
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10 10 1 38.69 10.46
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10 10 1 44.08 9.74
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10 10 2 24.23 8.98
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10 10 5 29.88 8.92
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10 10 5 21.4 9.18
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10 10 6 13.47 6.32
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10 10 7 -5.62 6.79
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10 10 8 14.89 7.5
10 10 8 11.2 10.1
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10 10 9 13.52 7.72
10 10 9 6.52 7.27
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10 10 10 -8.55 8.7
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10 10 11 6.24 7.66
10 10 12 10.98 10.79
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10 10 13 19.96 13.21
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10 10 15 -2.43 8.92
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10 10 16 12.1 11.92
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10 10 17 4.47 7.86
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10 11 -22 158.01 23.73
10 11 -21 72.6 18.93
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10 11 -21 63.69 17.16
10 11 -21 61.19 15.56
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10 11 -20 200.46 28.98
-10 11 20 179.26 28.8
10 11 -20 173.69 25.44
10 11 -20 230.66 27.89
-10 11 20 194.1 27.31
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10 11 -19 90.48 19.28
-10 11 19 81.19 20.48
10 11 -19 114.58 22.76
10 11 -19 98.62 18.13
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10 11 -18 228.96 34.83
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10 11 -18 131.73 22.94
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10 11 -18 176.01 25.04
10 11 -18 174.74 23.13
-10 11 18 132.74 22.6
10 11 -17 213.5 25.53
10 11 -17 212.09 27.09
-10 11 17 125.8 24.41
10 11 -17 211.22 31.18
-10 11 17 208.98 27.8
10 11 -17 213.56 27.95
-10 11 17 193 26.62
10 11 -17 152.89 25.96
10 11 -16 225.47 25.1
10 11 -16 203.56 26.72
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10 11 -16 222.51 32.23
-10 11 16 218.82 28.97
10 11 -16 222.14 27.79
-10 11 16 202.66 26.84
10 11 -16 197.94 28.74
10 11 -15 249.74 32.06
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10 11 -15 184.91 27.68
10 11 -15 185.07 25.2
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10 11 -15 180.21 23.73
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10 11 -15 194.86 23.69
10 11 -14 370.93 37.94
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10 11 -14 393.76 39.89
10 11 -14 369.65 34.39
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10 11 -14 333.76 32.89
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10 11 -14 315.56 29.64
10 11 -13 145.89 23.62
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10 11 -13 119.43 21.91
10 11 -13 128.43 20.47
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10 11 -13 110.88 18.37
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10 11 -13 116.83 18.16
10 11 -12 471.11 41.05
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10 11 -12 492.39 41.59
10 11 -12 384.84 34.38
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10 11 -12 422.17 35.46
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10 11 -12 385.04 31.95
10 11 -11 215.22 26.8
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10 11 -11 232.57 28.19
10 11 -11 225.58 25.67
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10 11 -11 196.28 24.04
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10 11 -11 229.58 24.45
10 11 -10 520.97 40.71
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10 11 -10 550.56 41.65
10 11 -10 484.45 38.06
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10 11 -10 467.9 31.12
10 11 -10 436.22 36.3
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10 11 -10 460.89 34.67
10 11 -9 259.86 28.09
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10 11 -9 288.84 28.84
10 11 -9 267.91 28.23
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10 11 -9 291.09 24.77
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10 11 -9 285.62 26.83
10 11 -8 517.15 38.96
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10 11 -8 552.9 39.44
10 11 -8 541.5 39.05
10 11 -8 514.49 33.29
10 11 -8 531.04 36.97
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10 11 -7 274.84 26.48
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10 11 -7 247.26 23.39
10 11 -7 208.89 23.54
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10 11 -6 652.75 41.12
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10 11 -6 621.28 39.01
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10 11 -6 513.57 34.41
10 11 -6 522.98 37.48
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10 11 -5 223.37 23.09
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10 11 -5 230.73 22.64
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10 11 -5 219.25 22.45
10 11 -5 211.05 23.12
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10 11 -4 735.83 41.09
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10 11 -4 737.97 40.44
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10 11 -4 748.38 43.39
10 11 -4 706.74 43.85
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10 11 -3 320.29 25.32
10 11 -3 335.97 31.17
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10 11 -3 320.3 25.03
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10 11 -3 320.25 28.01
10 11 -3 321.23 29.89
10 11 -3 295.13 23.18
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10 11 -2 484.8 31.1
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10 11 -2 446.81 34.69
10 11 -2 466.12 35.51
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10 11 -2 519.88 38.61
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10 11 -1 333.2 28.5
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10 11 -1 348.26 30.4
10 11 -1 324.86 30.47
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10 11 0 434.95 33.22
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10 11 1 315.79 28.94
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10 11 2 388.74 31.98
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10 11 2 503.83 35.97
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10 11 3 206.08 24.26
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10 11 3 205.87 23.5
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10 11 5 167.72 22.15
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10 11 5 239.11 23.86
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10 11 6 256.85 28.54
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10 11 6 224.86 23.72
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10 11 6 284.64 30.2
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10 11 7 305.73 26.9
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10 11 8 256.12 24.7
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10 11 8 261.37 30.08
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10 11 9 81.34 14.52
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10 11 10 211.54 22.48
10 11 10 193.42 26.22
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10 11 11 45.84 12.98
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10 11 13 62.28 17.75
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10 11 14 208.07 29.98
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10 11 16 66.98 17.97
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10 12 -18 4.49 10.75
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10 12 -1 1.46 5.88
10 12 -1 3.89 6
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10 12 1 27.42 9.75
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10 12 2 7.76 6.94
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10 12 2 8.31 5.93
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10 12 6 28.47 10.38
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10 12 6 39.03 11.46
-10 12 -6 11.9 6.38
10 12 6 1.21 6.7
-10 12 -7 89.32 14.77
-10 12 -7 93.94 19.14
10 12 7 46.24 13.08
-10 12 -7 103 18.16
10 12 7 91.38 15.47
-10 12 -7 83.68 18.1
10 12 7 59.8 15.04
-10 12 -8 15.55 8.56
-10 12 -8 5.81 6.95
10 12 8 7.54 9.22
-10 12 -8 -1.15 7.44
10 12 8 16.76 8.31
-10 12 -8 5.31 6.79
10 12 8 15.28 10.48
-10 12 -9 55.66 13.34
-10 12 -9 40.68 12.64
-10 12 -9 61.45 15.35
-10 12 -9 50.18 13.58
10 12 9 51.58 11.59
10 12 9 50.91 13.02
-10 12 -10 -2.25 6.06
-10 12 -10 -6.57 9.13
-10 12 -10 0.7 5.9
-10 12 -10 -0.46 6.24
10 12 10 15.15 8.18
10 12 10 20.68 12.37
10 12 11 35.45 13.53
-10 12 -11 43.44 11.99
-10 12 -11 29.87 13.59
10 12 12 -7.28 10.34
-10 12 -12 9.24 8.62
-10 12 -12 14.06 11.28
10 12 13 20.03 12.91
-10 12 -13 17.89 10.11
-10 12 -13 18.83 10.85
10 12 14 -9.21 11.49
-10 12 -14 14.6 10.48
-10 12 -14 -0.97 7.86
10 12 15 3.48 11.67
-10 12 -15 11.03 8.45
-10 12 -15 -3.79 10.47
-10 12 -16 -10.7 9.34
-10 12 -16 -0.5 10.9
-10 13 20 33.06 11.01
10 13 -20 57.03 15.18
-10 13 19 84.34 18.15
10 13 -19 111.49 20.79
-10 13 19 88.13 18.84
10 13 -19 84.89 19.34
-10 13 19 94.46 22.53
10 13 -19 113.24 20.57
-10 13 18 54.43 15.08
10 13 -18 51.24 14.22
-10 13 18 40.56 13
10 13 -18 50.98 15.66
-10 13 18 43.66 15.18
10 13 -18 45.84 13.81
-10 13 17 112.55 20.58
10 13 -17 140.79 22.96
-10 13 17 167.25 25.51
10 13 -17 125.64 21.89
-10 13 17 100.85 23.3
10 13 -17 144.47 21.78
-10 13 16 102.29 20.21
-10 13 16 70.68 18.02
10 13 -16 77.75 17.88
10 13 -16 109.57 20.7
10 13 -16 93.99 18.11
-10 13 16 104.21 22.89
10 13 -15 248.55 32.34
-10 13 15 246.25 27.44
-10 13 15 194.92 29.68
10 13 -15 238.92 32.38
10 13 -15 201.41 26.24
-10 13 15 193.24 24.1
10 13 -15 224.57 27.68
-10 13 15 178.39 25.29
10 13 -15 200.43 25.07
10 13 -14 136.22 23.25
-10 13 14 124.63 19.4
-10 13 14 135.6 24.84
10 13 -14 170.09 27.13
10 13 -14 173.03 24.6
-10 13 14 162.11 22.32
10 13 -14 172.59 25.32
-10 13 14 162.95 23.58
10 13 -14 154.77 21.96
10 13 -13 352.2 37.52
-10 13 13 384.55 34.35
-10 13 13 383.23 39.93
10 13 -13 382.55 39.47
10 13 -13 343.65 34.99
-10 13 13 359.76 33.13
10 13 -13 329.76 33.31
-10 13 13 364.46 34.95
10 13 -13 322.08 31.91
10 13 -12 169.57 24.64
-10 13 12 153.68 21.11
-10 13 12 133.07 23.17
10 13 -12 184.74 26.53
10 13 -12 170.64 24.74
-10 13 12 181.74 23.76
10 13 -12 151.92 22.66
-10 13 12 155.37 22.6
10 13 -12 175 23.34
10 13 -11 367.1 36.15
-10 13 11 370.48 34
-10 13 11 332.57 35.82
10 13 -11 367.43 36.62
10 13 -11 309.34 32.63
-10 13 11 383.21 34.13
10 13 -11 320.7 33.04
-10 13 11 371.69 34.46
10 13 -11 366.43 33.22
10 13 -10 279.89 30.56
-10 13 10 244.88 27.3
-10 13 10 272.8 32.7
10 13 -10 259.49 29.83
10 13 -10 210.79 25.91
-10 13 10 202.41 24.69
10 13 -10 233.04 27.71
10 13 -10 213.5 22.81
-10 13 10 219.68 25.97
10 13 -10 230.63 26.14
10 13 -9 366.47 34.34
-10 13 9 344.72 32.67
-10 13 9 329.99 35.33
10 13 -9 325.6 32.18
10 13 -9 287.71 30.46
-10 13 9 334.43 31.86
10 13 -9 300.68 27.33
-10 13 9 267.09 28.34
10 13 -9 325.98 31.27
-10 13 8 421.51 35.93
-10 13 8 380.12 37.24
10 13 -8 374.22 34.06
-10 13 8 418.72 36.16
10 13 -8 457.15 37.07
10 13 -8 371.35 30.06
-10 13 8 343.41 30.98
10 13 -8 348.63 31.97
-10 13 7 377.05 34.28
-10 13 7 330.41 33.9
10 13 -7 313.26 30.42
-10 13 7 358.56 33.63
10 13 -7 342.71 31.13
10 13 -7 311.17 28.7
-10 13 7 353.87 30.34
10 13 -7 344.09 31.83
-10 13 6 500.85 41.85
10 13 -6 607.25 40.63
-10 13 6 515.55 40.52
10 13 -6 557.98 44.71
10 13 -6 542.48 38.7
10 13 -6 518.76 37.34
10 13 -6 549.29 40.12
-10 13 6 533.44 41.91
-10 13 5 485.8 40.98
10 13 -5 478.62 35.22
-10 13 5 543.21 41.57
10 13 -5 531.17 36.34
10 13 -5 487.9 36.51
10 13 -5 521.52 39.67
-10 13 5 528.47 41.21
10 13 -5 563.42 43.86
10 13 -4 606.93 38.77
-10 13 4 581.33 43.67
-10 13 4 522.21 41.82
10 13 -4 624.51 46.18
10 13 -4 499.35 37.63
10 13 -4 519.83 40.36
-10 13 4 570.47 43.64
-10 13 3 345.69 30.99
-10 13 3 356.89 34.04
-10 13 3 315.06 27.84
10 13 -3 327.88 30.67
-10 13 3 344.28 33.93
10 13 -3 357.81 34.11
10 13 -3 318.83 31.94
-10 13 2 525.99 37.22
-10 13 2 515.93 41.35
10 13 -2 517.83 35.22
-10 13 2 528.92 36.78
10 13 -2 477.33 37.77
-10 13 2 492.14 41.08
10 13 -2 508.9 40.32
10 13 -2 591.99 43.12
-10 13 1 357.33 30.66
-10 13 1 311.1 31.83
10 13 -1 385.06 30.88
-10 13 1 299.72 27.69
10 13 -1 246.34 27.41
10 13 -1 318.91 32.41
-10 13 1 298.9 31.86
10 13 -1 359.87 33.21
10 13 0 261.17 27.92
-10 13 0 229.2 28.1
-10 13 0 253.1 25.8
-10 13 0 206.06 23.12
10 13 0 167.72 20.55
-10 13 0 199.2 25.35
10 13 0 235.85 28.2
10 13 0 212.06 26.76
10 13 1 390.47 33.7
10 13 1 374.25 35.16
10 13 1 317.37 29.36
-10 13 -1 384.27 36.28
10 13 1 386.53 33.83
-10 13 -1 387.68 37.07
-10 13 -1 359.28 29.61
10 13 2 182.49 23.19
10 13 2 198.95 25.9
-10 13 -2 174.73 25.28
10 13 2 193.65 23.66
10 13 2 241.41 26.51
-10 13 -2 175.52 24.86
10 13 3 385.43 34.08
-10 13 -3 345.73 35.78
10 13 3 350.06 35.35
-10 13 -3 358.58 36.56
10 13 3 391.69 33.31
10 13 3 414.98 36.52
10 13 4 125.73 20.41
-10 13 -4 86.3 16.45
10 13 4 52.96 15.33
10 13 4 137.55 21.43
-10 13 -4 119.54 20.74
10 13 4 130.51 18.98
-10 13 -4 132.31 21.86
10 13 5 265.54 30.25
-10 13 -5 205.63 27.93
10 13 5 253.96 31.76
10 13 5 265.96 30.1
-10 13 -5 269.44 31.07
10 13 5 260.18 27.08
-10 13 -5 229.82 28.59
10 13 6 109.59 20.42
-10 13 -6 105.1 20.04
10 13 6 112.68 21.4
10 13 6 121.42 21.55
-10 13 -6 92.02 18.34
10 13 6 156.88 20.42
-10 13 -6 112.19 20.19
10 13 7 181.4 25.31
-10 13 -7 141.83 23.34
10 13 7 127.38 23.52
10 13 7 65.25 15.6
-10 13 -7 99.01 17.8
10 13 7 94.03 16.9
-10 13 -7 112.15 19.26
-10 13 -8 69.11 17.72
10 13 8 51.25 15.99
-10 13 -8 57.45 14.2
10 13 8 73.37 14.13
-10 13 -8 46.53 13.48
10 13 8 61.31 15.74
-10 13 -9 157.14 25.88
10 13 9 146.62 24.05
-10 13 -9 143.08 21.38
-10 13 -9 171.55 23.08
10 13 9 170.35 22.43
10 13 9 173.56 26.72
-10 13 -10 80.6 19.64
-10 13 -10 95.54 18.2
10 13 10 68.55 18.58
-10 13 -10 71.3 18.01
10 13 10 82.15 15.37
10 13 10 109.38 22.23
-10 13 -11 183.09 28.38
10 13 11 177.61 28.6
-10 13 -11 168.93 23.08
10 13 11 177.63 26.86
-10 13 -12 63.25 19.01
10 13 12 100.63 22.84
10 13 12 87.11 19.76
-10 13 -12 80.64 17.47
10 13 13 157.51 26.73
-10 13 -13 177.59 24.86
-10 13 -13 158.36 27.69
10 13 14 82.93 19.76
-10 13 -14 88.18 18.59
-10 13 -14 51.49 17.18
10 13 15 95.84 21
-10 13 -15 69.71 17.99
-10 13 -15 40.84 14.51
10 14 -19 -2.31 8.86
-10 14 18 17.07 11.09
10 14 -18 19.66 10.56
-10 14 18 -1.52 8.53
10 14 -18 0.81 8.94
-10 14 18 -3.28 9.7
10 14 -18 -11.16 10.71
-10 14 17 -6.06 8.97
10 14 -17 -10.79 11.54
-10 14 17 -1.96 7.4
10 14 -17 5.19 9.54
-10 14 17 0.04 9.85
10 14 -17 12.99 8.24
-10 14 16 28.99 12.18
-10 14 16 4.58 6.87
10 14 -16 18.38 11.6
10 14 -16 17.32 11.47
10 14 -16 -2.77 7.5
-10 14 16 6.86 7.85
-10 14 15 6.9 8.55
-10 14 15 8.33 7.03
10 14 -15 3.08 7.92
-10 14 15 10.24 7.64
10 14 -15 17.74 10.38
10 14 -15 8.27 9.83
-10 14 15 8.46 7.76
10 14 -14 54.37 16.97
-10 14 14 32.92 10.59
-10 14 14 28.56 12.2
10 14 -14 37.57 14.87
10 14 -14 31.15 11.32
-10 14 14 27.93 10.29
10 14 -14 25.89 10.77
-10 14 14 35.56 12.9
10 14 -14 48.37 14.49
10 14 -13 21.06 10.4
-10 14 13 8.66 7.19
-10 14 13 21.66 10.73
10 14 -13 8.04 7.53
10 14 -13 12.74 8.25
-10 14 13 23.48 10.46
10 14 -13 -3.16 7.73
-10 14 13 17.17 8.97
10 14 -13 5.16 8.37
10 14 -12 56.77 16.28
-10 14 12 68.24 14.93
-10 14 12 49.69 14.7
10 14 -12 43.86 14.29
10 14 -12 62.87 16.19
-10 14 12 64.13 15.39
10 14 -12 67.03 16.68
-10 14 12 43.21 12.1
10 14 -12 61.11 16.65
10 14 -11 42.3 12.38
-10 14 11 36.14 11.29
-10 14 11 17.15 11.44
10 14 -11 5.54 8.24
10 14 -11 16.4 9.12
-10 14 11 37.5 12.13
10 14 -11 10.36 9.59
10 14 -11 17.73 9.29
-10 14 11 20.36 10.09
10 14 -11 12.38 9.5
10 14 -10 59.91 15.48
-10 14 10 25.69 9.99
-10 14 10 38.51 13.82
10 14 -10 38.47 13
10 14 -10 47.22 13.68
-10 14 10 32.16 11.82
10 14 -10 24.27 9.92
-10 14 10 45.06 11.64
10 14 -10 30.43 11.71
10 14 -9 14.06 8.63
-10 14 9 34.87 10.45
-10 14 9 4.15 6.66
10 14 -9 14.3 8.69
10 14 -9 13.53 8.74
-10 14 9 14.54 9.43
10 14 -9 30.81 10
-10 14 9 30.13 10.58
10 14 -9 24.66 11.17
-10 14 8 63.57 16.03
10 14 -8 51.66 13.34
-10 14 8 45.17 13.08
10 14 -8 60.21 14.27
10 14 -8 35.45 10.57
10 14 -8 46.95 12.79
10 14 -8 79.41 19
-10 14 8 55.49 15.3
-10 14 7 12.83 8.95
10 14 -7 12.36 8.12
-10 14 7 12.46 8.65
10 14 -7 -7.52 8.68
10 14 -7 0.75 6.01
10 14 -7 -0.85 7.11
10 14 -7 -3.72 7.89
-10 14 7 0.61 8.23
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10 14 -6 10.53 7.08
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10 14 -6 0.11 5.39
10 14 -6 9.83 6.94
10 14 -6 2.11 6.34
10 14 -6 6.52 7.19
-10 14 6 1.16 7.19
10 14 -5 17.56 6.57
-10 14 5 46.05 12.45
10 14 -5 24.68 12.21
-10 14 5 22.07 10.4
10 14 -5 31.99 10.63
10 14 -5 17.92 9.91
-10 14 5 40.65 13.36
-10 14 4 18.98 9.54
-10 14 4 3.34 6.77
10 14 -4 1.74 7.36
-10 14 4 9.91 7.7
10 14 -4 5.64 6.76
10 14 -4 4.59 8.31
-10 14 4 1.51 6.35
-10 14 3 71.94 16.02
-10 14 3 70.39 15.54
-10 14 3 79.08 14.56
10 14 -3 77.93 15.62
10 14 -3 63.35 15.73
-10 14 3 57.04 15.03
10 14 -3 55.87 14.65
-10 14 2 7.05 6.12
10 14 -2 3.5 4.75
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-10 14 2 4.54 5.74
10 14 -2 1.06 6.55
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10 14 -2 -2.29 6.06
10 14 -2 -7.68 7.62
-10 14 1 20.31 8.87
10 14 -1 3.47 4.61
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10 14 -1 -4.78 6.97
10 14 -1 7.69 6.18
-10 14 1 8.92 6.77
10 14 -1 10.04 7.7
-10 14 0 0.09 5.29
10 14 0 -5.5 8.01
-10 14 0 0.15 7.2
10 14 0 -5.7 7.9
10 14 0 9.53 9.94
-10 14 0 1.55 5.55
10 14 0 8.66 7.22
-10 14 0 0.24 7.05
10 14 1 14.79 9.32
10 14 1 5.1 5.39
-10 14 -1 25.63 12.84
10 14 1 2.77 7.47
-10 14 -1 9.34 9.41
10 14 1 -3 8.46
10 14 2 12.81 9.52
-10 14 -2 1.73 8
10 14 2 -0.31 5.34
-10 14 -2 -0.95 7.48
-10 14 -2 4.33 5.98
10 14 2 0.86 7.69
10 14 3 27.7 10.68
-10 14 -3 10.23 7.37
10 14 3 33.37 11.59
10 14 3 11.34 7.01
10 14 3 50.33 13.11
-10 14 -3 19.81 10.95
10 14 4 -0.81 7.7
-10 14 -4 -1.79 6.96
10 14 4 2.34 5.46
10 14 4 0.88 6.93
10 14 4 -5.69 6.53
-10 14 -4 7.24 8.94
-10 14 -5 87.96 18.4
10 14 5 81.09 18.49
10 14 5 57.69 15.47
-10 14 -5 64.99 15.78
10 14 5 65.09 16.17
10 14 5 96.61 17.14
-10 14 -5 88.72 18.56
-10 14 -6 2.65 7.02
10 14 6 1.26 7.81
10 14 6 -4.63 7.71
-10 14 -6 -4.57 9.44
10 14 6 10.34 10.87
10 14 6 10.94 9.32
-10 14 -6 19.21 9.59
-10 14 -7 47.62 12.52
10 14 7 64.35 17.95
10 14 7 57.16 16.35
-10 14 -7 54.12 14.8
10 14 7 68.79 17.67
10 14 7 46.19 12.79
-10 14 -7 64.03 15.84
-10 14 -8 -1.98 8.1
10 14 8 -1.11 10.61
10 14 8 11.66 9.8
-10 14 -8 -10.73 10.01
10 14 8 8.31 10.34
10 14 8 20.16 10.6
-10 14 -8 2.44 6.73
-10 14 -9 64 17.34
10 14 9 55.21 17.68
10 14 9 66.16 17.56
-10 14 -9 52.55 11.33
10 14 9 61.74 16.19
10 14 9 68.16 14.99
-10 14 -9 50.9 15.37
-10 14 -10 -7.23 10.14
10 14 10 6.57 9.86
10 14 10 -2.95 9.73
-10 14 -10 7.05 7.79
10 14 10 -2.96 7.74
-10 14 -10 14.22 9.31
10 14 10 7.35 6.54
-10 14 -11 12.63 8.77
10 14 11 37.49 16.64
10 14 11 34.17 13.53
10 14 11 29.9 12.9
10 14 11 24.84 11.37
10 14 12 -3.05 7.15
10 14 12 7.14 11.7
-10 14 -12 7.91 10.88
10 14 12 -4.85 9.39
10 14 13 36 16.67
10 14 13 39.96 16.64
-10 14 -13 37.44 13.85
10 14 14 10.18 13.28
-10 14 -14 28.18 13.55
10 15 -17 156.01 23.77
-10 15 17 124.47 22.41
-10 15 16 17.88 11.49
10 15 -16 17.25 13.26
10 15 -16 15.5 12.05
10 15 -16 13.15 11.16
-10 15 16 -16.07 10.79
-10 15 15 119.72 24.76
-10 15 15 97.52 19.33
10 15 -15 132.93 23.28
-10 15 15 105.61 18.63
10 15 -15 112.03 20.7
-10 15 15 117.2 19.46
10 15 -15 109.94 20.47
-10 15 14 27.89 13.7
-10 15 14 15.35 10.03
10 15 -14 3.4 7.84
-10 15 14 34.48 11.75
10 15 -14 30.23 13.16
-10 15 14 35.65 12.43
10 15 -14 31.9 12.24
-10 15 13 170.14 28.46
-10 15 13 138.02 21.93
10 15 -13 176.84 25.89
-10 15 13 163.09 22.76
10 15 -13 116.13 19.96
10 15 -13 169.66 24.42
-10 15 13 127.99 20.66
10 15 -12 46.63 14.47
-10 15 12 54.21 14.08
-10 15 12 41.59 17.78
10 15 -12 36.77 14.1
10 15 -12 21.22 10.98
-10 15 12 45.79 13.84
10 15 -12 32 12.88
-10 15 12 42.16 12.51
10 15 -12 54.28 15.45
10 15 -11 249.44 30.21
10 15 -11 211.39 31.31
-10 15 11 269.19 29.65
-10 15 11 198.41 29.16
10 15 -11 253 31.96
10 15 -11 231.29 29.32
-10 15 11 158.22 22.96
10 15 -11 189.45 26.87
10 15 -11 196.08 23.52
-10 15 11 209.62 25.89
10 15 -11 260.03 29.55
10 15 -10 26.93 11.53
-10 15 10 46.49 12.75
-10 15 10 66.57 18.49
10 15 -10 32.98 12.36
10 15 -10 53.47 13.85
-10 15 10 49.77 14.34
10 15 -10 41.83 11.66
10 15 -10 70.02 16.84
10 15 -10 54.53 13.9
-10 15 9 415 37.58
-10 15 9 325.08 36.96
10 15 -9 337.57 34.67
10 15 -9 287.83 32.45
10 15 -9 327.61 30.43
10 15 -9 466.37 44.23
10 15 -9 382.93 35.93
-10 15 9 382.35 35.67
10 15 -9 344.96 33.76
-10 15 8 43.09 14.12
10 15 -8 44.44 12.44
-10 15 8 47 13.86
10 15 -8 51.44 13.8
10 15 -8 36.94 12.35
10 15 -8 30.4 12.9
10 15 -8 30.57 12.35
-10 15 8 57.58 14.3
-10 15 7 446 42.48
10 15 -7 462.68 38.37
-10 15 7 429.7 38.51
10 15 -7 507.52 38.79
10 15 -7 440.13 36.06
10 15 -7 410.64 37.52
-10 15 7 438.49 39.36
10 15 -7 522.7 45.78
10 15 -6 76.16 15.78
-10 15 6 96.54 18.79
10 15 -6 66.72 17.9
-10 15 6 73.05 16.72
10 15 -6 62.92 14.06
10 15 -6 70.94 17.1
-10 15 6 77.9 18.74
10 15 -5 308.28 29.61
-10 15 5 299.87 32.07
10 15 -5 295.07 33.39
-10 15 5 288.19 31.97
10 15 -5 266.87 29.19
10 15 -5 257.79 30.11
-10 15 5 263.75 31.78
-10 15 4 129.32 21.55
10 15 -4 107.16 19.36
10 15 -4 129.92 20.65
10 15 -4 163.45 24.64
-10 15 4 126.88 21.7
-10 15 4 156.43 22.35
-10 15 3 373.41 33.93
-10 15 3 318.98 33.35
-10 15 3 316.34 30.15
10 15 -3 354.52 34.05
10 15 -3 349.81 35.57
-10 15 3 318.25 33.46
10 15 -3 345.57 35.44
-10 15 2 25.37 11.35
10 15 -2 38.25 11.23
-10 15 2 55.97 14.7
-10 15 2 56.36 13.94
10 15 -2 39.21 12.82
10 15 -2 65.18 17.7
-10 15 2 53.83 14.52
10 15 -2 56.66 15.51
-10 15 1 481.32 37.48
-10 15 1 440.95 39.81
10 15 -1 447.96 35.37
-10 15 1 415.82 35.08
10 15 -1 400.15 37.51
10 15 -1 435.32 39.23
-10 15 1 422.7 38.8
10 15 -1 382.76 37.59
-10 15 0 79.89 15.91
10 15 0 70.1 14.79
-10 15 0 96.53 19.05
10 15 0 57.64 15.4
10 15 0 90.04 18.98
-10 15 0 86.1 16.75
10 15 0 65.45 15.66
-10 15 0 98.09 20.39
-10 15 -1 235.45 29.63
10 15 1 242.82 27.51
10 15 1 197.12 27.88
10 15 1 226.19 28.48
-10 15 -1 262.63 28.21
10 15 1 215.47 26.62
-10 15 -1 270.41 30.87
10 15 2 44.74 13.91
10 15 2 26.34 9.78
-10 15 -2 30.53 13.01
10 15 2 65.95 16.38
-10 15 -2 47.41 12.87
10 15 2 35.71 12.67
10 15 3 175.63 27.25
10 15 3 156.62 23.08
-10 15 -3 168.13 24.92
-10 15 -3 172.89 24.04
10 15 3 178.55 24.4
-10 15 -3 191.31 27.52
10 15 4 89.32 19.02
-10 15 -4 57.34 15.48
10 15 4 81.55 17.14
10 15 4 121.89 20.08
-10 15 -4 67.94 18.02
10 15 4 61.17 15.13
10 15 5 176.79 27.41
-10 15 -5 194.32 27.03
10 15 5 156.73 24.02
-10 15 -5 194.63 27.01
10 15 5 214.68 25.85
10 15 5 256.75 30.44
10 15 6 25.32 12.08
-10 15 -6 24.56 10.41
10 15 6 50.94 16.82
10 15 6 34.92 11.75
-10 15 -6 15.81 8.43
10 15 6 36.44 13.04
-10 15 -6 58.86 16.51
10 15 7 203.94 28.37
-10 15 -7 177.06 27.4
10 15 7 191.98 30.66
10 15 7 174.64 26.38
-10 15 -7 212.54 28.36
10 15 7 262.33 28.78
-10 15 -7 195.77 27.38
10 15 8 43.92 14.67
-10 15 -8 46.1 15.53
10 15 8 32.34 16.24
10 15 8 20.72 11.2
-10 15 -8 40.01 13.1
10 15 8 33.25 11.12
-10 15 -8 27.92 12.17
10 15 9 280.19 34.4
-10 15 -9 263.38 34.06
10 15 9 231.32 33.29
10 15 9 313.15 37.15
-10 15 -9 244.17 29.28
-10 15 -9 299.6 32.16
10 15 10 2.92 7.83
-10 15 -10 -1.13 9.09
10 15 10 21.72 13.35
10 15 10 7.11 8.56
-10 15 -10 17.19 11.99
-10 15 -10 12.87 10.36
-10 15 -11 217.23 32.14
10 15 11 224.59 33.89
10 15 11 195.2 31.55
10 15 11 263.85 33.85
-10 15 -12 -0.6 9.33
10 15 12 3.52 8.68
10 15 12 -1.08 9.19
10 15 12 3.3 11.02
-10 16 16 -18.49 11.53
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10 16 -15 22.92 11.01
-10 16 15 5.47 9.09
10 16 -15 6.27 9.47
10 16 -15 34.46 12.62
-10 16 15 0.28 8.54
-10 16 14 18.63 11.75
-10 16 14 58.59 15.58
10 16 -14 46.48 14.74
-10 16 14 37.47 13.47
10 16 -14 46.08 15.38
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10 16 -14 52.47 15.96
-10 16 13 -2.91 8.62
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10 16 -13 0.92 7.78
-10 16 13 -2.75 7.85
10 16 -13 10.45 8.75
-10 16 13 -4.61 8.71
10 16 -13 -0.48 8.05
10 16 -12 52.79 15.07
10 16 -12 90.85 19.94
-10 16 12 86.96 17.9
10 16 -12 68.64 17.32
-10 16 12 62.72 15.18
-10 16 12 75.49 19.03
-10 16 11 0.25 6.32
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10 16 -11 -5.78 9.48
10 16 -11 1.23 7.77
-10 16 11 1.19 7.88
10 16 -11 -9.22 9.93
10 16 -11 28.21 11.27
10 16 -11 -12.84 12.25
10 16 -11 12.44 10.12
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-10 16 10 65.51 18.53
10 16 -10 70.92 17.77
10 16 -10 61.17 16.62
-10 16 10 72.3 18.29
10 16 -10 79.44 16.42
10 16 -10 90.83 18.96
10 16 -10 67.8 16.96
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10 16 -9 15.46 9.35
10 16 -9 -6.87 9.82
10 16 -9 3.14 5.82
10 16 -9 8.44 9.84
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10 16 -9 8.26 9.75
10 16 -8 50.89 14.59
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10 16 -8 39.03 11.65
10 16 -8 32.08 12.03
-10 16 8 51.04 14.22
10 16 -8 19.32 10.76
10 16 -7 19.77 10
-10 16 7 17.95 9.88
-10 16 7 22.9 12.25
10 16 -7 7.35 7.01
10 16 -7 14.87 10.15
-10 16 7 29.13 11.77
10 16 -7 41.83 13.94
10 16 -6 44.3 14.24
-10 16 6 48.94 15.62
-10 16 6 60.84 16.56
10 16 -6 51.92 15.01
10 16 -6 54.54 16.65
-10 16 6 22.56 10.57
10 16 -6 28.46 11.17
10 16 -5 13.22 8.59
10 16 -5 7.37 9.02
10 16 -5 15.61 10.59
-10 16 5 21.39 9.71
-10 16 5 33.14 13.28
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10 16 -4 0.51 7.06
10 16 -4 13 9.65
-10 16 4 6.58 8.55
10 16 -4 7.8 10.23
-10 16 3 8.55 9.78
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10 16 -3 -6.23 9.3
10 16 -3 -2.15 8.67
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10 16 -3 22.84 13.74
10 16 -2 -1.68 8.77
10 16 -2 27.25 13.05
-10 16 2 -8.6 8.37
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10 16 -2 3.2 9.55
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-10 16 2 16.75 7.55
10 16 -1 22.46 12.39
10 16 -1 18.4 10.38
10 16 -1 8.79 7.79
-10 16 1 20.93 11.2
-10 16 1 18.63 9.84
10 16 -1 25.07 11.52
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10 16 0 8.68 8.33
10 16 0 -13.3 11.63
10 16 0 -1.11 5.6
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10 16 0 16.58 11.38
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-10 16 0 9.62 7
-10 16 -1 45.89 12.49
10 16 1 54.57 13.47
-10 16 -1 91.56 18.99
10 16 1 44.5 13.57
-10 16 -1 55.14 15.73
10 16 1 85.68 20.3
10 16 1 62.87 16.8
10 16 2 33.46 12.55
-10 16 -2 9.95 9.04
10 16 2 26.73 9.87
-10 16 -2 15.59 10.12
10 16 2 15.75 12.77
10 16 2 18.06 9.94
10 16 3 15.27 9.26
-10 16 -3 22.44 10.28
10 16 3 13.22 7.97
-10 16 -3 19.73 11.73
10 16 3 30.19 12.97
-10 16 -3 15.7 8.42
10 16 3 21.93 10.47
10 16 4 4.8 6.62
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10 16 4 0.66 6.53
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-10 16 -4 21.73 11.51
10 16 4 -3.15 8.11
-10 16 -5 6.01 7.2
10 16 5 2.55 8.6
10 16 5 12.19 12.14
10 16 5 12.8 9.13
-10 16 -5 -8.15 9.71
10 16 5 14.86 7.9
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10 16 6 12.9 11.01
10 16 6 -5.11 11.84
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10 16 6 -8.64 8.18
10 16 7 -12.99 9.78
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10 16 7 0.27 8.35
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10 16 7 2.96 9.88
10 16 8 15.46 12.41
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10 16 8 5.81 9.48
-10 16 -8 5.97 10.14
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10 16 8 3.83 9.36
10 16 9 13.88 9.49
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10 16 9 10.26 13.27
-10 16 -9 -2.98 7.72
-10 16 -9 5.13 8.36
10 16 9 -1.79 9.66
10 16 10 -11.75 12.34
10 16 10 0.15 7.97
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10 16 10 -10.98 11.95
10 16 11 4.33 9.02
-10 16 -11 3.05 8.16
10 16 11 7.31 8.38
-10 17 15 171.99 26.19
-10 17 14 5.38 8.07
-10 17 14 4.41 9.15
10 17 -13 190.32 27.03
10 17 -13 201.17 28.61
-10 17 13 224.3 28.18
10 17 -13 212.16 29.4
-10 17 13 189.46 25.94
-10 17 13 166.68 30.08
10 17 -12 -17.46 12.2
10 17 -12 -12.11 10.99
-10 17 12 1.64 7.26
-10 17 12 -8.29 9.64
-10 17 12 15.26 9.92
10 17 -11 221.46 28.27
10 17 -11 181.2 26.86
10 17 -11 142.56 21.38
-10 17 11 173.63 24.98
10 17 -11 135.89 23.91
-10 17 11 167.22 24.74
-10 17 11 205.32 32.06
10 17 -10 37.49 14.64
10 17 -10 39.18 12.51
-10 17 10 34.4 12.74
10 17 -10 30.07 14.59
-10 17 10 42.24 12.29
-10 17 10 10.84 7.26
10 17 -9 108.5 20.66
10 17 -9 175.54 24.1
-10 17 9 107.39 20.37
10 17 -9 95.69 20.76
-10 17 9 122.29 21.3
-10 17 9 138.87 26.55
10 17 -8 36.79 13.44
-10 17 8 39.78 14.01
-10 17 8 44.9 16.06
10 17 -8 33.39 10.75
-10 17 8 17.5 10
10 17 -8 32.24 12.02
10 17 -7 239.72 28.82
-10 17 7 242.86 30.33
-10 17 7 230.21 32.61
10 17 -7 265.8 29.69
-10 17 7 249.86 30.94
10 17 -7 229.04 29.81
-10 17 6 8.9 9.07
-10 17 6 26.49 14.49
-10 17 6 7.92 8.39
10 17 -6 8.07 9.15
10 17 -5 399.72 37.42
10 17 -5 381.17 39.23
-10 17 5 380.38 38.06
-10 17 5 434.29 40.49
-10 17 4 3.58 8.14
-10 17 4 11.58 6.58
10 17 -4 40.02 12.82
-10 17 4 29.63 12.42
10 17 -4 45.35 16.57
-10 17 3 296.5 33.8
-10 17 3 301.61 32.1
10 17 -3 225.21 28.85
-10 17 3 276.5 31.92
10 17 -3 203.74 29.7
10 17 -2 5.18 8.07
10 17 -2 16.19 7.43
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10 17 -1 225.77 30.41
10 17 -1 167.03 25.85
-10 17 1 147.23 24.58
-10 17 1 222.64 27.5
-10 17 1 240.88 31.06
-10 17 1 199.76 26.14
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10 17 0 40.88 14.21
10 17 0 28.45 9.92
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10 17 0 27.74 14.34
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10 17 1 261.35 30.05
-10 17 -1 260.47 32.59
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10 17 1 339.72 38.31
10 17 1 231.03 30.57
10 17 2 -5.12 9.56
-10 17 -2 5.52 11.73
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10 17 2 12.4 10.76
10 17 2 7.49 8.53
10 17 3 247.08 30.88
-10 17 -3 252.67 32.62
-10 17 -3 285.62 34.29
10 17 3 294.42 37.04
10 17 3 262.83 34.03
10 17 4 3.57 8.07
-10 17 -4 8.47 10.2
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10 17 4 1.18 9.68
10 17 4 -2.91 7.62
10 17 5 193.1 26.96
-10 17 -5 191.89 28.62
-10 17 -5 200.4 29.08
10 17 5 146.62 27.88
10 17 5 216.61 32.15
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10 17 6 7.93 9.07
-10 17 -6 10.81 10.77
10 17 6 11.13 11.23
-10 17 -7 153.73 25.5
10 17 7 148.31 27.27
10 17 7 163.12 27.23
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10 17 7 171.15 26.16
-10 17 -8 11.77 11.05
10 17 8 6.48 8.91
10 17 8 1.5 8.63
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10 17 8 -13.48 11.96
-10 17 -9 115.92 24.7
-10 17 -9 125.71 23.6
10 17 9 136.56 25.07
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10 17 9 165.67 27.18
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10 17 10 0.56 8.85
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-10 18 11 -7.42 10
10 18 -10 17.99 11.63
10 18 -10 2.17 7.28
-10 18 10 48.23 14.98
10 18 -10 34.97 15.29
-10 18 10 16.04 11.41
-10 18 10 21.84 14.63
10 18 -9 25.03 13.45
10 18 -9 4.35 8.04
-10 18 9 8.39 8.92
10 18 -9 -21.36 13.73
-10 18 9 -4.38 7.76
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10 18 -8 23.09 11.41
10 18 -8 27.36 11.75
-10 18 8 26.35 12.4
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10 18 -7 -0.27 7.79
10 18 -7 -16.23 11.27
-10 18 7 -2.62 8.52
-10 18 7 -5.73 10.41
10 18 -6 -6.45 9.1
10 18 -6 13.29 10.34
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10 18 -5 -5.35 10.25
10 18 -5 -3.25 8.13
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-10 18 5 0.48 8.33
10 18 -4 34.35 14.76
10 18 -4 40.49 13.88
-10 18 4 7.85 8.63
10 18 -3 35.77 13.21
10 18 -3 48.47 15.99
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-10 18 2 0.21 9.35
10 18 -2 17.49 11.23
10 18 -2 18.7 8.98
-10 18 2 33.38 14.57
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10 18 -1 25.78 13.83
10 18 -1 -7.54 12.14
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10 18 0 3.85 6.38
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10 18 0 -0.08 8.01
10 18 0 22.87 12.13
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10 18 1 18.03 11.65
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10 18 1 0.47 8.84
10 18 1 1.94 8.69
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10 18 2 8.06 10.01
10 18 2 18.63 12.07
10 18 2 8.64 8.84
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10 18 3 -4.08 11.11
10 18 3 -9.21 8.29
10 18 3 8.78 8.52
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10 18 4 -12.84 11.64
10 18 4 4.52 10.33
10 18 4 2.59 7.95
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10 18 5 -6.55 8.43
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10 18 6 4.26 11.51
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10 18 7 7.7 8.06
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10 19 -9 180.81 26.07
10 19 -8 90.21 19.49
10 19 -7 172.99 25.97
10 19 -6 110.67 21.32
10 19 -5 165.9 27.46
10 19 -5 132.32 24.4
10 19 -4 115.91 22.53
10 19 -4 90.92 20.36
-10 19 4 126.95 23.75
-10 19 4 82.63 18.28
10 19 -3 236.43 30.35
10 19 -3 134.75 24.8
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-10 19 3 172.42 27.04
10 19 -2 64.96 17.63
10 19 -2 75.17 19.67
-10 19 2 80.58 19.64
-10 19 2 96.17 20.92
10 19 -1 191.9 28.57
10 19 -1 152.91 26.28
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-10 19 1 216.01 30.59
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10 19 0 65.82 18.95
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10 19 0 70.26 17.41
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10 19 1 144.2 25.71
10 19 1 151.89 23.92
10 19 2 91.38 19.34
10 19 3 171.58 26.79
10 19 4 23.37 13.15
11 -18 -7 192.66 30.61
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11 -18 -6 54.21 17.99
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-11 -18 5 231.84 32.51
11 -18 -5 278.61 36.25
11 -18 -5 215.25 32.25
11 -18 -5 210.99 28.56
-11 -18 5 267.95 37.35
11 -18 -4 66.78 18.67
11 -18 -4 86.09 20.46
11 -18 -4 36.67 14.11
-11 -18 4 84.78 23.34
11 -18 -3 267.96 34.17
11 -18 -3 288.03 37.92
11 -18 -3 178.99 26.34
-11 -18 3 258.24 37.19
11 -18 -2 77.4 19.64
11 -18 -2 111.38 23.55
11 -18 -2 83.85 19.09
-11 -18 2 85.41 24.36
11 -18 -1 184.66 28.45
11 -18 -1 274.46 35.65
11 -18 -1 172.35 26.08
-11 -18 1 187.9 30.65
11 -18 0 74.14 19.27
11 -18 0 55.54 19.09
11 -18 0 51.06 15.75
-11 -18 0 66.94 22.24
11 -18 1 201.41 29.5
11 -18 1 186.98 27.33
11 -18 1 186.69 29.69
11 -18 2 111.41 22.92
11 -18 3 175.82 28
-11 -17 12 23.09 12.12
-11 -17 11 16.31 13.2
11 -17 -11 -1.58 10.02
11 -17 -11 6.89 8.03
-11 -17 10 28.93 15.11
11 -17 -10 16.92 13.23
11 -17 -10 6.89 10.36
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11 -17 -9 18.38 11.68
11 -17 -9 7 9.57
-11 -17 9 -13.58 11.86
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11 -17 -8 37.55 15.32
11 -17 -8 15.68 10.72
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11 -17 -7 -16.84 13.35
11 -17 -7 1.61 10.17
-11 -17 7 -0.3 7.41
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11 -17 -6 4.54 7.82
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11 -17 -6 16.04 11.92
11 -17 -6 21.63 11.05
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11 -17 -5 -6.7 10.59
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11 -17 -5 7.3 9.75
11 -17 -5 1.63 9.21
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11 -17 -4 16.49 11.92
11 -17 -4 35.68 15.86
11 -17 -4 11.97 6.36
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11 -17 -3 6.27 8.71
11 -17 -3 1.53 11.53
11 -17 -3 -0.67 7.97
-11 -17 3 -0.19 10.1
11 -17 -2 -3.44 8.17
11 -17 -2 9.9 9.25
11 -17 -2 26.65 11.81
-11 -17 2 -7.62 9.75
11 -17 -1 -5.71 10.29
11 -17 -1 25.79 14.1
11 -17 -1 11.84 6.33
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11 -17 0 15.69 9.81
11 -17 0 4.21 10.45
11 -17 0 6.25 8.88
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11 -17 1 4.44 8.5
11 -17 1 3.03 8.67
11 -17 1 13.01 9.94
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11 -17 2 -6.74 9.19
11 -17 2 10.19 11.56
11 -17 2 4.21 8.3
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11 -17 3 1.41 7.89
11 -17 3 18.76 10.6
11 -17 3 1.74 7.89
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11 -17 4 6.77 9.2
11 -17 4 21.48 14.84
11 -17 4 0.46 8.05
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-11 -17 -4 -10.15 13.13
11 -17 5 24.75 12.76
11 -17 5 14.71 9.73
11 -17 5 8.31 7.44
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-11 -17 -5 -6.94 10.29
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11 -17 6 -8.92 11.89
11 -17 6 -8.75 10.38
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11 -17 7 0.02 8.73
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11 -16 -14 -22.99 13.62
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11 -16 -13 229.56 31.41
11 -16 -13 160.45 29.32
-11 -16 12 5.39 11.53
11 -16 -12 18.38 10.07
11 -16 -12 28 13.58
-11 -16 12 21.36 14.74
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11 -16 -11 257.57 34.53
11 -16 -11 207.57 29.85
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-11 -16 10 17.52 10.41
11 -16 -10 24.41 13.11
11 -16 -10 1.05 8.07
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11 -16 -9 294.77 35.7
11 -16 -9 334.91 38.02
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-11 -16 8 -4.2 7.43
11 -16 -8 11.71 12.05
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11 -16 -8 1.02 8.51
11 -16 -8 -5.86 7.15
-11 -16 7 339.81 38.35
11 -16 -7 358.04 39.15
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11 -16 -7 369.54 40.86
11 -16 -7 269.65 30.44
-11 -16 6 9.77 11.04
11 -16 -6 -2.77 9.86
-11 -16 6 5.83 9.57
11 -16 -6 7.96 8.65
11 -16 -6 7.26 6.2
-11 -16 5 516.64 46.51
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11 -16 -5 487.84 44.47
11 -16 -5 442.78 39.2
11 -16 -5 393.18 41.62
11 -16 -4 -0.39 10.02
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11 -16 -4 0.24 7.32
11 -16 -4 6.65 9.18
11 -16 -4 -2.36 7.4
-11 -16 4 17.94 14.36
-11 -16 3 376.83 41.33
11 -16 -3 333.26 36.62
11 -16 -3 420.87 38.7
11 -16 -3 391.46 41.93
11 -16 -3 392.31 37.33
-11 -16 2 0.34 11.02
11 -16 -2 17 11.13
11 -16 -2 12.71 9.97
11 -16 -2 -10.04 10.44
11 -16 -2 7.84 9.19
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11 -16 -1 379.12 39.38
11 -16 -1 349.48 36.28
11 -16 -1 314.18 36.24
11 -16 -1 415.91 37.92
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11 -16 0 15.37 11.24
11 -16 0 0.03 7.99
11 -16 0 -3.65 8.65
11 -16 0 10.56 8.74
11 -16 1 278.47 33.33
11 -16 1 299.53 35.31
11 -16 1 287.78 32.7
-11 -16 -1 247.48 34.56
11 -16 2 6.33 8.88
11 -16 2 0.48 10.68
11 -16 2 16.07 10.6
-11 -16 -2 3.38 9.15
11 -16 3 144.47 25.09
11 -16 3 218.36 30.05
11 -16 3 185.77 25.99
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11 -16 4 11.22 7.88
11 -16 4 -0.04 8.23
11 -16 4 -11.7 11.48
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11 2 -3 748.12 36.99
11 2 -3 724.07 32.44
-11 2 3 741.5 40.97
11 2 -2 678.37 40.11
-11 2 2 681.71 46.18
-11 2 2 724.03 39.35
11 2 -2 662.2 34.48
11 2 -2 659.7 34.18
-11 2 2 662.24 45.82
11 2 -1 1104.45 41.82
11 2 -1 1111.58 45.95
-11 2 1 1097.03 60.56
-11 2 1 1190.22 44.35
11 2 -1 1160.28 52.56
11 2 -1 1105.92 41.82
-11 2 1 1294.78 53.05
11 2 -1 1162.8 48.71
-11 2 1 1062.9 59.08
-11 2 1 1236.68 52.58
11 2 0 315.77 21.99
11 2 0 330.14 22.7
-11 2 0 388.94 34.1
-11 2 0 351.33 23.51
11 2 0 314.14 25.48
11 2 0 349.35 22.09
-11 2 0 363.64 26.47
11 2 0 361.58 26.47
11 2 0 336.78 24.82
-11 2 0 301.13 30.32
-11 2 0 310.89 26.01
11 2 1 987.56 43
11 2 1 970.22 40.62
-11 2 -1 990.72 55.84
-11 2 -1 1039.51 45.16
11 2 1 1017.67 46.49
11 2 1 993.37 41.71
-11 2 -1 1029.32 45.89
11 2 1 950.6 46.52
11 2 1 1052.7 45.32
-11 2 -1 909.74 53.37
-11 2 -1 967.39 48.07
11 2 2 352.42 25.45
11 2 2 381.59 23.64
-11 2 -2 406.75 28.44
11 2 2 354.14 25.48
11 2 2 322.6 23.05
-11 2 -2 382.99 26.61
-11 2 -2 369.14 32.82
11 2 2 347.66 27.4
-11 2 -2 347.43 28.33
11 2 2 365.71 25.27
-11 2 -2 267.67 27.95
11 2 3 594.49 35.14
11 2 3 597.92 33.38
-11 2 -3 597.63 42.18
11 2 3 581.22 37.31
11 2 3 645.13 30.5
11 2 3 616.95 33.32
-11 2 -3 632.16 38.24
-11 2 -3 632.88 39.28
11 2 3 656.36 34.01
-11 2 -3 524.6 39.28
11 2 4 145.81 18.1
11 2 4 146.46 15.44
-11 2 -4 132.91 18.47
11 2 4 178.54 18.76
-11 2 -4 133.89 20.99
11 2 4 148.72 19.91
-11 2 -4 132.05 19.65
-11 2 -4 161.68 21.61
11 2 4 181.86 17.18
11 2 5 464.18 32.71
11 2 5 472.07 27.1
-11 2 -5 395.7 32.66
11 2 5 392.98 29.1
11 2 5 472.66 32.68
-11 2 -5 380.24 33.11
11 2 5 414.32 32.79
-11 2 -5 471.74 35.08
11 2 5 472.61 27.84
-11 2 -5 440.71 35
11 2 6 130.65 14.6
-11 2 -6 121.72 18.23
-11 2 -6 93 16.43
11 2 6 112.11 16.01
11 2 6 125.89 17.42
-11 2 -6 125.74 19.4
11 2 6 115.26 17.68
-11 2 -6 177.15 22.1
11 2 6 118.49 17.18
11 2 7 443.41 34.63
-11 2 -7 400.89 36.56
11 2 7 405.17 31.79
11 2 7 444.1 32.44
-11 2 -7 428.92 34.4
11 2 7 477.9 36.57
-11 2 -7 453.73 35.9
11 2 7 420.47 26.09
-11 2 -7 429.4 33.82
11 2 8 29.63 8.52
-11 2 -8 33.72 11.52
11 2 8 43.5 10.41
11 2 8 44.46 11.6
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11 2 8 17.57 7.03
-11 2 -8 46.47 12.6
11 2 8 27.7 9.5
11 2 9 535.43 40.5
-11 2 -9 527.72 45.71
11 2 9 551.82 40.2
11 2 9 501.33 35.7
-11 2 -9 485.09 36.46
11 2 9 573.01 41.94
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11 2 9 513.42 28.99
-11 2 -10 40.07 16.25
11 2 10 37.78 11.49
11 2 10 37.84 11.72
11 2 10 38.14 11.63
-11 2 -10 53.36 12.88
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11 2 10 56.2 14
11 2 11 529.54 41.93
11 2 11 518.35 41.53
11 2 11 508.73 36.87
-11 2 -11 508.58 48.49
11 2 11 547.43 42.95
-11 2 -11 507.97 36.74
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11 2 12 37.17 12.3
-11 2 -12 40.83 14.31
11 2 12 17.76 9.45
-11 2 -12 31.79 12.76
11 2 12 32.54 12.6
11 2 12 40.3 12.86
11 2 13 283.56 32.72
-11 2 -13 288.25 37.08
-11 2 -13 225.03 30.4
11 2 13 280.04 32.83
11 2 13 271.19 28.26
11 2 14 106.81 22.36
-11 2 -14 110.5 24.32
-11 2 -14 98.89 21.57
11 2 14 91.01 18.85
11 2 14 72.38 15.74
11 2 15 310.71 34.22
11 2 15 275.02 29.5
-11 2 -15 292.56 37.96
-11 2 -15 310.5 37.29
11 2 15 360.25 38.59
11 2 16 44.72 14.32
-11 2 -16 32.6 15.31
11 2 16 51.1 13.57
11 2 16 60.22 15.14
11 2 16 76.41 19.99
-11 2 -16 26.85 13.81
11 2 17 194.21 27.16
11 2 17 223.85 27.36
-11 2 -17 236.33 34.71
-11 2 -17 236.54 35.91
11 2 18 27.46 11.28
11 2 18 24.53 11.58
-11 2 -18 34.94 17.03
-11 2 -18 49.12 19.91
11 2 19 105.45 20.12
11 2 19 166.99 25.49
-11 2 -19 135.38 26.56
-11 2 -19 66.97 19.99
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11 3 -24 24.33 11.68
11 3 -24 4.91 6.77
11 3 -24 -3.85 10.06
-11 3 24 0.55 6.45
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11 3 -23 5.16 10.11
11 3 -23 19.89 10.91
11 3 -23 3.29 8.05
-11 3 23 -2.45 6.44
-11 3 23 -6.99 10.18
11 3 -22 16.67 11.42
11 3 -22 22.88 9.84
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11 3 -22 -3.59 10.35
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11 3 -21 -8.46 9.22
-11 3 21 15.05 11.77
-11 3 21 16.74 9.21
11 3 -21 5.67 7.33
11 3 -21 12.47 10.27
11 3 -20 6.34 7.2
-11 3 20 9.48 10.17
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11 3 -20 -2.02 8.47
11 3 -20 16.93 10.71
11 3 -19 37.21 13.08
-11 3 19 35.09 14.32
-11 3 19 28.67 10.44
11 3 -19 42.59 13.03
11 3 -19 15.13 9.79
11 3 -18 5.95 6.91
-11 3 18 17.42 8.79
-11 3 18 15.56 7.91
11 3 -18 17.24 10.83
11 3 -18 28.92 12.18
11 3 -17 33.49 12.3
-11 3 17 17.24 11.18
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11 3 -17 7.27 7.94
11 3 -17 1.68 7.27
-11 3 16 19.1 8.25
11 3 -16 2.26 6.86
-11 3 16 20.94 10.3
-11 3 16 5.42 6.51
11 3 -16 13.58 8.99
11 3 -16 -3.28 9.17
-11 3 15 42.18 11.11
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11 3 -15 59.82 14.08
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11 3 -15 47.86 14.19
11 3 -15 44.35 12.58
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11 3 -14 12.88 8.06
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-11 3 14 38.72 10.72
11 3 -14 34.39 10.98
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11 3 -13 41.03 10.5
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11 3 -13 37.84 10.78
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11 3 -12 17.9 7.92
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11 3 -12 30.99 9.8
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11 3 -11 -0.65 5
-11 3 11 -9.74 8.38
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11 3 -11 -9.54 7.31
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11 3 -10 28.67 7.62
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11 3 -10 26.57 9.39
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11 3 -9 31.13 9.19
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11 3 -8 -0.54 4.66
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11 3 -8 -7.17 4.96
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11 3 -8 2.6 3.54
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11 3 -7 -2.99 4.2
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11 3 -7 0.72 4.67
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11 3 -6 -4.73 4.32
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11 3 -6 2.72 6.6
11 3 -6 1.49 2.9
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11 3 -5 -1.14 3.49
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11 3 -5 10.21 4.46
11 3 -5 6.37 4.18
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11 3 -4 4.75 4.69
11 3 -4 2 4.51
11 3 -4 -2.42 3.67
11 3 -4 2.81 3.33
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11 3 -3 -1.05 5.21
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11 3 -2 28.59 6.48
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11 3 -2 17.79 6.17
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11 3 -1 -2.13 5.24
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11 3 0 -4.05 4.51
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11 3 1 6.57 4.75
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11 3 1 4.15 2.79
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11 3 1 -0.36 4.38
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11 3 2 -1.3 3.06
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11 3 2 -4.95 6.46
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11 3 2 -0.25 3.62
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11 3 3 19.91 6.65
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11 3 3 10.53 4.31
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11 3 3 19.06 7.69
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11 3 3 9.92 5.35
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11 3 4 9.86 5.05
11 3 4 6.35 4.21
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11 3 4 8.13 5.51
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11 3 4 13.32 5.27
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11 3 4 11.81 4.53
11 3 5 0.96 4.85
11 3 5 7.59 4.43
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11 3 5 4.71 4.26
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11 3 5 4.16 6.31
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11 3 6 21.76 8.42
11 3 6 11.78 5.02
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11 3 6 8.32 3.77
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-11 3 -6 22.68 10.24
11 3 6 8.25 5.13
11 3 7 35.75 13.75
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11 3 7 5.16 4.55
11 3 7 8.29 6.89
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11 3 7 17.96 5.62
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11 3 7 4.44 5.93
11 3 8 27.49 10.53
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11 3 8 11.78 6.55
11 3 8 6.38 5.79
11 3 8 8.57 4.31
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11 3 9 -4.72 7.07
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11 3 10 -3.02 7.09
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11 3 10 -14.58 10.08
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11 3 11 18.16 10.97
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11 3 11 22.66 11.79
11 3 11 -7.01 6.87
11 3 12 -8.43 11.12
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11 3 12 1.68 7.91
11 3 12 11.59 9.43
11 3 13 23.21 11.62
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-11 3 -13 22.13 9.39
11 3 13 20.2 14.38
11 3 13 30.23 10.83
11 3 14 -17.06 12.28
11 3 14 -5.6 7.61
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11 3 14 -6.62 9.35
11 3 15 38.04 14.99
11 3 15 61.4 14.83
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11 3 15 34.92 12.8
-11 3 -15 57.44 17.66
11 3 15 74.81 19.33
11 3 16 19.01 11.62
-11 3 -16 14.2 12.81
11 3 16 3.12 10.5
11 3 16 23.73 10.55
11 3 16 15.57 11.35
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11 3 17 8.27 8.59
11 3 17 5.13 6.95
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11 3 18 -5.98 10.41
11 3 18 8.54 7.17
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11 3 19 6.63 7.92
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-11 3 -19 14.71 9.93
11 3 19 10.45 10.53
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-11 4 24 100.27 22.17
11 4 -24 79.22 17.55
11 4 -24 91.29 18.9
11 4 -24 112.19 20.75
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11 4 -23 101.73 20.35
-11 4 23 125.69 22.79
11 4 -23 129.45 23.04
-11 4 22 73.38 18.81
11 4 -22 77.28 17.46
-11 4 22 84.46 17.96
11 4 -22 108.99 20.24
11 4 -21 105.93 19.33
11 4 -21 117.12 21.02
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11 4 -21 131.84 23.31
11 4 -20 183.8 25.41
11 4 -20 157.13 23.69
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-11 4 20 163.87 23.85
11 4 -20 139.88 23.61
11 4 -19 181.54 24.98
11 4 -19 139.6 22.52
-11 4 19 106.35 20.63
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11 4 -19 171.94 26.01
11 4 -18 200.67 25.13
11 4 -18 196.19 25.72
-11 4 18 211.86 29.87
-11 4 18 218.93 26.56
11 4 -18 183.24 27.02
11 4 -17 226.43 26.36
11 4 -17 239.29 27.59
-11 4 17 168.22 26.57
11 4 -17 192.46 27.57
-11 4 17 175.12 23.3
11 4 -16 200.57 27.02
-11 4 16 206.35 24.74
11 4 -16 237.94 26.47
-11 4 16 192.75 21.93
-11 4 16 197.4 22.26
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11 4 -16 185.79 24.01
11 4 -15 301.85 32.62
-11 4 15 314.05 29.63
11 4 -15 319.7 29.96
-11 4 15 282.19 26.42
-11 4 15 328.71 28.79
-11 4 15 306.66 34.79
11 4 -15 295.33 28.82
11 4 -14 219.87 27.31
-11 4 14 243.3 25.1
11 4 -14 233.7 25.03
-11 4 14 231.22 24.18
-11 4 14 231.7 24.21
-11 4 14 248.16 30.98
11 4 -14 250.15 26.4
11 4 -13 601.68 44.43
-11 4 13 522.83 36.82
11 4 -13 608.96 39.49
-11 4 13 586.18 38.3
-11 4 13 521.31 36.94
-11 4 13 557.9 45.44
11 4 -13 571.84 39.06
-11 4 12 238.34 24.7
-11 4 12 263.48 24.63
11 4 -12 273.9 25.79
-11 4 12 256.35 26.2
-11 4 12 295.08 31.67
11 4 -12 252.49 25.1
-11 4 11 609.49 40.38
-11 4 11 659.67 38.8
11 4 -11 622.84 38.52
-11 4 11 633.41 41.62
11 4 -11 718.72 42.66
-11 4 11 664.91 46.66
11 4 -11 700.92 33.61
-11 4 10 339 30.09
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11 4 -10 356.74 27.84
-11 4 10 343.14 30.28
11 4 -10 376.81 30.05
-11 4 10 376.38 34.03
11 4 -10 323.12 22.3
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-11 4 9 566.07 33.65
11 4 -9 489.85 32.66
-11 4 9 524.06 38.17
11 4 -9 557.56 36.01
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11 4 -9 517.32 28.69
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11 4 -8 656.25 36.87
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11 4 -8 703.75 40.39
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11 4 -8 735.18 34.16
-11 4 7 664.62 43.91
-11 4 7 702.9 35.73
11 4 -7 634.76 35.55
-11 4 7 588.52 42.1
11 4 -7 648.2 37.99
-11 4 7 729.06 43.8
11 4 -7 681.74 32.62
-11 4 6 517.65 38.98
-11 4 6 603.96 32.46
11 4 -6 541.31 31.78
-11 4 6 529.11 40.01
11 4 -6 497.89 32.87
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11 4 -6 594.6 30.33
11 4 -5 544.38 28.76
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-11 4 5 599.88 31.81
11 4 -5 571.05 31.85
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11 4 -5 614.47 29.68
11 4 -5 619.14 35.68
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11 4 -5 570.83 30.23
11 4 -4 620.37 31.8
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-11 4 4 614.64 31.78
11 4 -4 617.64 32.58
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11 4 -4 652.38 36.57
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11 4 -4 632.18 32.49
11 4 -3 430.22 27.47
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-11 4 3 478.12 26.83
11 4 -3 435.89 26.47
11 4 -3 484.98 28
11 4 -3 460.97 29.98
-11 4 3 430.7 37.59
-11 4 3 458.94 30.75
-11 4 2 724.02 49.5
-11 4 2 657.82 46.71
11 4 -2 660.28 32.18
11 4 -2 639.04 35.74
11 4 -2 661.84 35.94
-11 4 2 719.71 38.12
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-11 4 1 518.18 41.08
11 4 -1 501.54 26.9
11 4 -1 488.72 31.3
-11 4 1 555.87 33.47
-11 4 1 536.92 41.87
-11 4 0 1074.51 44.22
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-11 4 0 1084.23 46.84
-11 4 0 1136.74 62
11 4 0 1036.1 49.01
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11 4 0 1014.48 43.51
-11 4 -1 558.03 33.22
-11 4 -1 475.77 39
-11 4 -1 465.57 29.06
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11 4 1 513.27 33.81
-11 4 -1 551.11 34.17
11 4 1 453.07 29.05
11 4 2 634.11 35.74
11 4 2 618.09 35.32
-11 4 -2 479.01 32.9
-11 4 -2 705.17 35.07
-11 4 -2 574.16 43.22
11 4 2 585.77 32.78
11 4 2 679.92 39.97
-11 4 -2 616.51 37.62
11 4 2 628.91 33.41
-11 4 -2 586.67 43.02
11 4 3 634.8 37.84
11 4 3 668.83 35.79
-11 4 -3 724.03 41.64
-11 4 -3 656.72 33.64
-11 4 -3 574.13 42.91
11 4 3 698.61 34.8
11 4 3 647 41.01
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11 4 3 646.58 33.48
-11 4 -3 669.2 45.46
11 4 4 650.79 39.03
11 4 4 601.56 32.48
11 4 4 561.92 32.44
-11 4 -4 600.93 39.6
11 4 4 610.31 36.95
-11 4 -4 632.33 40.06
-11 4 -4 499.76 39.19
11 4 4 581.34 30.9
11 4 4 554.22 30.41
-11 4 -4 590.25 42.08
11 4 4 569.24 39.02
11 4 5 839.56 48.99
-11 4 -5 754.05 47.87
11 4 5 841.41 42.25
11 4 5 869.85 44.96
-11 4 -5 873.58 48.7
-11 4 -5 808.43 50.11
11 4 5 972.06 40.62
-11 4 -5 875.42 51.91
11 4 5 885.53 48.26
11 4 6 171.91 22.83
-11 4 -6 192.52 24.2
11 4 6 161.33 18.75
11 4 6 169.07 19.61
-11 4 -6 210.07 24.24
-11 4 -6 223.7 26.11
11 4 6 191.13 16.63
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11 10 -11 100.46 17.4
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11 12 -19 83.01 17.53
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11 12 -18 162.89 22.77
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11 12 -16 92.99 19.59
11 12 -16 112.37 20.62
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11 12 -16 86.68 17.81
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11 12 -15 115.86 24.04
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11 12 -15 141.03 20.77
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11 12 -14 114.97 22.04
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-11 12 14 121 21.12
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11 12 -13 197.61 28.45
11 12 -13 174.24 24.62
-11 12 13 258.42 28.73
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11 12 -13 150.79 21.7
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-11 12 12 117.31 19.43
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11 12 -12 178.92 25.85
11 12 -12 129.22 21.74
-11 12 12 149.46 21.27
11 12 -12 113.85 19.31
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11 12 -12 104.19 17.55
11 12 -11 219.03 28
-11 12 11 242.12 27.63
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11 12 -11 160.2 23.81
11 12 -11 211.42 26.67
-11 12 11 181.95 24.42
11 12 -11 176.02 24.73
-11 12 11 137.39 22.5
11 12 -11 166.67 22.73
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-11 12 10 335.68 35.13
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11 12 -10 279.54 29.65
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11 12 -10 302.03 31.75
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11 12 -8 241.31 26.1
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11 12 -7 164.84 22.69
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11 12 -7 154.54 19.56
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11 12 0 403.61 35.82
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11 12 1 266.2 27.72
11 12 1 182.12 24.88
11 12 1 192.05 22.13
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11 12 1 217.06 25.37
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11 12 2 353.04 31.2
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11 12 2 378.93 35.88
11 12 2 378.84 33.07
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11 12 2 370.23 34.18
11 12 3 258.57 31.05
11 12 3 244.63 26.56
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11 12 3 291.15 29.04
-11 12 -3 257.28 31.74
11 12 3 249.29 28.74
11 12 4 288.55 33.1
11 12 4 226.63 26.36
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11 12 4 283.58 28.38
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11 12 4 248.26 29.25
11 12 5 248.94 30.95
11 12 5 277.42 30.52
-11 12 -5 246.96 30.01
11 12 5 303.17 28.89
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11 12 5 229.82 28.52
-11 12 -6 198.81 26.47
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11 12 6 216.67 27.27
11 12 6 228.97 24.87
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11 12 6 186.36 26.24
-11 12 -7 261.62 31.57
-11 12 -7 213.4 28.01
11 12 7 227 28.83
11 12 7 254.25 26.32
-11 12 -7 234.84 29.35
11 12 7 202.95 27.56
-11 12 -8 236.65 26.6
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11 12 8 225.15 29.97
-11 12 -8 232.07 28.27
11 12 8 196.97 23.17
11 12 8 230.37 29.29
-11 12 -9 202.32 24.81
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11 12 9 212.64 29.42
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11 12 9 199 27.94
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-11 12 -10 150.7 26.02
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-11 12 -10 148.9 22.52
11 12 10 157.65 26.23
11 12 11 123.46 22.92
-11 12 -11 149.09 23.07
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11 12 13 104 22.24
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11 12 14 130.67 24.6
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11 13 -6 -0.12 6.17
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11 13 -4 17.78 10.42
11 13 -3 23.69 9.84
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11 13 0 1.43 9.38
11 13 1 5.5 7.33
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11 13 1 2.55 7.49
11 13 1 6.35 9.09
11 13 1 7.27 5.15
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11 13 2 1.68 5.95
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11 13 2 0.89 6.29
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11 13 5 -2.73 8.68
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11 13 6 5.57 5.79
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11 13 6 25.77 11.35
-11 13 -6 24.29 11.44
11 13 6 11.57 7.31
11 13 6 10.11 9.23
11 13 7 25.59 11.35
-11 13 -7 23.39 12.95
-11 13 -7 45.33 15.18
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11 13 7 9.55 7.96
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11 13 8 -11.47 10.85
-11 13 -8 -0.27 6.75
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11 13 8 8.1 6.69
11 13 8 16.77 11.43
-11 13 -9 34.84 12.51
-11 13 -9 0.82 7.57
11 13 9 4.56 7.35
11 13 9 31.2 14.35
-11 13 -9 24.79 11.47
-11 13 -10 4.38 8.38
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11 13 10 6.9 8.61
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11 13 11 0.68 10.23
11 13 11 30.25 13.83
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11 13 12 0.02 9.16
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11 13 13 3.28 10.43
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11 13 13 26.58 13.9
-11 13 -14 -12.88 13.72
11 14 -18 33.52 14.15
-11 14 17 168.47 26.17
-11 14 17 184.17 31.26
11 14 -17 199.16 26.63
-11 14 16 18.16 10.32
11 14 -16 23.65 11.33
11 14 -16 22.81 11.86
11 14 -16 17.91 10.45
-11 14 16 19.69 9.67
-11 14 15 226.11 33.55
-11 14 15 180.19 26.21
11 14 -15 152.62 23.97
-11 14 15 183.95 25.19
11 14 -15 169.98 25.91
11 14 -15 193.79 26.22
-11 14 15 135.77 21.86
-11 14 14 38.82 14.83
-11 14 14 12.67 8.94
11 14 -14 28.52 11.48
-11 14 14 64.72 14.29
11 14 -14 34.24 12.43
11 14 -14 26.05 11.04
-11 14 14 55.97 14.89
-11 14 13 213.35 26.46
-11 14 13 210.43 31.28
11 14 -13 174.79 27.64
11 14 -13 198.63 27.93
-11 14 13 194.1 26.34
11 14 -13 181.86 25.44
-11 14 13 223.63 28.67
11 14 -13 220.1 27.28
11 14 -12 40.54 13.98
-11 14 12 73.93 17.05
-11 14 12 53.05 17.01
11 14 -12 58.09 16.23
11 14 -12 27.78 11.98
-11 14 12 63.43 15.44
11 14 -12 45.09 14.16
-11 14 12 30.61 11.07
11 14 -12 65.07 15.82
11 14 -11 221.44 29.44
-11 14 11 219.51 27.36
-11 14 11 249.79 33.21
11 14 -11 263.75 33.32
11 14 -11 175.08 25.48
-11 14 11 220.78 27.68
11 14 -11 200.61 26.99
-11 14 11 243.54 29.02
11 14 -11 231.96 27.54
11 14 -10 49.76 14.56
-11 14 10 59.09 14.79
-11 14 10 90.17 19.94
11 14 -10 58.22 15.09
11 14 -10 58.42 15.82
-11 14 10 72.21 16.74
11 14 -10 23.94 10.35
-11 14 10 57.66 15.12
11 14 -10 59.58 15.44
11 14 -9 296.74 35.49
-11 14 9 237.6 29.35
-11 14 9 303.41 34.7
11 14 -9 263.16 30.1
11 14 -9 258.4 29.83
-11 14 9 248.39 29.16
11 14 -9 247.58 26.03
11 14 -9 281.46 29.74
11 14 -9 269.91 30.23
11 14 -8 105.99 20.01
-11 14 8 98.48 18.88
-11 14 8 76.54 17.76
11 14 -8 72.8 15.74
11 14 -8 99.13 19.06
11 14 -8 92.39 16.2
11 14 -8 89 17.44
11 14 -8 80.47 16.7
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-11 14 7 353.05 35.19
11 14 -7 375.86 35.49
11 14 -7 358.65 31.58
-11 14 7 417.49 40.73
-11 14 7 364.24 36.19
11 14 -7 373.55 38.91
-11 14 6 70.56 16.99
11 14 -6 88.95 18.95
11 14 -6 83.13 16.18
-11 14 6 75.21 16.99
11 14 -6 80.84 17.59
-11 14 6 92.74 18.42
-11 14 5 277.15 31.38
11 14 -5 265.05 29.76
11 14 -5 285.14 29.12
-11 14 5 298.32 33.87
11 14 -5 306.39 34.3
-11 14 5 237.61 29.45
11 14 -4 143.5 21.53
-11 14 4 160.49 24.28
11 14 -4 183.86 27.55
-11 14 4 132.77 22.45
11 14 -4 157.35 23.08
11 14 -3 352.66 34.06
-11 14 3 369.81 37.03
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11 14 -3 388.77 37.31
11 14 -3 348.06 34.77
11 14 -2 215.5 26.22
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11 14 -2 288.91 32.05
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11 14 -2 274.85 31.29
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-11 14 1 348.93 35.6
11 14 -1 440.81 39.16
-11 14 1 293.79 33.51
11 14 -1 338.67 35.03
11 14 0 173.82 25.12
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11 14 0 173.04 24.99
-11 14 0 200.06 27.76
11 14 0 190.31 26.46
11 14 1 257.49 31.7
11 14 1 328.05 35.48
11 14 1 271.5 28.59
-11 14 -1 302.62 34.09
11 14 1 349.47 33.23
-11 14 -1 321.67 34.76
11 14 2 107.85 21.24
11 14 2 115.74 22.18
11 14 2 139.25 21.84
-11 14 -2 122.24 22.43
11 14 2 131.71 21.1
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11 14 3 219.61 29.93
11 14 3 204.82 25.92
-11 14 -3 247.24 31.95
11 14 3 262.34 29.61
-11 14 -3 239.04 31.45
11 14 4 80.47 19.38
11 14 4 119.35 19.99
-11 14 -4 97.92 20.92
11 14 4 100.49 19.5
11 14 4 133.54 21.22
-11 14 -4 111.47 22.04
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-11 14 -5 178.76 26.46
11 14 5 194.71 26.79
11 14 5 230.59 26.63
-11 14 -5 205.33 28.58
11 14 6 103.48 22.14
11 14 6 94.87 19.18
-11 14 -6 74.02 17.84
11 14 6 82.83 18.76
11 14 6 114.6 19.33
-11 14 -6 75.78 18.86
11 14 7 167.37 28.05
11 14 7 145.01 24.88
-11 14 -7 149.38 24.76
11 14 7 187.18 26.9
11 14 7 183.1 23.87
-11 14 -7 200.13 28.03
-11 14 -8 56.78 16.68
11 14 8 59.69 19.24
-11 14 -8 58.38 15.38
11 14 8 90.4 19.81
11 14 8 72.71 18.78
-11 14 -8 86.48 17.72
11 14 8 89.05 17.12
-11 14 -9 148.25 26.11
11 14 9 157.24 28.77
-11 14 -9 106.73 20.56
11 14 9 138 25.23
11 14 9 132.8 24.08
-11 14 -9 124.81 21.49
11 14 9 150.97 22.95
11 14 10 42.06 15.63
11 14 10 48.45 16.79
11 14 10 17.69 12.6
-11 14 -10 30.02 11.5
11 14 11 117.57 22.66
11 14 11 131.8 25.24
11 14 11 150.67 28.77
-11 14 -11 134.08 24.51
11 14 12 23.94 11.96
11 14 12 12.66 11.02
-11 14 -12 31.1 14.22
-11 15 16 28.32 13.71
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11 15 -14 20.24 10.89
-11 15 13 -3.48 8.11
-11 15 13 15.17 9
11 15 -13 0.37 8.42
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11 15 -13 18.39 10.02
-11 15 13 13.24 11.3
11 15 -13 8.95 10.06
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11 15 -11 -4.55 9.64
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11 15 -11 -6.67 9.39
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11 15 -10 52.44 15.87
11 15 -10 44.71 14.97
-11 15 10 50.37 15.17
11 15 -10 70.07 17.36
11 15 -10 40.15 12.88
11 15 -10 35.52 14.16
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11 15 -9 2.38 10.55
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11 15 -9 -6.05 10.13
11 15 -9 0.16 7.06
11 15 -8 65.29 15.39
11 15 -8 43.03 12.49
-11 15 8 60.99 16.1
11 15 -8 45.2 14.4
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11 15 -8 73.31 18.86
-11 15 8 32.42 12.47
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11 15 -7 5.98 7.68
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11 15 -6 20.64 9.67
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11 15 -6 23.04 10.56
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11 15 -5 0.79 7.07
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11 15 -3 -3.12 9.78
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11 15 -2 -7.02 8.14
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11 15 -1 -8.37 8
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11 15 -1 0.61 8.71
11 15 0 0.97 9.99
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11 15 1 3.78 8.24
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11 15 1 -7.44 8.96
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11 15 1 -4.2 9.19
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11 15 2 -0.36 8.81
11 15 2 9.38 7.78
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11 15 3 4.43 8.08
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11 15 4 0.56 9.5
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11 15 5 18.14 12.78
11 15 5 -7.87 9.1
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11 15 5 27.97 13.17
11 15 6 9.84 10.05
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11 15 6 8.48 11.51
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11 15 6 2.87 7.34
11 15 7 10.43 8.95
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11 15 7 17.94 13.58
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11 15 7 6.47 9.26
11 15 8 3.32 7.07
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11 15 8 -7.97 11.53
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11 15 8 9.7 10.5
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11 15 9 1.37 10.7
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11 15 9 7.16 8.88
11 15 10 -12.38 11.42
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11 15 10 -3.06 9.57
11 15 10 -13.2 13.89
11 15 11 0.65 8.92
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11 15 11 0.21 8.75
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11 16 -13 226.71 28.85
11 16 -13 226.76 30.01
-11 16 13 186.72 25.73
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11 16 -12 -7.45 12.79
11 16 -12 25.2 11.78
11 16 -12 11.66 9.95
-11 16 12 10.31 9.24
-11 16 12 18.01 8.81
-11 16 11 302.54 39.51
11 16 -11 200.55 29.17
11 16 -11 257.6 30.35
11 16 -11 202.06 28.63
-11 16 11 246.12 30.13
-11 16 11 250.94 29.7
-11 16 10 20.46 13.35
11 16 -10 8.05 10.23
11 16 -10 -4.36 9.59
11 16 -10 14.7 11.31
-11 16 10 8.87 6.87
-11 16 10 1.8 7.53
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11 16 -9 234.53 30.83
11 16 -9 242.98 30.05
11 16 -9 265.97 28.95
-11 16 9 268.88 31.43
-11 16 9 296.22 33.14
-11 16 8 6.64 8.99
11 16 -8 4.79 8.05
11 16 -8 2.77 6.56
-11 16 8 1.85 7.82
-11 16 8 16.27 11.26
11 16 -8 17.21 11.72
11 16 -7 334.52 34.75
11 16 -7 348.7 33.53
-11 16 7 294.59 35.82
-11 16 7 259.83 31.54
-11 16 7 304.35 33.62
11 16 -6 -5.3 8.01
11 16 -6 14.14 9.34
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11 16 -5 384.48 36.91
11 16 -5 444.11 41.11
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11 16 -4 18.78 9.22
11 16 -4 -4.59 9.24
-11 16 4 -0.63 7.71
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11 16 -3 349.14 35.57
11 16 -3 355.56 37.35
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-11 16 3 345.62 36.8
11 16 -2 -6.15 8.56
11 16 -2 -9.7 9.93
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-11 16 2 15.82 12.49
11 16 -1 326.99 35.46
11 16 -1 349.67 37.81
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11 16 1 243.51 31.33
11 16 1 272.57 33.81
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11 16 2 6.09 11.08
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11 16 2 -3.98 9.28
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11 16 3 168.98 27.15
11 16 3 170.27 28.88
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11 16 7 129.2 23.91
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12 2 -18 -2.88 8.25
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12 2 -17 6.41 6.66
12 2 -17 -7.88 10.75
12 2 -16 10.41 8.54
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12 2 -16 0.17 6.98
12 2 -16 -7.86 10.38
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12 2 -15 54.07 13.98
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12 2 -14 -5.67 8.28
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12 2 -10 4.36 5.68
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12 2 -10 10.77 7.47
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12 2 -8 7.43 5.55
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12 2 2 1.69 4.6
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12 2 7 79.11 17.46
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12 3 -23 154.05 24.13
12 3 -23 166.56 24.07
12 3 -23 142.2 23.72
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12 3 -22 71.61 17.26
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12 3 -22 101.56 21.51
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12 3 -21 171.29 25.56
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12 3 -21 187.93 26.21
12 3 -21 231.92 29.74
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12 3 -20 95.07 19.25
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12 3 -20 117.15 21.94
12 3 -20 88.25 19.81
12 3 -20 159.05 24.76
12 3 -19 235.22 28.3
12 3 -19 269.7 32.1
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12 3 -19 272.18 33.31
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12 3 -18 123.11 21.48
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12 3 -18 92.84 20.04
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12 3 -16 80.09 16.71
12 3 -16 81.48 16.49
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12 3 -15 325.47 30.82
12 3 -15 367.94 33.41
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12 3 -11 518.73 36.91
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12 3 -10 26.27 9.03
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12 3 -9 663.69 38.04
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12 3 -8 69.69 13.1
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12 4 9 6.35 6.81
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12 4 9 9.03 6.51
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12 4 10 -6.57 7.83
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12 4 11 1.03 7.1
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12 4 11 -0.63 5.81
12 4 12 11.04 8.23
12 4 12 1.74 6.49
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12 4 13 21.87 12.09
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12 4 13 10.69 7.02
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12 4 13 31.33 13.6
12 4 13 2.41 8.37
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12 4 14 28.45 14.03
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12 4 14 26.54 13.34
12 4 14 9.73 8.12
12 4 14 35.36 14.78
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12 4 14 39.57 14.08
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12 4 15 -3.57 9.58
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12 4 16 -2.38 6.72
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12 4 16 18.12 12.65
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12 4 17 10.45 11.43
12 4 17 7.06 10.11
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12 4 18 4.95 8.63
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12 5 -23 23.41 11.13
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12 5 -22 122.37 22.16
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12 5 -21 39.14 13.61
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12 5 -21 51.83 15.7
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12 5 -20 211.93 28.05
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12 5 -20 247.43 30.65
12 5 -19 46.09 14.19
12 5 -19 47.57 14.85
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12 5 -19 44.83 14
12 5 -18 239.24 28.5
12 5 -18 256.56 29.59
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12 5 -18 328.61 36.63
12 5 -17 115.96 20.23
12 5 -17 88.82 18.46
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12 5 -17 114.5 22.03
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12 5 -16 360.95 36.83
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12 5 -16 315.61 31.4
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12 5 -16 323.44 32.3
12 5 -15 70.71 18.37
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12 5 -15 69.99 15.42
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12 5 -15 69.33 15.38
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12 5 -14 277.15 28.72
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12 5 -13 118.67 18.64
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12 5 -13 122.37 19.84
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12 5 -12 336.44 29.53
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12 5 -12 327.88 30.3
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12 5 -11 257.42 25.71
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12 5 -11 272.81 27.66
12 5 -10 405.08 37.19
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12 5 -10 392.32 30.5
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12 5 -10 361.08 31.14
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12 5 -9 222.61 22.5
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12 5 -8 425.06 30.43
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12 5 -8 438.81 32.63
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12 5 -8 433.92 27.28
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12 5 -7 289.59 26.51
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12 5 -5 267.04 22.19
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12 5 -4 643.17 34.48
12 5 -3 199.27 19.22
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12 5 -3 175.01 19.75
12 5 -3 184.22 18.86
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12 5 1 243.12 22.6
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12 5 1 230.65 23.1
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12 5 2 640.39 38.17
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12 7 -17 9.73 9.3
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12 10 -7 3.9 8
12 10 -7 12.9 8.52
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12 11 -19 26.18 13.21
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12 11 -18 247.55 31.1
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12 11 -17 17.92 11.12
12 11 -17 10.48 9.54
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12 11 -16 251.06 30.76
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12 11 -16 314.59 34.14
12 11 -16 249.32 27.18
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12 11 -15 51.42 15.56
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12 11 -15 78.15 15.48
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12 11 -14 154.2 27.08
12 11 -14 140.53 22.55
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12 11 -14 194.7 26.86
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12 11 -14 166.79 21.82
12 11 -13 93.71 20.27
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12 11 -13 92.15 19.11
12 11 -13 73.6 17.05
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12 11 -13 107.26 19.95
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12 11 -12 262.77 32.35
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12 11 -12 231.94 29.22
12 11 -12 202.28 25.88
-12 11 12 213.2 26.16
12 11 -12 241.03 28.42
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12 11 -12 226.58 25.39
12 11 -11 179.3 25.9
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12 11 -11 178.18 24.83
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12 11 -11 153.65 22.99
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12 11 -10 327.58 32.58
12 11 -10 284.55 31.31
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12 11 -10 301.06 31.32
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12 11 -9 160.01 21.63
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12 11 -6 338.72 31.71
12 11 -6 414.2 32.04
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12 11 -6 350.49 32.46
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12 11 -6 460 36.06
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12 11 -5 126.81 19.83
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12 11 -4 346.83 32.19
12 11 -4 351.19 30.65
12 11 -4 409.61 37.65
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12 11 1 66.17 14.95
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12 11 11 114.84 22.12
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12 13 -16 66.25 17.11
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12 13 -14 92.57 18.07
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12 13 -8 121.63 20.88
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12 13 -7 150.02 23.18
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12 13 -6 159.74 25.74
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12 13 1 212.29 28.92
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12 13 2 247.6 31.13
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12 13 5 198.85 29.5
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12 13 6 152.76 21.61
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12 13 6 158.6 27.75
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12 13 7 120.03 21.7
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12 13 7 155.91 25.5
12 13 7 156.88 27.29
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12 13 8 108.61 21.51
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12 13 8 97.07 21.47
12 13 8 132.43 26.09
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12 13 9 76.91 20.17
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12 13 10 107.16 22.25
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12 13 11 66.89 18.12
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12 13 12 35.54 14.7
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13 2 4 103.95 14.82
-13 2 -4 88.49 15.55
13 2 4 137.79 19.6
-13 2 -4 116.58 21.29
13 2 4 137.04 20.29
-13 2 -4 119.61 20.27
13 2 4 95.77 15.55
-13 2 -5 528.92 40.51
13 2 5 544.8 38.12
13 2 5 559.4 39.65
-13 2 -5 588.77 46.14
13 2 5 543.12 40.52
-13 2 -5 627.63 45.43
13 2 5 530.09 33.44
13 2 6 171.76 18.43
-13 2 -6 156.15 22.24
13 2 6 165.46 21.9
-13 2 -6 184.75 25.99
13 2 6 160.35 22.86
-13 2 -6 144.87 22.39
13 2 6 112.42 17.63
-13 2 -7 399.72 38.13
13 2 7 356.58 32.63
13 2 7 345.57 31.38
13 2 7 329.54 25.82
-13 2 -7 354.24 35.59
-13 2 -7 341.87 34.97
13 2 7 302.95 32.44
-13 2 -8 99.04 19.8
13 2 8 97.2 17.84
-13 2 -8 80.1 18.61
13 2 8 79.7 14.97
13 2 8 89.42 18.48
-13 2 -8 74.97 17.18
13 2 8 82.79 18.38
-13 2 -9 224.55 26.96
13 2 9 245.38 27.49
13 2 9 208.33 26.86
-13 2 -9 215.42 30.58
13 2 9 261.88 29.91
-13 2 -9 233.74 29.67
13 2 9 244.16 29.89
-13 2 -10 47.58 13.89
13 2 10 58.33 16.36
-13 2 -10 42.98 16.14
13 2 10 66.87 15.67
13 2 10 51.47 13.58
-13 2 -10 31.1 12.02
13 2 10 33.84 11.55
13 2 11 202.16 28.39
-13 2 -11 184.18 29.31
13 2 11 222.26 28.97
13 2 11 228.05 29.02
-13 2 -11 228.34 30.83
13 2 11 205.38 25.86
13 2 12 30.22 13.02
-13 2 -12 21.75 9.69
13 2 12 12.11 9.92
13 2 12 37.35 13.86
-13 2 -12 3.12 8.83
13 2 12 36.72 13.47
-13 2 -13 90.25 23.78
13 2 13 95.34 22.2
-13 2 -13 89.34 20.87
13 2 13 99.47 19.56
13 2 13 79.46 17.36
-13 2 -14 25.79 15.55
13 2 14 4.49 9.98
13 2 14 37.92 13.04
-13 2 -14 17.11 12.2
-13 2 -15 151.78 31.18
13 2 15 91.79 18.56
-13 2 -16 18.48 11.71
13 2 16 31.29 11.68
13 2 16 28.92 12.42
-13 2 -16 15.33 13.05
13 3 -22 9.7 10.2
13 3 -22 11.62 12.78
-13 3 22 7.35 7.89
13 3 -22 9.57 9.16
13 3 -21 -0.69 8.51
13 3 -21 0.79 8.74
-13 3 21 -4.88 9.15
13 3 -21 3.26 7.78
13 3 -20 0.9 7.36
13 3 -20 -4.29 9.93
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13 3 -20 -7.63 9.14
13 3 -19 0.64 9.58
13 3 -19 6.34 7.4
13 3 -19 24.76 11.42
-13 3 19 8.75 10.22
13 3 -18 0.57 7.12
13 3 -18 -6.9 10.16
13 3 -18 9.14 12.28
13 3 -18 9.06 9.98
-13 3 18 -6.59 12.68
13 3 -17 -5.41 9.37
13 3 -17 8.18 7.94
13 3 -17 0.96 7.94
13 3 -17 16.34 13.37
-13 3 17 -5.61 13.42
13 3 -16 -1.76 6.82
13 3 -16 -5.1 9.24
13 3 -16 -1.38 7.89
-13 3 16 8.02 11.81
-13 3 16 4.29 7.27
13 3 -15 -2.67 7.25
13 3 -15 -4.06 9.96
13 3 -15 -2.28 8.12
-13 3 15 -8.48 8.57
-13 3 15 16.72 10.73
-13 3 14 18.82 11.4
13 3 -14 8.43 8.58
-13 3 14 17.01 9.39
13 3 -14 15.2 8.33
-13 3 13 -5.24 10.24
13 3 -13 9.61 8.78
-13 3 13 13.61 9.22
13 3 -13 0.5 6.28
13 3 -12 28.39 10.4
13 3 -12 17.82 9.27
-13 3 12 33.53 12.84
-13 3 12 12.63 7.19
-13 3 12 28.92 11.31
13 3 -11 30.05 9.31
13 3 -11 27.29 8.71
-13 3 11 38.02 14.09
-13 3 11 27.51 11.53
-13 3 11 10.99 7.48
13 3 -10 6.93 6.75
13 3 -10 15.42 10.16
-13 3 10 -6.1 10.65
-13 3 10 -6.15 8.02
-13 3 10 -10.6 10.45
13 3 -9 2.67 5.17
-13 3 9 8.1 7.55
-13 3 9 -2.58 7.14
13 3 -9 4.37 6.63
-13 3 9 8.36 7.34
-13 3 8 -0.94 6.86
-13 3 8 2.07 8.33
13 3 -8 11.78 8.67
-13 3 8 -2.35 9.22
-13 3 7 17.47 9.41
-13 3 7 3.3 7.26
13 3 -7 -2.18 6.14
-13 3 7 11.21 9.22
-13 3 6 6.7 8.35
-13 3 6 5.66 8.65
-13 3 6 14.41 7.95
13 3 -6 -2.6 7.89
13 3 -6 9.89 4.84
-13 3 5 6.65 7.52
-13 3 5 2.14 6.46
-13 3 5 6.25 6.32
13 3 -5 4.28 5.85
13 3 -5 2.87 5.36
-13 3 4 41.09 13.19
-13 3 4 47.72 11.9
-13 3 4 39.61 14.59
13 3 -4 33.02 8.74
13 3 -4 48.55 13.22
13 3 -3 -4.59 7.52
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13 3 -3 -0.97 4.45
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13 3 -3 0.34 4.55
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13 3 -2 28.45 9.48
-13 3 2 11.03 8.52
13 3 -2 8.89 5.57
-13 3 2 17.98 10.9
13 3 -2 29 9.27
-13 3 2 25.88 9.51
13 3 -1 4.96 5
-13 3 1 12.04 11.03
13 3 -1 -1.12 6.32
-13 3 1 -9.6 10.05
13 3 -1 -0.16 5.43
13 3 -1 -0.17 5.47
-13 3 1 0.44 6.3
-13 3 0 -10.54 7.85
13 3 0 3.99 5.76
-13 3 0 -0.19 7.51
13 3 0 14.81 7.97
-13 3 0 -4.65 5.35
-13 3 0 3.34 5.08
13 3 0 15.02 7.93
-13 3 -1 -4.76 9.18
13 3 1 9.88 6.92
-13 3 -1 11.49 6.62
13 3 1 9.86 9.03
-13 3 -1 24.43 9.44
13 3 1 4.94 6.32
-13 3 -1 9 9.96
-13 3 -2 17.52 11.86
13 3 2 11.84 8.52
-13 3 -2 -1.67 7.81
13 3 2 -1.5 5.86
13 3 2 2.41 4.57
-13 3 -2 3.58 7.02
13 3 3 64.03 11.72
-13 3 -3 73.44 13.46
-13 3 -3 61.7 15.1
13 3 3 62.87 11.92
-13 3 -3 61.6 16.26
-13 3 -3 56.42 13.77
13 3 3 70.04 14.38
13 3 4 27.24 10.31
-13 3 -4 22.94 9.15
13 3 4 18.05 8.59
13 3 4 27.98 7.33
-13 3 -4 47.58 14.96
-13 3 -4 -0.18 9.38
-13 3 -4 22.08 8.49
13 3 4 38.17 11.48
13 3 5 133.56 20.48
-13 3 -5 157.96 22.38
13 3 5 158.13 21.01
13 3 5 126.3 15.4
-13 3 -5 108.69 20.6
-13 3 -5 134.63 21.97
-13 3 -5 128.65 20.03
13 3 5 122.28 18.39
13 3 6 21.79 9.87
-13 3 -6 20.81 8.92
13 3 6 27.66 10.76
13 3 6 37.56 8.98
-13 3 -6 34.58 12.86
13 3 6 25.94 9.55
-13 3 -6 27.66 11.72
-13 3 -6 26.21 10.03
-13 3 -7 99.45 19.1
13 3 7 116.18 18.52
-13 3 -7 90.98 18.73
13 3 7 103.44 18.5
-13 3 -7 78.4 16.88
13 3 7 87.07 17.03
-13 3 -8 8.17 9.55
13 3 8 13.43 8.74
-13 3 -8 7.21 9.71
13 3 8 5.04 8.04
-13 3 -8 6.82 7.94
13 3 8 1.7 7.8
-13 3 -9 37.23 13.81
13 3 9 39.32 11.82
-13 3 -9 50.97 15.71
13 3 9 53.34 14.78
-13 3 -9 39.19 12.27
13 3 9 40.29 11.53
-13 3 -10 18.07 9.82
13 3 10 19.56 12.22
-13 3 -10 18.57 13.32
13 3 10 13.91 11.05
-13 3 -10 5.02 6.59
13 3 10 -5.25 7.62
13 3 11 56.44 16.16
-13 3 -11 27.56 13.81
13 3 11 57.96 16.25
-13 3 -11 41.85 14.43
13 3 11 48.2 14.84
13 3 12 -2.22 7.97
-13 3 -12 25.82 14.86
13 3 12 -18.8 14.01
-13 3 -12 29.27 13.75
13 3 12 5.48 8.14
13 3 13 40.92 12.14
-13 3 -13 22.04 13.32
13 3 13 19.4 11.24
-13 3 -14 38.07 17.67
13 3 14 17.83 11.82
-13 3 -14 18.68 12.39
13 3 14 38.64 15.15
13 3 14 38.35 13.37
-13 3 -15 11.9 12.89
-13 3 -15 -5.15 9.67
13 3 15 1.65 7.43
13 3 15 0.25 9.2
-13 3 -16 -12.65 13.14
13 3 16 33.97 13.9
13 3 16 22.31 12.95
-13 3 -16 35.52 15.45
13 4 -22 105.22 20.44
13 4 -22 114.54 21.69
-13 4 21 88.79 21.62
13 4 -21 95.84 20.3
13 4 -21 94.89 20.66
13 4 -21 99.9 20.16
-13 4 20 133.06 25.7
13 4 -20 139.27 24.24
13 4 -20 156.53 24.2
13 4 -20 159.18 26.03
13 4 -19 145.79 22.75
13 4 -19 139.79 22.87
-13 4 19 123.2 25.11
-13 4 18 210.09 32.16
13 4 -18 180.29 28.74
13 4 -18 218.42 27.44
13 4 -18 210.73 27.26
-13 4 17 172.74 30.06
13 4 -17 190.47 27.73
13 4 -17 139.36 22.83
13 4 -17 181.27 24.5
13 4 -16 344.78 33.08
13 4 -16 295.08 34.32
-13 4 16 269.79 28.7
-13 4 16 247.86 35.28
13 4 -16 251.72 29.59
13 4 -15 166.67 22.6
13 4 -15 176.72 27.41
-13 4 15 127.24 20.36
-13 4 15 200.49 30.93
13 4 -15 131.25 20.75
13 4 -14 244.89 28.15
13 4 -14 260.09 27.08
-13 4 14 260.06 28.39
-13 4 14 213.27 26.24
-13 4 14 209.56 31.24
13 4 -14 218.04 29.41
13 4 -13 108.31 18.87
13 4 -13 153.51 21.11
-13 4 13 141.68 21.29
-13 4 13 118.28 19.84
-13 4 13 174.34 26.1
13 4 -13 176.89 26.18
-13 4 12 117.32 20.76
-13 4 12 142.97 21.69
-13 4 12 162.14 25.44
13 4 -12 158.95 21.03
13 4 -12 164.93 21.99
-13 4 11 321.57 32.48
-13 4 11 349.57 34.21
-13 4 11 361.26 37.26
13 4 -11 358.11 29.88
13 4 -11 342.54 31.31
-13 4 10 88.86 17.11
-13 4 10 80.13 16.24
-13 4 10 66.64 16.34
13 4 -10 81.15 14.39
13 4 -10 96.48 16.82
-13 4 9 371.48 36.24
-13 4 9 460.82 40.38
-13 4 9 455.05 39.46
13 4 -9 467.45 32.58
13 4 -9 468.23 35.6
-13 4 8 245.09 29.18
-13 4 8 149.54 23.02
-13 4 8 229.11 27.26
13 4 -8 224.93 22.02
13 4 -8 216.77 24.03
13 4 -7 379.07 31.05
-13 4 7 343.26 35.59
-13 4 7 298.07 33.5
-13 4 7 354.42 32.75
13 4 -6 233.8 24.13
-13 4 6 257.09 31.35
-13 4 6 211.74 28.02
-13 4 6 181.55 23.06
13 4 -5 349.79 28.91
-13 4 5 300.71 34.56
-13 4 5 352.08 36.49
-13 4 5 360.35 31.56
13 4 -4 175.57 19.97
-13 4 4 157.73 20.68
-13 4 4 139.68 25.66
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-13 4 3 307.28 35.47
-13 4 3 302.85 27.78
13 4 -3 305.89 25.95
-13 4 3 307.62 36.33
13 4 -3 294.04 29.22
-13 4 2 144.28 24.27
-13 4 2 113.85 22.73
13 4 -2 122.44 18.98
13 4 -2 127.06 17.02
-13 4 2 145.32 18.45
13 4 -2 146.06 17.73
-13 4 1 354.05 37.59
-13 4 1 357.65 29.18
13 4 -1 406.94 32.77
13 4 -1 341.4 28.14
-13 4 1 375.68 39.71
13 4 -1 376.55 28.39
-13 4 0 321.89 36.58
-13 4 0 289.48 34.33
13 4 0 269.44 24.46
-13 4 0 239.4 23.46
13 4 0 262.48 25.79
13 4 0 287.46 26.78
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13 4 0 269.89 23.87
-13 4 -1 213.9 29.82
13 4 1 255.84 23.06
-13 4 -1 249.94 23.25
13 4 1 264.1 26.21
-13 4 -1 253.18 26.15
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13 4 1 241.3 24.27
-13 4 -2 227.55 29.9
13 4 2 249.41 22.83
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13 4 2 221.07 24.61
-13 4 -2 192.14 23.45
13 4 2 221.59 22.28
-13 4 -3 127.24 21.74
13 4 3 148.76 17.5
13 4 3 155.74 20.22
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13 4 3 130.88 19.43
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13 4 3 165.84 18.65
-13 4 -4 333.18 30.68
13 4 4 326.17 28.89
13 4 4 299.79 28.29
-13 4 -4 270 31.91
13 4 4 354.07 26.46
-13 4 -4 368.45 37.68
-13 4 -4 340.3 32.22
13 4 4 377.98 33.75
13 4 5 122.81 20.17
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13 4 5 108.45 17.68
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13 4 5 112.39 14.81
-13 4 -5 107.6 21.85
-13 4 -5 99.15 17.81
13 4 5 140.1 19.65
13 4 6 208.03 26.36
-13 4 -6 197.39 25.83
13 4 6 226.32 25.37
-13 4 -6 196.34 26.65
-13 4 -6 205.39 28.17
-13 4 -6 221.5 26.8
13 4 6 175.6 22.56
13 4 7 118.05 20.42
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13 4 7 159.99 20.81
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-13 4 -7 182.91 24.99
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13 4 7 171.83 23.33
13 4 8 184.18 25.58
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13 4 8 192.15 23.28
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13 4 8 158.4 23.39
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-13 4 -9 143.8 22.46
13 4 9 184.23 23.55
-13 4 -9 134.14 24.44
13 4 9 161.3 24.07
-13 4 -9 134.59 23.05
13 4 9 178.53 26.48
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13 4 10 164.21 25.19
-13 4 -10 111.05 23.1
-13 4 -10 194.61 27.92
13 4 10 115.84 21.89
13 4 10 136.89 20.7
13 4 11 174.55 26.68
-13 4 -11 216.82 33.2
-13 4 -11 184.77 27.93
13 4 11 203.27 28.66
13 4 11 181.02 24.23
13 4 12 133.21 24.44
13 4 12 115.28 19.82
-13 4 -12 152.38 29.32
-13 4 -12 132.93 24.94
13 4 12 124.48 23.02
-13 4 -13 172.34 31.04
13 4 13 208.68 29.73
13 4 13 169.2 23.58
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13 4 13 152.73 26.49
-13 4 -14 93.34 22.53
13 4 14 69.68 18.26
13 4 14 85.3 18.53
-13 4 -14 69.06 18.59
-13 4 -15 127.7 25.67
13 4 15 140.51 25.19
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13 4 15 153.03 23.55
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13 4 16 76.98 17.24
13 5 -22 -3.19 9.81
13 5 -21 -7.15 8.15
13 5 -21 4.53 10.51
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13 5 -20 6.99 8.64
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13 5 -19 -0.06 9.63
13 5 -19 -4.23 10.28
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13 5 -18 -12.71 9.97
13 5 -18 3.17 9.04
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13 5 -17 4.41 8.47
13 5 -17 8.48 7.53
13 5 -17 7.07 7.32
13 5 -16 1.71 9.15
13 5 -16 3.4 7.54
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13 5 -16 2.04 8.14
13 5 -15 27.16 12.24
13 5 -15 9.84 8.21
-13 5 15 12.85 8.18
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13 5 -15 22.77 15.79
13 5 -14 -1.63 7.99
13 5 -14 13.09 8.58
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13 5 -14 15.6 9.42
13 5 -13 0.81 8.44
13 5 -13 16.51 11.51
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13 5 -13 2.68 7.63
13 5 -12 13.54 9.51
13 5 -12 19.23 9.04
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13 5 -12 2.59 8.99
13 5 -11 -0.82 6.93
13 5 -11 -0.37 5.37
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13 5 -11 -6.59 9.35
13 5 -10 6.05 7.36
13 5 -10 15.51 8.45
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13 5 -10 10.95 6.88
13 5 -9 2.39 7.39
13 5 -9 -1.61 5.98
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13 5 -9 18.41 11.98
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13 5 -8 4.97 5.58
13 5 -8 11.11 8.33
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13 5 -7 19.03 8.09
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13 5 -7 27.87 12.09
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13 5 -6 -10.56 8.07
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13 5 -5 48.68 12.16
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13 5 -4 16.11 7.59
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13 5 -3 2.8 4.09
13 5 -3 8.25 6.56
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13 5 -2 127.46 16.67
13 5 -2 116.97 16.87
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13 5 -2 122.04 15.72
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13 5 -1 21.22 7.66
13 5 -1 1.52 4.61
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13 5 -1 19.76 7.41
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13 5 0 59.39 12.42
13 5 0 53.18 12.13
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13 5 0 53.55 11.13
13 5 0 48.94 11.47
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13 5 1 98.51 14.73
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13 5 1 88.49 14.45
13 5 1 114.66 17.46
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13 5 1 90.2 14.21
13 5 1 78.81 13.46
-13 5 -1 87.32 15.1
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13 5 2 24.18 8.5
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13 5 2 31.13 9.87
-13 5 -2 15.21 8.99
13 5 2 23.27 8.19
13 5 3 58.55 13.03
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13 5 3 49.41 10.6
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13 5 3 38.71 12.07
13 5 4 28.16 9.28
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13 5 4 23.17 6.85
-13 5 -4 33.07 13
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13 5 4 29.09 10.08
13 5 5 17 9.5
-13 5 -5 8.62 9.15
13 5 5 3.4 5.88
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13 5 5 3.55 6.37
13 5 6 -4.28 9.24
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13 5 6 -4.63 6.34
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13 5 6 -8.16 7.91
13 5 7 26.02 11.61
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13 5 7 28.06 8.45
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-13 5 -7 9.22 9.15
13 5 7 15.37 10.45
13 5 8 5.88 9.6
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13 5 8 2.49 5.76
-13 5 -8 8.46 6.51
-13 5 -8 6.35 8.01
-13 5 -8 9.24 10.1
13 5 8 34.71 12.43
13 5 9 34.81 13.89
-13 5 -9 28.87 13.4
13 5 9 31.27 11.22
-13 5 -9 25.3 11.75
13 5 9 29.19 12.28
-13 5 -9 23.11 10.24
-13 5 -9 31.3 12.33
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13 5 10 9.54 9.18
13 5 10 5.75 6.53
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-13 5 -10 7.05 6.89
13 5 10 11.8 10.35
13 5 11 13.49 8.48
13 5 11 24.92 12.51
13 5 11 36.07 13.58
-13 5 -11 19.12 9.94
-13 5 -11 26.81 12.71
13 5 11 36.67 14.38
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13 5 12 -11.23 11.26
13 5 12 5.47 6.21
-13 5 -12 4.49 7.85
13 5 12 -3.63 8.91
-13 5 -13 1.71 12.16
13 5 13 19.29 11.71
13 5 13 42.58 12.79
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13 6 -20 185.91 27.43
13 6 -19 31.21 11.27
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13 6 -18 275.48 31.1
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13 6 -18 295.37 32.26
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13 6 -17 27.85 12.91
13 6 -17 9.19 7.29
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13 6 -16 283.79 30.75
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13 6 -16 294.2 32.06
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13 6 -16 280.33 35.11
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13 6 -14 374.94 34.02
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13 6 -14 365.94 39.04
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13 9 13 2.03 8.14
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13 10 -16 316.9 33.83
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13 10 -16 316.78 34.61
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13 10 -14 303.17 35.92
13 10 -14 293.84 32.7
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13 10 -14 293.84 32.25
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13 10 -13 17.08 10.39
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13 10 -13 3.12 9.08
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13 10 -13 36.05 14.56
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13 10 -12 406.98 37.03
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13 10 -12 419.57 38.2
13 10 -12 357.63 30.9
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13 10 -11 4.84 7.1
13 10 -11 20.08 10.87
13 10 -11 12.16 8.85
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13 10 -10 444.8 37.14
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13 10 -10 420.74 37.8
13 10 -10 354.21 30.8
13 10 -10 425.75 40.09
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13 10 -9 28.35 9.24
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13 10 -9 20.02 8.62
13 10 -9 31.37 11.33
13 10 -9 25.16 11.34
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13 10 -8 444.79 36.97
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13 10 -8 412.94 36.98
13 10 -8 411.12 33.45
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13 10 -7 47.13 13.15
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13 10 -7 55.34 14.4
13 10 -7 67.87 14.24
13 10 -7 63.13 14.27
13 10 -6 623.63 41.54
13 10 -6 578.05 43.06
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13 10 -6 515.28 38.67
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13 10 -5 23.31 9.49
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13 10 -5 32.7 11.9
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13 10 -4 495.13 37.2
13 10 -4 474.89 35.29
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13 10 -4 486.51 37.41
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13 10 -3 29.53 10.91
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13 10 -3 22.41 11.11
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13 10 -2 415.02 35.6
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13 10 -2 483.6 39.88
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13 10 -1 10.27 6.66
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13 10 -1 23.79 10.33
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13 10 0 405.69 35.99
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13 10 2 394.23 37.43
13 10 2 373.73 32.79
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13 10 11 38.66 16.21
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13 11 10 15.58 13.04
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13 12 -16 128.09 23.18
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13 12 -15 37.6 14.21
13 12 -15 50.85 16.42
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13 12 -14 246.86 30.5
13 12 -14 165.37 23.15
13 12 -14 202.51 27.34
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13 12 -13 69.32 18.12
13 12 -13 53.54 14.01
13 12 -13 69.73 16.63
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13 12 -12 160.4 22.06
13 12 -12 155.1 24.57
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13 12 -11 117.65 20.77
13 12 -11 98.54 17.89
13 12 -11 161.12 24.84
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13 12 -11 126.04 23.23
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13 12 -10 143.39 22.87
13 12 -10 134.86 20.21
13 12 -10 156.32 23.98
13 12 -10 143.85 23.72
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13 12 -9 135.94 21.62
13 12 -9 121.16 19.32
13 12 -9 116.89 21.22
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13 12 -9 201.23 27.26
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13 12 -8 159.6 23.32
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13 12 -8 149.69 23.84
13 12 -8 155.42 22.62
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13 12 -7 77.37 16.57
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13 12 -7 69.13 16.81
13 12 -7 70.08 16.45
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13 12 -6 149.91 21.68
13 12 -6 132.91 21.02
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13 12 -5 151.4 22.11
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13 12 -5 149.91 22.29
13 12 -5 132.14 22.9
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13 12 -4 124.32 20.81
13 12 -4 126.58 22.71
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13 12 -3 106.31 18.78
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13 12 -3 124.68 20.96
13 12 -3 138.06 22.94
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13 12 -2 176.93 23.98
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13 12 -2 146.36 22.02
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13 12 -1 151.16 22.55
13 12 -1 183.75 25.8
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13 12 -1 120.18 21.45
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13 12 0 243.88 28.54
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13 12 0 210.87 27.4
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13 12 1 143.22 21.71
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13 12 1 110.27 20.13
13 12 1 111.51 21.1
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13 12 2 261.45 29.18
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13 12 2 262.74 32.26
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13 12 3 93.33 17.51
13 12 3 107.78 21.83
13 12 4 274.25 32.52
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13 12 4 264.48 28.35
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13 12 4 240.64 31.74
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13 12 5 72.58 18.6
13 12 6 197.15 28.65
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13 12 6 189.11 29.27
13 12 7 152.95 25.73
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13 12 7 115.06 24.79
13 12 8 126.11 23.36
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13 12 8 127.06 24.66
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13 12 9 77.74 18.25
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13 12 9 72.96 18.62
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13 12 10 23.33 9.32
13 12 10 55.3 17.4
13 12 11 34.43 12.31
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13 13 -12 4.19 8.9
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13 13 -12 13.09 8.05
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13 13 -11 14.41 8.85
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13 13 -11 7.77 7.58
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13 13 -10 9.65 8.25
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13 13 -9 5.8 8.09
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13 13 -8 1.39 7.28
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14 1 -8 8.63 10.01
14 1 -8 11.22 7.74
-14 1 7 499.64 45.83
-14 1 7 576.4 44.15
14 1 -7 522.4 40.83
14 1 -7 523.37 35.95
-14 1 6 13.26 8.94
14 1 -6 -2.56 7.68
14 1 -6 3.29 5.23
-14 1 6 1.29 7.58
-14 1 5 478.76 39.23
-14 1 5 557.08 50.31
14 1 -5 526.7 40.58
14 1 -5 561.24 35.57
-14 1 4 13.66 11.95
14 1 -4 7.61 6.81
-14 1 4 11.73 8.44
14 1 -4 13.92 8.14
-14 1 3 541.29 49.42
14 1 -3 536.78 40.33
-14 1 3 576.42 41.54
14 1 -3 551.31 38.9
-14 1 2 6.65 8.37
14 1 -2 4.88 5.98
14 1 -2 12.89 8.89
-14 1 2 19.2 9.98
14 1 -1 426.25 31.43
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14 1 -1 357.51 30.58
14 1 -1 439.07 34.55
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14 1 0 11.62 6.39
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14 1 0 16.53 8.49
14 1 0 8.16 7.75
-14 1 0 30.89 10.72
14 1 1 514.49 37.18
-14 1 -1 530.18 47.59
14 1 1 582.02 38.42
14 1 1 633.91 39.9
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14 1 2 1.11 6.59
-14 1 -2 10.07 9.77
14 1 2 14.96 8.91
14 1 2 14.84 9.34
-14 1 -2 8.31 9.29
14 1 3 659.5 44.5
-14 1 -3 689.78 53.29
14 1 3 709.31 41.85
14 1 3 673.69 39.83
-14 1 -3 643.68 47.06
-14 1 -4 0.99 9.55
14 1 4 17.46 11.44
-14 1 -4 9.78 11.79
14 1 4 31.42 10.77
-14 1 -4 22.82 10.31
14 1 4 4.6 8.68
-14 1 -5 579.28 46.33
14 1 5 581.06 43.82
-14 1 -5 543.05 47.1
14 1 5 546.92 36.25
-14 1 -5 617.54 44.92
14 1 5 665.66 45.78
-14 1 -6 -2.52 10.01
-14 1 -6 16.29 9.68
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14 1 6 4.29 7.53
-14 1 -7 504.01 43.66
14 1 7 459.04 38.24
14 1 7 550.47 42.08
-14 1 -7 411.53 40.49
-14 1 -7 557.18 46.61
14 1 7 502.44 34.14
14 1 7 423.3 39.06
-14 1 -8 38.41 13.5
-14 1 -8 34.07 13.93
14 1 8 31.67 10.54
-14 1 -8 56.81 16.29
14 1 8 19.03 10.19
14 1 8 29.4 9.67
-14 1 -9 298.67 33.59
-14 1 -9 365.14 39.29
14 1 9 321.31 32.85
-14 1 -9 274.05 34.58
14 1 9 346.28 36.07
14 1 9 331.27 34.3
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14 1 10 23.54 10.57
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14 1 10 13.58 8.08
14 1 10 11.85 10.64
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14 1 11 211.09 27.9
14 1 11 212.82 27.04
-14 1 -11 216.66 32.17
14 1 12 -9.03 9.9
-14 1 -12 4.83 11.05
14 1 13 173.45 25.17
-14 1 -13 194.11 34.63
-14 1 -13 122.13 24.47
14 1 14 7.6 8.21
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14 2 -21 1.95 7.92
14 2 -21 -0.08 7.66
14 2 -20 6.57 6.92
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14 2 -20 7.42 9.51
14 2 -20 4.88 7.32
14 2 -19 -5.39 8.11
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14 2 -19 3.7 9.61
14 2 -19 18.57 10.22
14 2 -18 18.02 8.63
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14 2 -18 8.32 9.14
14 2 -18 27.93 11.35
14 2 -17 5.41 7.29
14 2 -17 13.45 10.81
14 2 -17 22.87 9.72
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-14 2 16 7.97 8.68
14 2 -16 8.36 8.54
14 2 -16 18.2 12.17
-14 2 16 11.89 9.22
14 2 -16 7.45 8.37
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14 2 -15 -10.8 8.48
14 2 -15 -6.13 6.37
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14 2 -15 -3.77 8.03
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14 2 -14 24.27 11.88
14 2 -14 26.15 10.22
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14 2 -14 25.2 8.87
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14 2 -13 11.69 10.32
14 2 -13 -2.37 7.96
-14 2 13 12.28 10.66
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14 2 -12 102.03 19.63
14 2 -12 90.19 16.24
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14 2 -11 24.78 12.12
14 2 -11 32.28 11.59
-14 2 11 17.16 10.51
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14 2 -10 56.95 15.47
14 2 -10 57.58 12.93
-14 2 10 68.9 17.3
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14 2 -9 38.69 12.22
14 2 -9 42.23 12.58
-14 2 9 33.36 11.58
-14 2 8 25.57 13.19
14 2 -8 40.28 12.97
14 2 -8 35.23 11.54
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14 2 -7 12.79 8.28
14 2 -7 10 6.53
-14 2 7 17.73 8.64
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14 2 -6 54.07 14.4
14 2 -6 43.57 11.77
-14 2 5 1.67 7.41
-14 2 5 -2.12 7.05
-14 2 5 2.18 9.02
14 2 -5 1.93 6.01
14 2 -5 1.44 4.99
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14 2 -4 42.75 12.6
14 2 -4 58.53 12.22
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14 2 -3 14.75 8.59
14 2 -3 38.95 11.77
-14 2 3 28.28 13.71
-14 2 3 13.24 8.17
-14 2 2 98.41 22.6
14 2 -2 113.43 17.14
-14 2 2 106.83 22.64
14 2 -2 151.03 20.5
-14 2 2 102.51 16.85
14 2 -1 -2.63 5.76
-14 2 1 8.71 7.49
14 2 -1 5.68 5.05
14 2 -1 -0.09 6.11
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14 2 0 98.29 15.93
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14 2 0 77.91 14.27
14 2 0 70.58 13.38
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14 2 1 -0.01 6.37
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14 2 1 4.78 7.91
14 2 1 11.71 7.44
-14 2 -1 -1.9 6.38
14 2 2 5.91 5.23
-14 2 -2 23.16 12.08
14 2 2 14.65 8
14 2 2 11.13 5.48
-14 2 -2 14.45 8.95
-14 2 -3 16.92 11.58
14 2 3 7.7 6.87
14 2 3 7.71 5.65
-14 2 -3 16.24 10.73
-14 2 -4 14.56 9.94
-14 2 -4 39.88 13.68
14 2 4 24.96 8.96
14 2 4 32.12 10.52
14 2 4 35.97 9.72
14 2 5 0.98 6.92
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-14 2 -5 5.57 6.8
14 2 5 -6.33 9.46
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14 2 5 7.29 5.77
14 2 6 51.55 14.88
-14 2 -6 31.85 11.78
-14 2 -6 33.87 12.26
-14 2 -6 45.13 14.06
14 2 6 45.24 10.91
14 2 6 18.93 9.52
-14 2 -7 25.87 11.97
-14 2 -7 15.64 9.6
14 2 7 30.07 9.91
-14 2 -7 10.42 8
14 2 7 25.2 12.25
14 2 7 36.12 13.99
-14 2 -8 29.95 12.21
-14 2 -8 22.64 11.35
14 2 8 42.22 13.38
-14 2 -8 27.93 13.99
14 2 8 41.55 14.18
14 2 8 24.65 10.76
-14 2 -9 60.82 16.32
-14 2 -9 75.09 19.26
14 2 9 56.13 15.22
-14 2 -9 71.8 17.16
14 2 9 104.79 20.41
14 2 9 89.85 17.89
-14 2 -10 15.06 9.23
14 2 10 13.33 9.25
-14 2 -10 26.28 13.92
14 2 10 1.55 10.71
14 2 10 19.36 11.29
-14 2 -11 28.06 12.88
14 2 11 45.37 15.26
14 2 11 25.59 10.89
-14 2 -11 33.79 14.64
14 2 12 24.84 10.95
-14 2 -12 16.57 11.07
14 2 13 11.04 8.7
-14 2 -13 32.64 15.21
14 2 14 26.03 12.18
-14 2 -14 17.25 15.4
-14 2 -14 25.83 14.96
14 3 -21 212.29 27.67
14 3 -20 61.19 15.68
-14 3 20 65.31 19.43
14 3 -20 52.73 15.19
14 3 -20 33.91 12.87
14 3 -19 244.34 28.91
-14 3 19 268.93 38.78
14 3 -19 201.02 27.83
14 3 -19 212.04 29.11
14 3 -18 91.12 18.77
-14 3 18 90.04 24.16
14 3 -18 146.81 25.08
14 3 -18 70.48 17.99
14 3 -17 248.43 28.37
14 3 -17 219.54 28.98
14 3 -17 251.39 30.35
-14 3 17 230.32 35.9
-14 3 16 165.94 29.7
14 3 -16 104.08 18.68
14 3 -16 126.32 22.47
14 3 -16 156.57 25.53
-14 3 16 98.81 18.59
14 3 -16 153.21 24.39
-14 3 15 288.77 38.71
14 3 -15 249.2 27.03
14 3 -15 260.3 31.29
14 3 -15 275.1 33.67
-14 3 15 255.34 30.31
14 3 -15 270.34 30.55
14 3 -14 151.84 24.23
-14 3 14 157.79 28.06
-14 3 14 145.81 22.53
14 3 -14 223.87 27.01
14 3 -14 214.17 25.49
14 3 -13 377.67 36.92
-14 3 13 330.26 39.13
-14 3 13 338.74 35.53
14 3 -13 414.07 35.99
14 3 -13 427.32 34.67
-14 3 12 258.13 34.03
14 3 -12 266.91 31.46
14 3 -12 258.22 27.27
-14 3 12 201.23 27.79
-14 3 11 266.72 32.91
-14 3 11 214.39 28.64
14 3 -11 238.87 28.62
14 3 -11 237.59 26.35
-14 3 10 159.87 25.24
-14 3 10 158.93 25.26
-14 3 10 148.14 24.94
14 3 -10 122.18 21.48
14 3 -10 155.95 20.73
-14 3 9 279.47 31.97
-14 3 9 272.83 32.25
-14 3 9 243.88 30.64
14 3 -9 264.12 30.3
14 3 -9 283.4 27.95
-14 3 8 135.72 22.62
-14 3 8 138.23 23.45
-14 3 8 114.05 21.86
14 3 -8 135.99 20.83
14 3 -8 150.15 19.71
-14 3 7 400.9 37.1
-14 3 7 370.94 39.03
-14 3 7 352.96 38.35
14 3 -7 442.69 37.82
14 3 -7 386.14 31.8
-14 3 6 67.64 14.81
-14 3 6 105.92 21.96
-14 3 6 83.62 20.16
14 3 -6 81.71 15.88
14 3 -6 58 12.18
-14 3 5 383.3 33.85
-14 3 5 381.44 40.11
-14 3 5 336.12 39.3
14 3 -5 355.9 33.59
14 3 -5 365.62 30.21
-14 3 4 26.25 10.47
-14 3 4 28.31 13.13
-14 3 4 30.93 13.86
14 3 -4 6.33 7.07
14 3 -4 15.95 5.65
-14 3 3 302.06 29.15
-14 3 3 313.14 37.27
14 3 -3 283.63 29.97
14 3 -3 289.09 25.64
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14 3 -2 18.49 8.69
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-14 3 2 25.95 9.18
14 3 -2 27.38 9.63
-14 3 1 337.74 30.27
-14 3 1 412.58 43.21
14 3 -1 389.15 30.55
14 3 -1 384.54 31.17
-14 3 1 340.24 39.07
14 3 -1 367.2 32.21
-14 3 0 62.68 13.41
14 3 0 34.42 9.16
14 3 0 69.1 13.52
-14 3 0 18.1 12.78
-14 3 0 56.74 17.59
14 3 0 31.06 10.23
-14 3 -1 300.62 30.32
14 3 1 289.82 27.78
14 3 1 283.71 26.31
-14 3 -1 306.44 35.9
-14 3 -1 278.07 34.3
14 3 1 274.89 26.37
-14 3 -2 107.81 18.76
-14 3 -2 84.29 21.03
14 3 2 95 16.55
14 3 2 85.97 14.66
-14 3 -2 109.94 22.69
14 3 2 100.47 15.74
14 3 3 299.89 29.92
-14 3 -3 363.7 34.15
-14 3 -3 273.23 34.24
14 3 3 336.71 27.62
-14 3 -3 340.8 37.26
14 3 3 344.95 32.14
14 3 4 186.37 23.9
-14 3 -4 131.68 21.11
-14 3 -4 143.71 23.91
14 3 4 160.82 19.22
14 3 4 113.62 19.37
14 3 5 226.08 25.67
-14 3 -5 244.8 29.31
-14 3 -5 164.32 26.61
14 3 5 202.85 20.87
14 3 5 189.51 25.4
14 3 6 99.04 18.48
-14 3 -6 82.94 17.29
-14 3 -6 97.05 19.09
-14 3 -6 92.87 20.25
14 3 6 96.12 20.06
-14 3 -7 95.81 19.64
14 3 7 174.91 23.41
-14 3 -7 112.35 21.67
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14 3 7 102.74 18.22
14 3 7 148.13 23.63
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14 3 8 50.47 14.4
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14 3 8 23.06 11.71
14 3 8 30.49 11.44
-14 3 -9 142.97 24.33
-14 3 -9 239.06 31.21
-14 3 -9 203.23 29.29
14 3 9 217.34 29.42
14 3 9 163.04 24.67
14 3 9 185.69 24.87
-14 3 -10 31.77 13.18
-14 3 -10 55.39 17.13
14 3 10 49.42 14.77
14 3 10 56.8 15.53
14 3 10 68.23 16.46
-14 3 -11 117.62 23.99
14 3 11 157.36 25.27
-14 3 -11 157.25 27.29
14 3 11 162.19 23.25
-14 3 -12 41.78 15.64
-14 3 -12 40.82 16.09
14 3 12 57.26 15.09
-14 3 -13 117.77 26.91
14 3 13 101.06 19.79
-14 3 -13 91.16 21.97
-14 3 -14 23.81 15.08
14 3 14 24.89 11.68
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14 3 14 15.74 9.11
14 4 -21 3.5 9.48
14 4 -20 33.54 13.44
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14 4 -20 11.81 11.93
14 4 -20 11.29 10.4
14 4 -19 17.25 10.36
14 4 -19 -4.57 9.34
14 4 -19 9.1 8.11
14 4 -18 17.47 9.64
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14 4 -18 29.53 13.8
14 4 -18 7.74 8.15
14 4 -17 -5.63 7.5
14 4 -17 -9.47 9.94
14 4 -17 0.66 8.79
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14 4 -16 -5.6 8.57
14 4 -16 4.45 8.57
14 4 -16 -11.9 10.65
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14 4 -16 -11.81 10.33
14 4 -15 7.59 7.43
14 4 -15 4.21 7.36
14 4 -15 2.13 8.71
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14 4 -14 5.06 8.73
14 4 -14 -2.88 8.46
14 4 -14 10.19 9.36
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14 4 -13 21.49 9.36
14 4 -13 -4.03 6.83
14 4 -13 15.57 12.23
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14 4 -12 -3.44 6.68
14 4 -12 3.66 8.11
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14 4 -12 -7.47 7.22
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14 4 -11 25.92 12.2
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14 4 -10 -1.85 7.51
-14 4 10 4.7 7.09
-14 4 9 5.57 8
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14 4 -9 23.64 11.1
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-14 4 8 -7.53 8.16
14 4 -8 14.22 8.37
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14 4 -7 19.45 9.57
14 4 -7 24.96 9.87
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14 4 -6 -0.33 6.93
14 4 -6 1.98 6.9
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14 4 -5 46.18 12.7
14 4 -5 37 10.5
-14 4 4 8.56 9.09
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14 4 -4 15.82 7.33
14 4 -4 7.76 5.96
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14 4 -3 4.18 5.7
14 4 -3 5.02 6.28
-14 4 2 71.02 18.41
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-14 4 2 49.76 11.64
14 4 -2 48.03 10.99
14 4 -2 64.25 14.87
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14 4 -1 8.08 7.23
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14 4 -1 30.55 10.24
14 4 -1 20.17 10.13
-14 4 0 48.32 11.17
14 4 0 50.1 11.91
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14 4 0 45.76 10.68
-14 4 0 45.16 18.34
14 4 0 38.99 11.49
-14 4 -1 17.59 9.5
14 4 1 -1.91 6.3
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14 4 1 8.35 5.22
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14 4 1 17.06 7.97
-14 4 -2 62.68 15.03
-14 4 -2 56.51 17.29
14 4 2 71.06 14.02
-14 4 -2 34.12 13.42
14 4 2 58.04 11.94
14 4 2 73.83 13.91
14 4 3 4.13 6.41
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-14 4 -3 -5.66 11.76
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14 4 3 26.56 8.53
14 4 3 12.79 8.77
14 4 4 116.99 18.71
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14 4 4 80.5 13.4
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14 4 4 102 18.28
14 4 5 22.69 9.28
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-14 4 -5 19.2 10.87
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14 4 5 31.34 10.43
14 4 6 30.53 9.89
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14 4 6 59.38 15.03
14 4 7 62.32 14.99
-14 4 -7 40.94 12.29
-14 4 -7 44.69 15.42
-14 4 -7 33.54 13.23
14 4 7 51.72 14.21
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14 4 8 44.08 11.92
-14 4 -8 18.53 12.13
-14 4 -8 65.42 16.88
14 4 8 49.33 14.44
14 4 8 67.19 18.7
-14 4 -9 24.2 11.42
-14 4 -9 23.45 11.68
-14 4 -9 66.16 17.18
14 4 9 29.68 12.65
14 4 9 34.99 14.59
14 4 9 51.24 13.75
-14 4 -10 26.44 11.71
-14 4 -10 16.13 11.74
14 4 10 49.95 15.39
14 4 10 27.96 12.18
14 4 10 43.34 13
-14 4 -11 109.04 25.66
14 4 11 116.19 20.3
14 4 11 127.6 23.04
-14 4 -11 98.01 22.04
14 4 12 15.8 10.72
14 4 12 21.68 10.28
-14 4 -12 5.26 9.9
-14 4 -12 4.61 8.83
14 4 13 77.08 18.76
14 4 13 113.84 21.13
-14 4 -13 44.74 17.52
-14 4 -13 95.59 23.93
14 4 14 4.18 7.18
-14 4 -14 -15.18 11.24
14 5 -20 204.07 28.5
-14 5 20 207.92 33.25
14 5 -20 154.5 25.55
14 5 -20 170.33 26.32
-14 5 19 83.7 21.82
14 5 -19 78 18.78
14 5 -19 93.54 19.95
14 5 -18 123.3 22.58
14 5 -18 153.92 23.72
-14 5 17 131.53 27.16
14 5 -17 103.2 19.52
14 5 -17 116 21.84
-14 5 16 307.52 32.22
-14 5 16 251.71 36.02
14 5 -16 257.67 30.36
14 5 -16 263.52 29.64
14 5 -15 89.82 18.69
14 5 -15 112.03 19.46
-14 5 15 120.08 25.52
-14 5 15 74.91 17.24
-14 5 15 91.02 17.93
14 5 -15 87.42 19.36
14 5 -14 349.42 34.16
14 5 -14 343.52 33.04
-14 5 14 329.4 39.78
-14 5 14 339.78 34.94
-14 5 14 324.77 33.85
14 5 -14 374.51 40.17
14 5 -13 80.74 17.54
14 5 -13 77.33 15.58
-14 5 13 49.57 16.35
-14 5 13 90.98 19.11
-14 5 13 55.17 14.97
14 5 -13 63.05 17.12
14 5 -12 252.21 28.98
14 5 -12 240.59 26.14
-14 5 12 272.92 35.73
-14 5 12 259.6 30.98
-14 5 12 304.76 32.83
14 5 -12 308.75 35.47
14 5 -11 118.85 20.37
14 5 -11 90.76 17.02
14 5 -11 91.8 19.23
-14 5 11 75.97 15.93
-14 5 11 60.71 14.93
-14 5 11 98.16 20.62
-14 5 10 273.19 31.56
14 5 -10 336.73 36.26
-14 5 10 197.46 27.46
14 5 -10 231.7 26.14
-14 5 10 276.04 31.92
-14 5 9 121.26 21.58
14 5 -9 115.69 21.62
-14 5 9 119.33 21.12
14 5 -9 134.83 20.26
-14 5 9 127.58 22.89
-14 5 8 316.25 33.27
14 5 -8 367.87 37.42
-14 5 8 329.69 36.17
14 5 -8 280.91 28.75
-14 5 8 290.82 34.74
-14 5 7 190.42 25.71
14 5 -7 193.46 26.5
-14 5 7 155.59 25.55
14 5 -7 174.41 22.19
-14 5 7 153.37 25.43
14 5 -6 349.95 31.01
-14 5 6 417.47 41.48
-14 5 6 393.01 35.14
-14 5 6 417.3 40.97
14 5 -5 205.8 22.98
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14 5 -4 343.84 33.86
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14 5 -3 268.25 30.03
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14 5 -3 264.09 25.68
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14 5 1 81.6 15.36
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14 5 2 156.19 22
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-14 9 -4 333.77 37.89
-14 9 -4 320.36 37.22
14 9 4 374.06 38.3
14 9 4 307.27 33.97
-14 9 -5 22.61 10.28
-14 9 -5 6.18 8.39
-14 9 -5 22.16 13.66
14 9 5 22.56 11.87
14 9 5 0.16 7.16
-14 9 -6 244.58 30.32
-14 9 -6 285.34 34.13
-14 9 -6 261.63 32.8
14 9 6 284.58 33.88
14 9 6 225.51 31.03
14 9 7 -11.2 11.2
-14 9 -7 2.68 8.48
-14 9 -7 3.4 7.02
-14 9 -7 6.58 9.05
14 9 8 161.18 26.54
-14 9 -8 181.11 27.35
-14 9 -8 128.53 22.31
-14 9 -8 180.17 26.57
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-14 9 -9 -16.53 9.27
-14 9 -9 9.18 9.02
-14 9 -9 -4.39 8.68
14 9 10 190.59 29.87
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14 10 -17 8.11 8.29
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14 10 -16 17.62 11.03
-14 10 16 6.12 9.13
-14 10 16 5.49 10.21
14 10 -16 -7.5 9.22
14 10 -15 19.62 10.28
-14 10 15 21.18 9.78
14 10 -15 8.74 8.21
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14 10 -14 6.67 7.64
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14 10 -14 -8.93 9.55
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14 10 -13 -6.74 10.7
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14 10 -12 -8.98 8.11
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14 10 -12 -5.96 10.85
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14 10 -12 9.49 12.64
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14 10 -11 14.05 7.16
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14 10 -11 65.7 16.29
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14 10 -8 7.49 8
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14 10 -7 45.26 11.07
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14 10 -6 4.3 5.91
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14 10 -4 19.27 9.59
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14 10 -4 7.06 6.11
14 10 -4 25.69 12.04
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14 10 -3 58.75 15.25
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14 10 -1 32.58 10.94
14 10 -1 71.28 14.76
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14 10 1 44.21 13.52
14 10 1 33.99 11.39
14 10 1 28.8 10.82
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14 10 1 25.72 11.57
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14 10 2 46.02 15.28
14 10 2 40.74 13
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14 10 5 34.79 13.53
14 10 5 32.6 14.49
14 10 6 47.2 16.25
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-14 10 -6 70.89 17.43
14 10 7 20.05 10.43
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-14 10 -7 26.85 10.77
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14 10 10 -8.24 9.19
-14 11 16 156.56 28.96
14 11 -16 257.21 31.64
14 11 -15 25.91 12.59
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14 11 -15 17.51 10.28
-14 11 15 40.83 13.69
-14 11 15 18.4 8.6
14 11 -14 162.04 25.22
-14 11 14 251.95 31.13
14 11 -14 209.57 28.63
-14 11 14 198.63 27.62
-14 11 14 261.4 35.23
14 11 -13 19.2 8.01
-14 11 13 49.61 15.48
14 11 -13 35.53 12.63
-14 11 13 28.54 13.67
-14 11 13 43.64 14.17
14 11 -12 241.92 29.3
-14 11 12 162.71 27.38
14 11 -12 254.65 31.79
-14 11 12 269.4 33.27
-14 11 12 225.45 31.91
-14 11 11 7.64 7.18
-14 11 11 25.2 12.97
14 11 -11 38.8 12.73
14 11 -11 30.1 11.08
14 11 -11 19.98 9.23
-14 11 11 29.96 11.64
-14 11 10 271.2 32.87
14 11 -10 285.45 32.89
14 11 -10 275.92 31.5
14 11 -10 316.02 35.47
-14 11 10 360.63 38.38
14 11 -9 16.39 10.19
14 11 -9 35.7 11.87
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14 11 -8 204.21 25.07
14 11 -8 173.18 25.58
14 11 -8 216.31 26.65
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14 11 -7 56.98 13.12
14 11 -7 53.98 13.36
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14 11 -6 173.33 23.46
14 11 -6 180.94 25.96
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14 11 -5 53.96 14.34
14 11 -5 54.03 13.95
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14 11 -5 25.3 11.79
-14 11 5 60.85 18.04
14 11 -4 153.26 22.37
14 11 -4 196.97 26.59
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14 11 -4 207.73 28.54
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14 11 -3 108.44 20.71
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14 11 -3 105.76 19.6
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14 11 -2 146.25 22.23
14 11 -2 213.95 28.33
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14 11 -1 65.72 16.22
14 11 -1 64.7 15.59
-14 11 1 37.15 15.98
14 11 -1 60.81 14.42
-14 11 0 217.43 31.87
14 11 0 196.68 25.91
14 11 0 144 22.2
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14 11 0 181.52 25.44
-14 11 -1 38.08 16.08
14 11 1 26.11 11.76
14 11 1 15.11 9.37
-14 11 -1 34.93 16.59
14 11 1 34.92 13.14
14 11 2 159.01 25.09
14 11 2 202.24 25.43
-14 11 -2 184.9 29
-14 11 -2 151.47 27.27
14 11 3 21.18 11.86
-14 11 -3 27.77 13.39
-14 11 -3 11.1 11.15
14 11 4 154.34 25.16
-14 11 -4 151.64 26.48
14 11 4 181.28 27.76
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14 11 5 30.12 13.32
-14 11 -5 17.9 12.1
14 11 5 7.34 7.41
-14 11 -5 16.95 11.68
-14 11 -6 220.16 31.13
14 11 6 179.7 28.24
-14 11 -6 213.42 29.87
-14 11 -7 1.97 9.29
14 11 7 1.74 7.66
-14 11 -7 14.38 13.82
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14 11 9 -1.07 10.78
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14 12 -14 -2.4 7.41
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14 12 -10 -10.68 11.83
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14 12 -8 -1.24 7.77
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14 12 -8 -18.43 10.25
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14 12 0 17.82 10.68
14 12 0 37.67 12.05
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14 12 1 8.27 7.46
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14 12 1 3.61 8.02
14 12 1 -0.04 6.76
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14 12 2 57.13 15.63
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14 12 2 37.56 13.52
14 12 2 30.62 12.38
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14 12 5 25.19 14.72
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14 12 6 55.85 16.23
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14 12 7 2.33 10.93
14 12 7 23.39 13.13
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14 12 8 11.28 11.78
14 13 -13 130.14 23.5
-14 13 13 129.58 25.33
14 13 -12 107.91 20.49
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-14 13 12 100.86 21.39
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14 13 -11 127.36 20.96
-14 13 11 141.33 24.47
14 13 -11 116.41 22.25
-14 13 11 168.71 27.53
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14 13 -10 140.12 23.02
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14 13 -10 135.95 24.37
14 13 -10 112.68 19.57
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14 13 -9 165.09 24.78
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14 13 -9 142.61 23.68
-14 13 9 166.67 27.29
14 13 -9 140.76 21.45
14 13 -8 63.14 15.5
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14 13 -8 45.48 13.18
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14 13 -8 62.06 15.24
14 13 -7 134.68 21.66
14 13 -7 138.42 23.72
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-14 13 7 114.87 22.96
14 13 -7 134.94 21.25
14 13 -6 28.5 12.19
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-14 13 6 36.05 15.46
14 13 -6 35.56 13.16
14 13 -5 89.13 19.78
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14 13 -5 83.04 18.41
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14 13 -4 56.47 16.36
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14 13 -3 97.51 19.49
14 13 -2 56.8 15.15
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14 13 -2 53.98 15.4
14 13 -1 94.95 19.71
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14 13 -1 91.08 20.41
14 13 0 36.54 12.51
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14 13 0 42.41 14.82
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14 13 1 55.89 17.42
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14 13 1 124.57 22.84
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14 13 2 47.83 15.9
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14 13 2 40.78 15.29
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14 13 3 99.64 20.87
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14 13 3 87.08 21.53
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14 13 4 57.22 17.63
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14 13 5 81.63 20.31
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14 13 6 46.24 15.72
14 13 7 83.15 21.53
14 14 -11 -8.41 10.2
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14 14 -11 12.19 11.64
14 14 -10 43.39 13.93
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14 14 -10 41.43 13.38
14 14 -9 8.81 10.79
14 14 -9 -1.31 6.72
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14 14 -8 87.52 19.2
14 14 -8 94.99 19.23
14 14 -8 62.75 16.57
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14 14 -7 14.52 10.04
14 14 -7 13.93 11.22
14 14 -7 0.95 7.85
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14 14 -6 67.91 17.47
14 14 -6 48.94 15.8
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14 14 -5 0.24 7.65
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14 14 -1 2.76 7.79
14 14 -1 -1.95 7.08
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14 14 0 9.74 8.55
14 14 0 13.67 9.24
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14 14 1 -9.33 10.35
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14 14 3 11.45 9.05
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14 15 -8 24.23 12.99
14 15 -7 209.15 27.95
14 15 -7 139.28 23.93
14 15 -6 0.82 9.75
14 15 -5 190.39 27.01
14 15 -4 11.07 7.54
14 15 -3 160.03 26.03
14 15 -2 8.79 9.69
14 15 -1 140.07 24.66
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14 15 0 10.12 10.92
14 15 1 134.73 24.81
15 -13 -3 5.68 10.07
15 -13 -2 56.75 17.49
15 -13 -1 -1.68 8.91
15 -13 0 58.03 16.47
15 -13 0 63.09 16.46
15 -13 1 -6.54 8.25
15 -12 -10 207.69 27.94
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-15 -12 9 131.51 24.82
15 -12 -9 174.95 26.03
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15 -12 -8 191.7 28.95
15 -12 -8 147.14 24.43
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15 -12 -7 88.27 21.14
15 -12 -7 94.83 19.93
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15 -12 -6 115.83 23.07
15 -12 -6 127.88 22.36
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15 -12 -5 100.12 20.81
15 -12 -5 107.05 20.46
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15 -12 -4 128.45 23.02
15 -12 -4 139.03 23.77
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15 -12 -3 79.76 18.09
15 -12 -3 110.41 20.68
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15 -12 -2 90.86 20.94
15 -12 -2 102.22 19.76
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15 -12 -1 77.66 19.96
15 -12 -1 69.7 18.05
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15 -12 0 105.5 20.49
15 -12 0 104.14 22.44
15 -12 1 72.11 17
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15 -12 1 74.87 17.66
15 -12 1 87.18 19.98
15 -12 2 54.58 15.19
15 -12 2 80.98 18.84
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15 -12 3 44.01 13.91
15 -12 3 72.31 16.84
15 -12 4 35.74 13.31
15 -12 4 24.71 11.22
15 -11 -13 21.91 11.65
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15 -11 -11 9.44 8.55
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15 -11 -11 1.31 8.53
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15 -11 -10 22.04 11.13
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15 -11 -10 21.02 11.38
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15 -11 -9 38.87 13.27
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15 -11 -9 44.53 16.46
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15 -11 -8 0.53 7.86
15 -11 -8 7.59 8.02
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15 -11 -7 59.38 17.72
15 -11 -7 42.77 14.56
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15 -11 -6 3.18 10.37
15 -11 -6 -2.05 8.52
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15 -11 -5 39.15 14.59
15 -11 -5 37.97 13.81
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15 -11 -4 11.25 12.64
15 -11 -4 1.17 7.11
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15 -11 -3 46.56 15.46
15 -11 -3 33.23 12.31
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15 -11 -2 8.12 8.61
15 -11 -2 4.82 7.5
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15 -11 -1 48.32 15.04
15 -11 -1 31.08 12.21
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15 -11 0 12.83 7.85
15 -11 0 14.07 10.69
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15 -11 1 46.27 14.78
15 -11 1 30.64 12.12
15 -11 2 22.96 10.88
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15 -11 2 20.9 11.43
15 -11 2 30.58 11.03
15 -11 3 28.75 12.17
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15 -11 3 45.09 14.77
15 -11 3 38.57 13.93
15 -11 4 25.44 10.83
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15 -11 4 36.52 11.33
15 -11 4 45.96 15.18
15 -11 5 -7.5 10.31
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15 -10 -14 182.47 25.08
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15 -10 -13 42.02 15.08
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15 -10 -13 45.67 14.41
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15 -10 -12 219.81 29.46
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15 -10 -12 147.63 22.62
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15 -10 -11 15.02 8.28
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15 -10 -11 32.4 11.81
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15 -10 -10 210.04 29.23
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15 -10 -10 274.02 31.61
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15 -10 -9 5.09 9.82
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15 -10 -9 -4.14 10.32
15 -10 -8 213.09 28.33
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15 -10 -8 184.75 28.08
15 -10 -8 237.54 28.57
15 -10 -7 30.14 12.8
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15 -10 -7 34.51 12.56
15 -10 -7 60.18 17.02
15 -10 -6 248.19 30.04
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15 -10 -6 273.03 33.11
15 -10 -6 258.47 30.12
15 -10 -5 33.16 13.35
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15 -10 -5 26.36 9.64
15 -10 -5 16.86 10.4
15 -10 -4 252.15 30.26
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15 -10 -4 258.96 30.99
15 -10 -4 354.38 36.91
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15 0 -13 464.31 40.01
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15 0 8 -1.84 8.11
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15 1 -3 11.21 9.21
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15 1 -1 4.06 5.12
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15 1 2 77.71 14.41
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15 5 -8 4.55 7
15 5 -7 64.73 17.72
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15 5 -6 -5.97 8.33
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-17 6 4 86.89 24.1
17 6 -3 12.87 8.43
17 6 -3 38.13 13.9
-17 6 3 17.73 11.97
-17 6 3 25.89 13.57
17 6 -2 32.96 11.34
-17 6 2 92.21 24.59
-17 6 2 60.2 21.41
-17 6 1 31.86 17.31
-17 6 1 16.06 12.07
17 6 -1 49.22 14.64
-17 6 0 44.01 19.67
-17 6 0 49.28 17.29
17 6 0 58.4 16.33
-17 6 -1 58.97 21.64
-17 6 -1 109.63 25.63
17 6 1 112.68 20.84
-17 6 -2 116.82 25.48
17 6 2 84.85 18.22
-17 6 -3 69.45 19.61
17 6 3 35.54 13.22
17 6 4 58.76 15.18
17 6 4 62.07 17.57
-17 6 -4 69.35 20.03
17 6 5 37.33 15.46
-17 7 12 -0.49 9.51
-17 7 11 70.83 18.45
17 7 -11 81.79 19.86
-17 7 10 -2.64 9.81
17 7 -10 -3.6 9.4
17 7 -9 117.01 23.9
17 7 -9 122.76 21.53
17 7 -8 20.2 10.84
17 7 -8 19.3 11.31
-17 7 8 26.28 14.52
-17 7 8 -3.39 12.77
17 7 -7 97.42 20.54
-17 7 7 93.49 23.22
-17 7 7 92.07 20.95
17 7 -6 11.68 9.95
-17 7 6 40 18.03
-17 7 6 18.71 14.48
17 7 -5 67.43 18.46
-17 7 5 50.42 17.1
-17 7 5 78.53 21.09
17 7 -5 109.32 20.68
17 7 -4 2.12 8.87
-17 7 4 -9.45 13.42
-17 7 4 8.65 13.33
17 7 -4 7.78 7.87
-17 7 3 119.35 28.57
-17 7 3 123.24 28.31
17 7 -3 67.66 16.29
-17 7 2 -13.43 14.03
-17 7 2 -5.29 11.09
-17 7 1 44.45 19
-17 7 1 59.07 20.31
-17 7 0 -21.26 20.81
-17 7 0 -11.37 9.83
-17 7 -1 34.53 18.51
-17 7 -1 23.66 12.16
-17 7 -2 -6.47 11.16
-17 7 -2 15.06 14.74
17 7 4 1.45 9.29
17 8 -10 88.36 19.03
17 8 -9 11.87 10.33
17 8 -8 87.85 18.43
17 8 -8 100.71 21.53
17 8 -7 2.01 9.17
17 8 -6 70.01 17.65
17 8 -5 -2.55 10.78
17 8 -4 44.33 13.5
17 8 -4 31.15 14.84
17 9 -8 3.57 8.45
17 9 -7 94.26 20.4
17 9 -6 6.92 8.59
17 9 -5 66.7 19.69
18 -5 -3 47.87 15.45
18 -5 -2 36.99 13.97
18 -5 -1 6.23 9.91
18 -4 -6 124.91 22.93
18 -4 -5 67.86 17.55
18 -4 -4 102.1 20.34
18 -4 -3 67.59 17.12
18 -4 -2 92.05 19.91
18 -4 -1 76.6 17.8
18 -3 -7 70.85 18.36
18 -3 -6 38.95 15.63
18 -3 -5 93.13 20.36
18 -3 -5 76.61 17.36
18 -3 -4 62.34 15.54
18 -3 -4 31.06 12.88
18 -3 -3 54.16 15.02
18 -3 -3 69.16 18.24
18 -3 -2 100.77 20.14
18 -3 -2 88.99 18.04
18 -3 -1 26.48 11.45
18 -3 -1 36.07 12.42
18 -2 -8 85.23 19.54
-18 -2 8 147.26 27.07
18 -2 -7 42.47 15.15
-18 -2 7 5.17 10.11
18 -2 -6 55.43 16.3
18 -2 -6 73.42 17.74
-18 -2 5 32.04 17.68
18 -2 -5 44.39 13.47
18 -2 -5 10.17 8.56
-18 -2 4 87.25 25.5
18 -2 -4 71.35 18.46
18 -2 -4 65.21 16.3
-18 -2 3 46.44 20.04
18 -2 -3 46.46 13.44
18 -2 -3 52.12 14.41
-18 -2 2 95.58 25.84
18 -2 -2 104.37 20.05
18 -2 -2 98.35 19.55
18 -2 -1 32.94 12.04
18 -2 -1 12.1 8.38
18 -2 0 96.09 18.62
18 -2 1 27.16 10.55
-18 -1 9 71.82 20.18
18 -1 -8 -3.82 7.38
-18 -1 8 -14.28 10.8
18 -1 -7 109.87 21.54
-18 -1 7 93.61 21.09
-18 -1 7 76.64 22.29
18 -1 -7 93.53 19
18 -1 -6 19.77 12.86
-18 -1 6 10.31 10
-18 -1 6 -3.03 11.92
18 -1 -6 26.93 11.24
-18 -1 5 108.04 28.6
18 -1 -5 134.9 23.44
18 -1 -5 167.95 25.02
-18 -1 4 0.65 16.38
18 -1 -4 10.05 9.18
18 -1 -4 17.98 12.41
-18 -1 3 133.25 30.25
18 -1 -3 201.32 27.3
18 -1 -3 138.83 22.89
-18 -1 2 6.76 13.21
18 -1 -2 19.94 12.01
18 -1 -2 16.49 11.54
-18 -1 1 124.55 28.75
18 -1 -1 120.15 21.28
18 -1 0 0.98 7.23
18 -1 1 76.6 17.7
18 -1 2 24.37 10.13
-18 0 9 0.89 10.42
18 0 -8 32.04 13.63
18 0 -8 48.01 14.72
-18 0 8 31.39 15.26
18 0 -7 14.66 10.81
-18 0 7 -14.4 12.74
-18 0 7 -12.11 12.32
18 0 -7 7.35 8.09
18 0 -6 42.19 15.22
-18 0 6 32.81 13.28
-18 0 6 49.12 19.42
18 0 -6 31.58 12.2
-18 0 5 -14.8 15.02
18 0 -5 9.05 10.08
18 0 -5 -1.28 8.52
-18 0 4 99.71 25.71
18 0 -4 89.27 19.93
18 0 -4 90.62 18.41
-18 0 3 6.22 10.25
18 0 -3 -13.63 11.04
18 0 -3 1.53 8.35
-18 0 2 84.52 25.9
18 0 -2 92.15 17.9
18 0 -2 104.02 20.46
-18 0 1 3.76 12.83
18 0 -1 -13.14 9.19
-18 0 0 117.81 28.26
18 0 0 113.53 20.37
18 0 1 6.7 7.05
18 0 2 136.61 21.43
18 0 3 11.54 9.82
-18 1 9 103.55 22.62
18 1 -8 -17.92 14.41
18 1 -8 2.75 9.21
-18 1 8 17.16 12.5
18 1 -7 123.41 22.67
18 1 -7 107.62 22.01
-18 1 7 76.77 22.94
-18 1 7 69.58 17.87
18 1 -6 14.35 9.3
-18 1 6 18.93 12.19
-18 1 6 1.42 10.5
18 1 -6 37.9 14.68
18 1 -5 100.47 20.48
-18 1 5 85.19 19.23
-18 1 5 66.51 21.26
18 1 -4 34 15.44
18 1 -4 15.1 9.67
-18 1 3 123.42 29.09
18 1 -3 74.83 17.37
18 1 -3 141.87 22.44
-18 1 2 19.33 15.62
18 1 -2 1.89 8.36
18 1 -2 6.54 9.31
-18 1 1 79.45 22.3
18 1 -1 83.94 18.84
18 1 0 -0.42 7.17
18 1 1 62.21 14.1
18 1 2 36.67 11.83
-18 2 10 83.31 22.74
-18 2 9 30.67 13.7
18 2 -8 104.56 20.68
-18 2 8 103.92 23.16
18 2 -7 34.05 11.23
18 2 -7 10.08 7.89
-18 2 7 31.96 13.34
18 2 -6 94.55 20.04
18 2 -6 58.63 16.9
-18 2 6 54.52 20.39
-18 2 6 50.99 16.75
18 2 -5 21.91 8.72
-18 2 5 33.46 13.74
-18 2 5 31.44 19.66
18 2 -5 10.59 8.72
18 2 -4 54.98 16.51
-18 2 4 56.03 20.41
18 2 -4 81.67 18.71
18 2 -3 43.88 14.43
18 2 -3 51.68 15.73
-18 2 3 14.49 14.1
18 2 -2 105.06 19.49
-18 2 2 76.12 23.09
18 2 -1 42.99 13.49
18 2 0 101.57 21.39
18 2 0 85.79 17.53
18 2 1 62.21 17.58
18 2 1 48.94 14.08
-18 3 9 82.41 20.47
18 3 -8 24.25 13.09
-18 3 8 33.8 16.28
18 3 -7 79.05 18.36
18 3 -7 57.1 15.91
-18 3 7 63.84 18.26
18 3 -6 16.5 11.98
18 3 -6 12.62 7.81
-18 3 6 16.91 12.49
18 3 -5 63.47 18.73
18 3 -5 64 16.6
18 3 -4 64.65 17.76
18 3 -4 72.86 16.85
18 3 -3 44.78 13.03
18 3 -3 62.08 15.49
18 3 -2 125.65 21.79
18 3 -1 34.56 13.39
18 3 0 119.08 22.43
18 3 0 71.43 16.05
18 3 1 45.39 14.6
-18 4 9 24.5 13.07
-18 4 8 93.68 22.33
18 4 -7 62.81 17.12
-18 4 7 82.37 20.61
18 4 -6 132.12 24.62
18 4 -6 83.18 18.36
18 4 -5 71.16 18
18 4 -5 93.02 20.32
18 4 -4 83.32 19.15
18 4 -4 83.75 18.1
18 4 -3 80.21 18.34
18 4 -2 70.78 16.15
18 4 -1 120.68 22.22
18 4 -1 123.3 21.18
18 4 0 40.92 13.73
-18 5 9 22.77 15.08
18 5 -6 31.63 14
18 5 -5 41.93 13.86
18 5 -5 67.72 18.04
18 5 -4 34.72 12.21
18 5 -4 54.25 15.91
18 5 -3 42.86 14.56
18 5 -2 79.56 17.89
18 5 -1 33.83 13.18
18 5 0 37.88 13.75
18 6 -5 115.48 22.39
18 6 -4 43.54 14.56
18 6 -3 129.47 22.52
_iucr_refine_fcf_details
;
data_Os_PBE_CCDC1
_computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)'
_shelx_refln_list_code 4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x+1/2,y+1/2,-z+1/2
3 -x,-y,-z
4 x-1/2,-y-1/2,z-1/2
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/n 1'
_space_group_name_Hall '-P 2ybc (x-z,y,z)'
_symmetry_space_group_name_H-M 'P 1 21/n 1'
_symmetry_space_group_name_Hall '-P 2ybc (x-z,y,z)'
_symmetry_Int_Tables_number 14
_cell_length_a 10.8918(1)
_cell_length_b 13.7619(1)
_cell_length_c 17.0714(2)
_cell_angle_alpha 90
_cell_angle_beta 98.563(1)
_cell_angle_gamma 90
_cell_volume 2530.34(4)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_weight
_refln_observed_status
-15 0 -1 3613.800 4014.860 216.831 2.566 o
-15 0 1 4379.540 4365.920 312.110 1.250 o
-15 0 3 4918.040 5444.870 267.095 1.695 o
-15 0 5 6583.630 6605.820 397.790 0.770 o
-15 0 7 5713.680 5463.730 279.606 1.546 o
-15 0 9 6995.450 6782.470 450.614 0.601 o
-15 1 -2 1281.610 1267.860 86.212 15.872 o
-15 1 -1 6.744 -1.753 35.145 99.578 o
-15 1 0 2183.670 2254.610 115.155 8.908 o
-15 1 1 27.085 49.734 42.820 66.822 o
-15 1 2 1998.770 2085.720 116.540 8.734 o
-15 1 3 82.517 76.813 43.060 65.671 o
-15 1 4 2566.580 2831.220 138.872 6.168 o
-15 1 5 25.848 46.597 44.762 61.188 o
-15 1 6 3605.110 3754.180 161.293 4.569 o
-15 1 7 11.815 -49.098 47.482 54.556 o
-15 1 8 3144.790 3137.880 147.869 5.432 o
-15 1 9 2.337 46.327 39.459 78.850 o
-15 2 -2 60.857 103.347 45.699 58.418 o
-15 2 -1 3328.010 3317.230 140.031 6.019 o
-15 2 0 236.124 343.189 56.161 38.199 o
-15 2 1 5031.010 5154.600 191.304 3.249 o
-15 2 2 293.226 307.092 61.502 31.910 o
-15 2 3 6554.800 6531.090 208.299 2.732 o
-15 2 4 301.056 363.574 61.403 31.961 o
-15 2 5 3766.180 3896.240 164.063 4.415 o
-15 2 6 1187.670 1280.150 96.124 12.893 o
-15 2 7 4539.100 4509.550 176.769 3.800 o
-15 2 8 1789.340 1886.520 115.046 8.988 o
-15 2 9 4721.730 4629.190 180.868 3.631 o
-15 3 -1 36.274 72.491 63.750 30.200 o
-15 3 0 1357.310 1485.650 103.498 11.124 o
-15 3 1 272.062 247.949 61.211 32.281 o
-15 3 2 1022.160 1041.420 85.308 16.331 o
-15 3 3 218.424 251.003 48.638 50.793 o
-15 3 4 207.828 146.415 42.181 67.396 o
-15 3 5 323.568 298.546 53.918 41.215 o
-15 3 6 241.669 239.419 45.827 56.964 o
-15 3 7 720.756 674.858 71.987 22.964 o
-15 3 8 328.374 242.729 58.752 34.898 o
-15 4 0 1269.780 1318.930 94.545 13.288 o
-15 4 1 3286.350 3209.820 159.134 4.707 o
-15 4 2 1948.380 1983.920 118.123 8.520 o
-15 4 3 2852.850 3063.830 146.247 5.563 o
-15 4 4 2993.230 3125.210 205.899 2.852 o
-15 4 5 3503.560 3418.790 145.662 5.571 o
-15 4 6 2104.430 2137.890 118.040 8.508 o
-15 4 7 2609.000 2604.020 130.702 6.938 o
-15 5 2 201.875 137.610 52.004 44.765 o
-15 5 3 1504.930 1524.590 107.136 10.379 o
-15 5 4 167.085 133.756 56.628 37.923 o
-15 5 5 1256.470 1274.700 86.802 15.673 o
-14 0 -6 127.429 163.631 54.328 41.217 o
-14 0 -4 42.482 33.659 46.828 55.886 o
-14 0 -2 268.742 374.170 59.995 33.486 o
-14 0 0 478.419 498.524 74.844 21.505 o
-14 0 2 1034.410 1110.980 102.602 11.403 o
-14 0 4 1627.360 1757.530 146.717 5.609 o
-14 0 6 2371.700 2352.460 149.791 5.344 o
-14 0 8 3454.250 3323.150 203.967 2.899 o
-14 0 10 3171.290 3458.300 211.018 2.714 o
-14 0 12 1380.740 1382.350 143.524 5.876 o
-14 1 -7 7543.620 7494.510 159.459 4.502 o
-14 1 -6 243.271 197.031 39.990 74.302 o
-14 1 -5 8918.410 8777.270 182.374 3.465 o
-14 1 -4 48.845 186.660 39.804 76.543 o
-14 1 -3 10572.900 10409.700 207.069 2.702 o
-14 1 -2 133.452 116.853 37.653 84.893 o
-14 1 -1 8981.920 8918.020 208.991 2.678 o
-14 1 0 284.409 257.368 45.216 58.228 o
-14 1 1 6484.620 6356.310 165.931 4.220 o
-14 1 2 22.229 111.680 38.184 83.680 o
-14 1 3 8321.270 8426.490 227.204 2.290 o
-14 1 4 65.351 196.073 48.365 52.016 o
-14 1 5 8547.490 8443.390 227.846 2.276 o
-14 1 6 84.205 85.580 39.404 78.209 o
-14 1 7 8673.430 8186.190 210.320 2.653 o
-14 1 8 24.957 113.137 45.349 59.464 o
-14 1 9 8699.100 8679.120 237.253 2.104 o
-14 1 10 244.731 297.140 52.467 43.668 o
-14 1 11 7484.310 7392.550 207.610 2.736 o
-14 1 12 364.638 423.748 60.465 32.800 o
-14 1 13 7766.070 7551.830 229.292 2.257 o
-14 2 -6 656.998 595.109 47.841 50.250 o
-14 2 -5 59.349 47.158 30.740 128.376 o
-14 2 -4 515.271 491.799 43.744 60.287 o
-14 2 -3 73.994 132.881 34.166 103.366 o
-14 2 -2 260.792 216.592 33.657 103.014 o
-14 2 -1 36.141 43.161 34.420 103.066 o
-14 2 0 1241.570 1447.410 83.070 17.021 o
-14 2 1 6.842 28.291 31.798 121.332 o
-14 2 2 1675.490 1654.540 87.754 15.154 o
-14 2 3 292.511 265.001 48.733 50.318 o
-14 2 4 791.125 694.865 65.167 27.733 o
-14 2 5 42.502 2.273 36.537 91.715 o
-14 2 6 627.342 623.281 68.882 25.108 o
-14 2 7 172.471 180.151 45.602 57.965 o
-14 2 8 618.148 512.595 59.772 33.090 o
-14 2 9 502.608 556.423 60.731 32.226 o
-14 2 10 952.144 775.549 67.128 26.013 o
-14 2 11 234.068 173.900 52.854 43.230 o
-14 2 12 1565.200 1575.080 97.534 12.422 o
-14 2 13 84.819 103.745 43.643 63.859 o
-14 3 -6 1468.760 1568.380 81.188 17.657 o
-14 3 -5 3270.120 3161.880 113.353 9.006 o
-14 3 -4 2101.580 2239.680 90.479 14.100 o
-14 3 -3 4921.640 4897.260 137.235 6.130 o
-14 3 -2 1433.850 1514.950 76.527 19.771 o
-14 3 -1 4402.270 4413.250 128.010 7.032 o
-14 3 0 677.465 738.429 71.166 23.488 o
-14 3 1 6251.940 6028.860 156.129 4.744 o
-14 3 2 299.528 336.966 47.578 52.550 o
-14 3 3 4765.350 4812.220 168.598 4.153 o
-14 3 4 349.570 326.448 50.142 47.334 o
-14 3 5 5566.850 5681.610 179.581 3.656 o
-14 3 6 1085.820 1134.690 82.564 17.349 o
-14 3 7 6362.970 6238.820 190.873 3.236 o
-14 3 8 1840.530 2064.260 110.590 9.682 o
-14 3 9 4155.390 4140.030 138.254 6.104 o
-14 3 10 2328.010 2418.570 107.336 10.158 o
-14 3 11 3461.470 3657.290 138.016 6.173 o
-14 3 12 3746.110 3681.170 140.788 5.928 o
-14 3 13 5947.750 5918.170 178.317 3.696 o
-14 4 -6 748.134 801.179 58.974 33.526 o
-14 4 -5 500.230 388.782 53.248 41.695 o
-14 4 -4 1249.920 1330.380 70.561 23.218 o
-14 4 -3 123.819 123.641 32.285 114.663 o
-14 4 -2 849.144 982.255 62.767 29.551 o
-14 4 -1 206.495 186.928 32.601 110.567 o
-14 4 0 702.998 655.007 54.780 38.776 o
-14 4 1 183.685 247.157 36.748 87.792 o
-14 4 2 919.002 959.218 63.945 28.463 o
-14 4 3 110.655 172.303 40.709 72.825 o
-14 4 4 163.007 185.163 36.280 90.561 o
-14 4 5 674.626 650.498 60.358 32.295 o
-14 4 6 12.014 5.277 35.044 100.045 o
-14 4 7 132.595 134.114 42.294 67.550 o
-14 4 8 8.910 53.364 39.806 77.403 o
-14 4 9 157.387 122.887 42.575 66.559 o
-14 4 10 25.674 74.916 38.153 83.960 o
-14 4 11 356.198 348.336 50.602 46.455 o
-14 4 12 14.979 29.085 34.518 102.893 o
-14 5 -5 645.466 518.287 50.719 45.176 o
-14 5 -4 2688.120 2678.460 105.777 10.371 o
-14 5 -3 526.356 613.218 51.394 44.252 o
-14 5 -2 2583.080 2553.800 96.372 12.384 o
-14 5 -1 1553.220 1499.220 73.524 21.244 o
-14 5 0 2438.080 2378.600 110.479 9.603 o
-14 5 1 1546.710 1442.650 71.992 22.117 o
-14 5 2 3353.930 3332.830 119.069 8.192 o
-14 5 3 3800.220 4007.240 140.592 5.933 o
-14 5 4 5733.170 5647.830 168.016 4.148 o
-14 5 5 3463.060 3329.750 129.328 6.997 o
-14 5 6 6398.210 6417.360 180.537 3.597 o
-14 5 7 2582.060 2750.240 122.098 7.903 o
-14 5 8 4692.390 4833.380 154.127 4.932 o
-14 5 9 1744.970 1809.150 94.972 13.003 o
-14 5 10 4208.940 4427.930 158.744 4.683 o
-14 5 11 1365.110 1342.790 78.416 18.960 o
-14 6 -4 121.956 101.546 33.450 107.232 o
-14 6 -3 678.988 754.638 60.097 32.482 o
-14 6 -2 426.896 446.319 46.367 54.483 o
-14 6 -1 1062.730 1035.250 72.134 22.505 o
-14 6 0 533.996 481.373 45.810 55.222 o
-14 6 1 625.951 665.361 58.132 34.765 o
-14 6 2 101.301 142.625 38.339 82.127 o
-14 6 3 778.725 833.069 72.403 22.614 o
-14 6 4 30.533 2.822 41.298 71.955 o
-14 6 5 204.399 187.491 65.655 28.230 o
-14 6 6 94.493 55.944 35.014 98.752 o
-14 6 7 258.223 202.083 47.349 53.466 o
-14 6 8 110.600 87.096 35.776 94.268 o
-14 6 9 347.257 403.694 50.990 45.719 o
-14 6 10 342.353 305.980 59.983 33.439 o
-14 7 -2 7010.370 6970.580 173.147 3.876 o
-14 7 -1 131.789 179.036 39.681 76.375 o
-14 7 0 9435.620 9390.790 189.253 3.221 o
-14 7 1 467.573 475.011 51.722 44.058 o
-14 7 2 10193.600 10466.000 288.988 1.429 o
-14 7 3 433.157 518.925 64.155 29.085 o
-14 7 4 9770.920 9565.520 237.017 2.099 o
-14 7 5 699.227 814.380 77.027 20.116 o
-14 7 6 8543.100 8607.710 213.853 2.569 o
-14 7 7 537.234 478.480 55.621 38.176 o
-14 7 8 7397.280 7291.860 204.875 2.807 o
-14 7 9 478.618 514.981 54.892 39.239 o
-14 8 0 116.147 67.683 33.788 105.494 o
-14 8 1 1106.120 1142.220 71.646 22.729 o
-14 8 2 180.241 170.176 47.303 53.939 o
-14 8 3 1506.440 1402.080 94.397 13.261 o
-14 8 4 194.372 176.518 47.109 54.305 o
-14 8 5 1143.380 1205.210 91.831 14.105 o
-14 8 6 71.168 20.829 44.101 62.852 o
-14 8 7 279.464 270.018 44.924 58.956 o
-13 0 -9 5560.780 5615.890 187.131 3.379 o
-13 0 -7 9422.240 9410.170 235.958 2.120 o
-13 0 -5 9124.350 9084.180 223.922 2.346 o
-13 0 -3 13543.100 13526.300 262.741 1.698 o
-13 0 -1 15648.900 15711.200 401.711 0.744 o
-13 0 1 16010.800 16014.900 367.334 0.885 o
-13 0 3 13065.400 12777.800 287.363 1.433 o
-13 0 5 10376.500 10535.200 340.398 1.039 o
-13 0 7 10315.100 9775.060 333.829 1.080 o
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7 4 7 6775.080 6698.450 77.546 15.920 o
7 4 8 9291.060 9293.450 103.557 9.399 o
7 4 9 10418.100 10515.200 113.541 7.910 o
7 4 10 5269.940 5224.300 82.856 15.010 o
7 4 11 5174.940 5198.360 83.995 14.702 o
7 4 12 7146.600 7145.490 120.398 7.545 o
7 4 13 7268.120 7298.190 140.230 5.721 o
7 4 14 4484.780 4521.050 108.960 9.459 o
7 4 15 6130.730 6165.320 138.311 5.949 o
7 4 16 3955.090 4034.390 114.705 8.689 o
7 4 17 4632.340 4640.030 126.304 7.186 o
7 4 18 2082.390 2235.200 100.109 11.655 o
7 4 19 4253.410 4248.540 133.427 6.519 o
7 5 7 2506.420 2497.440 48.701 40.941 o
7 5 8 2185.310 2187.430 46.665 45.060 o
7 5 9 3524.290 3335.230 63.916 24.799 o
7 5 10 1090.200 1036.340 37.416 73.645 o
7 5 11 975.771 955.428 38.140 72.412 o
7 5 12 1385.380 1371.940 48.675 45.273 o
7 5 13 1202.360 1194.680 59.885 31.645 o
7 5 14 750.464 790.961 47.856 49.567 o
7 5 15 739.298 798.571 50.642 44.656 o
7 5 16 580.718 551.632 45.726 55.071 o
7 5 17 1135.110 1129.160 60.919 30.790 o
7 5 18 124.736 107.524 30.928 124.772 o
7 5 19 594.848 607.353 51.309 44.215 o
7 6 7 589.437 629.955 35.855 85.593 o
7 6 8 9895.240 9833.880 126.225 6.670 o
7 6 9 1368.750 1456.550 48.107 46.132 o
7 6 10 8032.850 8040.800 113.949 8.189 o
7 6 11 2616.300 2684.860 66.057 24.459 o
7 6 12 6074.040 6040.300 105.356 9.737 o
7 6 13 2624.750 2674.150 80.444 17.238 o
7 6 14 4548.260 4722.120 120.974 7.789 o
7 6 15 2896.980 2878.470 93.209 13.067 o
7 6 16 5241.480 5242.800 129.996 6.752 o
7 6 17 2073.830 2066.920 83.538 16.406 o
7 6 18 4685.380 4771.100 125.835 7.228 o
7 7 7 9484.940 9574.980 121.464 7.164 o
7 7 8 288.934 330.506 24.662 179.755 o
7 7 9 6868.270 6911.640 101.881 10.146 o
7 7 10 518.015 611.818 35.117 89.709 o
7 7 11 5467.350 5491.100 97.097 11.377 o
7 7 12 109.178 129.125 20.757 267.521 o
7 7 13 5077.860 5166.720 114.230 8.580 o
7 7 14 212.776 250.640 31.596 116.651 o
7 7 15 3868.270 3929.260 110.823 9.277 o
7 7 16 38.104 -3.422 30.738 129.412 o
7 7 17 867.333 863.630 59.617 32.623 o
7 7 18 49.949 53.573 37.421 87.106 o
7 8 7 57.656 25.778 16.863 415.513 o
7 8 8 5258.430 5390.260 90.157 12.990 o
7 8 9 28.548 53.703 17.006 412.345 o
7 8 10 9483.180 9422.070 142.623 5.409 o
7 8 11 146.649 144.072 21.677 242.921 o
7 8 12 6683.930 6691.950 109.434 9.000 o
7 8 13 17.571 44.439 24.787 198.199 o
7 8 14 5618.020 5524.100 124.474 7.278 o
7 8 15 330.966 353.121 39.671 74.187 o
7 8 16 3721.000 3942.270 115.209 8.647 o
7 8 17 1.054 -14.192 31.097 127.283 o
7 9 7 6563.770 6413.300 97.475 11.031 o
7 9 8 47.089 40.150 17.328 395.112 o
7 9 9 7187.550 7049.320 108.155 9.107 o
7 9 10 459.135 505.915 32.250 106.105 o
7 9 11 7315.330 7138.290 116.787 7.948 o
7 9 12 159.930 140.080 22.153 232.475 o
7 9 13 3810.940 3853.900 99.183 11.389 o
7 9 14 31.538 76.946 37.168 88.357 o
7 9 15 2550.940 2691.410 90.965 13.780 o
7 9 16 88.545 86.361 30.875 126.196 o
7 10 7 491.016 508.056 29.551 123.224 o
7 10 8 9013.850 8924.030 121.373 7.231 o
7 10 9 72.173 68.842 19.233 317.359 o
7 10 10 6173.770 6154.720 108.619 9.209 o
7 10 11 948.095 957.632 44.752 54.869 o
7 10 12 5424.160 5584.160 106.698 9.634 o
7 10 13 1329.510 1363.560 59.611 31.620 o
7 10 14 4358.130 4423.690 124.277 7.435 o
7 10 15 1306.400 1357.090 66.634 25.779 o
7 10 16 4139.530 4215.870 167.998 4.204 o
7 11 7 2293.830 2306.180 66.304 24.725 o
7 11 8 447.004 446.530 31.442 111.741 o
7 11 9 1336.120 1294.730 50.854 42.142 o
7 11 10 157.258 173.116 27.036 159.444 o
7 11 11 578.839 607.143 40.850 67.727 o
7 11 12 278.955 215.733 30.465 123.923 o
7 11 13 998.615 1047.440 57.796 34.220 o
7 11 14 286.672 270.854 35.766 91.160 o
7 11 15 1095.510 1157.190 65.227 27.133 o
7 12 7 2136.330 2196.140 79.237 18.037 o
7 12 8 5708.080 5519.230 104.023 10.043 o
7 12 9 2712.180 2768.580 75.982 19.038 o
7 12 10 5910.690 5937.830 117.302 8.064 o
7 12 11 2507.310 2584.090 79.065 17.858 o
7 12 12 3499.560 3386.960 93.200 12.870 o
7 12 13 3336.200 3485.150 104.073 10.530 o
7 12 14 1730.120 1662.350 77.140 19.285 o
7 13 7 352.037 372.626 32.656 106.379 o
7 13 8 546.847 522.437 36.283 84.736 o
7 13 9 280.681 277.213 40.501 71.948 o
7 13 10 592.564 555.012 41.754 65.127 o
7 13 11 35.410 56.360 25.493 186.353 o
7 13 12 1236.100 1176.160 60.215 31.293 o
7 14 7 5990.920 5978.330 128.505 6.825 o
7 14 8 944.160 875.263 52.760 40.805 o
7 14 9 4433.170 4513.290 114.738 8.610 o
7 14 10 1301.400 1185.890 57.308 34.156 o
7 14 11 3577.280 3509.620 98.674 11.571 o
7 15 7 681.717 665.712 46.101 53.604 o
7 15 8 2144.470 2116.170 81.546 17.119 o
7 15 9 400.561 366.654 53.831 41.087 o
7 16 7 6215.070 6291.720 140.704 5.756 o
8 0 8 7967.600 7824.910 143.517 5.443 o
8 0 10 1079.760 1132.030 61.782 30.063 o
8 0 12 1304.370 1210.580 66.779 25.744 o
8 0 14 1263.030 1239.520 88.323 15.163 o
8 0 16 593.059 631.722 71.267 23.528 o
8 0 18 2150.410 2299.310 136.221 6.441 o
8 1 8 124.614 157.064 17.945 345.500 o
8 1 9 22752.500 22761.800 201.515 2.648 o
8 1 10 71.382 135.868 23.288 217.561 o
8 1 11 17564.700 17630.000 187.834 3.092 o
8 1 12 198.289 216.620 25.708 172.744 o
8 1 13 11759.200 12068.300 181.846 3.410 o
8 1 14 894.761 915.754 51.271 43.087 o
8 1 15 6160.240 6326.870 168.481 4.108 o
8 1 16 47.791 31.620 30.651 129.560 o
8 1 17 3296.380 3392.220 111.166 9.324 o
8 1 18 83.184 151.430 39.976 75.763 o
8 2 8 4326.440 4352.610 68.066 21.467 o
8 2 9 231.874 240.706 19.522 279.440 o
8 2 10 3041.100 2994.040 69.021 22.254 o
8 2 11 111.670 109.963 20.884 265.168 o
8 2 12 1638.190 1518.190 58.940 31.737 o
8 2 13 924.554 985.062 53.930 39.109 o
8 2 14 1690.730 1669.540 71.435 22.262 o
8 2 15 266.368 267.811 33.865 101.374 o
8 2 16 1548.550 1613.880 75.437 20.219 o
8 2 17 22.100 2.181 28.860 147.116 o
8 2 18 546.928 576.667 51.867 43.482 o
8 3 8 3576.200 3603.830 65.275 23.805 o
8 3 9 8496.680 8313.040 106.723 9.090 o
8 3 10 4887.080 4917.660 85.260 14.458 o
8 3 11 7246.480 7153.920 115.021 8.170 o
8 3 12 3402.250 3391.480 82.625 16.009 o
8 3 13 5520.540 5652.200 125.514 7.170 o
8 3 14 839.561 860.810 54.175 39.090 o
8 3 15 4425.140 4488.690 122.109 7.675 o
8 3 16 918.319 1040.480 62.578 29.601 o
8 3 17 2668.980 2683.970 103.619 10.784 o
8 3 18 506.079 619.719 55.058 38.845 o
8 4 8 350.024 352.669 22.768 202.738 o
8 4 9 1969.310 2091.790 52.544 37.640 o
8 4 10 901.275 919.473 39.346 69.241 o
8 4 11 23.628 12.543 18.028 372.979 o
8 4 12 1390.940 1444.860 52.674 39.311 o
8 4 13 24.939 36.140 30.367 132.460 o
8 4 14 595.335 590.819 43.551 60.138 o
8 4 15 21.491 0.733 28.805 147.711 o
8 4 16 408.851 402.920 41.493 67.466 o
8 4 17 33.953 3.560 34.088 105.399 o
8 4 18 493.647 476.515 47.958 50.797 o
8 5 8 7334.200 7563.200 110.851 8.683 o
8 5 9 872.315 836.613 36.033 81.188 o
8 5 10 5801.440 5774.320 94.043 11.931 o
8 5 11 1378.570 1371.660 52.130 40.149 o
8 5 12 5967.830 5916.840 111.014 8.896 o
8 5 13 1656.610 1662.680 66.157 25.662 o
8 5 14 5251.690 5427.620 133.354 6.434 o
8 5 15 1819.620 1852.590 78.245 18.691 o
8 5 16 3966.650 4006.160 116.604 8.428 o
8 5 17 2060.400 2125.130 87.099 15.172 o
8 6 8 708.248 721.264 35.323 86.200 o
8 6 9 1725.730 1798.350 55.349 35.102 o
8 6 10 453.069 430.379 28.642 131.927 o
8 6 11 2446.480 2487.640 65.949 24.753 o
8 6 12 258.951 222.457 25.705 170.225 o
8 6 13 1475.870 1460.700 69.634 23.576 o
8 6 14 37.714 86.643 29.439 139.846 o
8 6 15 2757.910 2780.480 98.713 11.785 o
8 6 16 8.848 23.845 30.724 129.929 o
8 6 17 758.412 616.268 60.206 32.355 o
8 7 8 10068.200 9987.970 134.926 5.927 o
8 7 9 181.200 167.479 22.310 226.949 o
8 7 10 9184.680 9225.380 133.538 6.100 o
8 7 11 44.385 53.731 20.152 294.428 o
8 7 12 6668.010 6720.510 121.238 7.506 o
8 7 13 204.663 181.287 32.003 114.622 o
8 7 14 4772.650 4716.150 127.020 7.098 o
8 7 15 181.746 184.693 35.870 92.360 o
8 7 16 3881.810 4026.460 123.571 7.567 o
8 8 8 11.352 2.342 19.274 329.515 o
8 8 9 3756.520 3795.480 84.920 15.070 o
8 8 10 3.838 21.616 21.431 266.595 o
8 8 11 3412.290 3564.710 84.890 15.225 o
8 8 12 32.714 44.260 21.758 255.049 o
8 8 13 3343.690 3115.740 105.434 10.305 o
8 8 14 115.648 125.573 36.146 92.101 o
8 8 15 1781.870 1752.840 80.781 17.650 o
8 8 16 8.775 17.249 34.233 104.784 o
8 9 8 7675.980 7641.050 122.813 7.226 o
8 9 9 13.834 26.306 23.429 222.428 o
8 9 10 6005.670 6040.490 114.958 8.348 o
8 9 11 91.761 99.314 23.930 206.380 o
8 9 12 6609.450 6513.840 124.408 7.177 o
8 9 13 45.910 101.204 29.534 138.553 o
8 9 14 5259.920 5095.160 134.984 6.299 o
8 9 15 164.219 189.190 39.982 74.962 o
8 10 8 72.947 71.048 22.837 228.041 o
8 10 9 3209.990 3158.450 96.766 12.100 o
8 10 10 63.342 111.963 24.183 203.491 o
8 10 11 2429.670 2430.400 76.365 19.092 o
8 10 12 2.266 -4.104 26.884 170.245 o
8 10 13 552.458 602.020 49.728 47.042 o
8 10 14 101.018 124.333 37.515 85.793 o
8 11 8 7644.360 7771.810 144.810 5.369 o
8 11 9 299.477 339.630 35.984 89.595 o
8 11 10 6910.880 6771.250 133.098 6.325 o
8 11 11 745.345 773.745 47.069 51.153 o
8 11 12 4360.400 4314.380 123.359 7.542 o
8 11 13 558.066 642.082 54.795 39.071 o
8 12 8 282.223 264.123 31.030 119.203 o
8 12 9 521.780 520.545 41.480 66.453 o
8 12 10 166.080 153.130 29.044 139.184 o
8 12 11 326.905 350.052 36.986 84.743 o
8 12 12 283.619 259.866 45.664 57.126 o
8 13 8 2054.460 1966.560 70.779 22.289 o
8 13 9 6426.760 6225.570 129.489 6.695 o
8 13 10 2392.970 2359.950 85.934 15.410 o
8 13 11 2916.360 3001.840 95.249 12.537 o
8 14 8 1294.900 1271.160 66.662 25.809 o
8 14 9 226.158 239.855 38.448 80.113 o
9 0 9 23660.500 24172.800 349.868 0.957 o
9 0 11 18930.600 18991.600 345.143 0.993 o
9 0 13 16783.200 17284.500 384.318 0.810 o
9 0 15 8025.700 8159.520 270.675 1.634 o
9 0 17 5336.750 5525.660 231.009 2.249 o
9 1 9 323.884 286.780 23.637 193.088 o
9 1 10 1259.700 1326.900 50.835 42.319 o
9 1 11 251.779 235.581 24.364 187.671 o
9 1 12 640.286 763.036 52.529 41.990 o
9 1 13 3.133 27.645 31.239 125.783 o
9 1 14 268.862 269.618 43.188 63.676 o
9 1 15 0.375 -39.075 37.722 86.514 o
9 1 16 23.737 60.562 38.320 83.319 o
9 1 17 3.996 -48.590 36.985 89.952 o
9 2 9 8592.980 8692.780 129.491 6.490 o
9 2 10 2766.210 2818.850 74.221 19.807 o
9 2 11 10113.400 10174.200 154.776 4.638 o
9 2 12 2124.940 2234.840 79.570 17.895 o
9 2 13 8118.130 7919.520 153.722 4.793 o
9 2 14 1175.680 1194.390 63.444 28.467 o
9 2 15 8049.480 8568.270 188.167 3.282 o
9 2 16 224.296 161.253 44.372 60.934 o
9 2 17 3994.340 4006.960 144.067 5.655 o
9 3 9 1200.700 1202.430 43.029 57.104 o
9 3 10 507.979 575.074 37.896 78.392 o
9 3 11 966.512 1004.760 48.979 46.508 o
9 3 12 707.039 748.285 49.621 46.547 o
9 3 13 13.915 25.076 26.490 174.330 o
9 3 14 684.285 720.160 51.197 44.006 o
9 3 15 8.028 12.018 28.524 150.874 o
9 3 16 315.556 342.479 47.152 53.399 o
9 3 17 189.189 128.815 36.365 90.173 o
9 4 9 3596.050 3731.770 82.089 16.064 o
9 4 10 3941.980 4157.380 89.911 13.523 o
9 4 11 2000.710 1934.980 62.924 27.595 o
9 4 12 3084.520 3214.680 100.908 11.216 o
9 4 13 1877.780 1919.590 77.253 19.093 o
9 4 14 1752.720 1704.710 75.601 19.999 o
9 4 15 1717.070 1806.070 79.904 18.031 o
9 4 16 1905.150 1978.560 84.600 16.100 o
9 5 9 789.581 736.070 38.636 72.923 o
9 5 10 464.206 458.947 33.845 97.505 o
9 5 11 584.961 576.408 36.054 85.061 o
9 5 12 122.202 117.671 26.313 170.287 o
9 5 13 775.343 729.141 47.503 50.268 o
9 5 14 101.801 115.304 33.215 108.931 o
9 5 15 10.612 19.271 30.522 131.662 o
9 5 16 370.355 359.219 46.231 55.202 o
9 6 9 159.676 170.546 26.226 168.837 o
9 6 10 6141.400 6010.330 113.095 8.583 o
9 6 11 113.440 93.244 24.573 195.152 o
9 6 12 7178.480 7109.760 144.299 5.436 o
9 6 13 112.628 92.662 30.081 132.130 o
9 6 14 5149.670 5282.880 132.510 6.520 o
9 6 15 358.835 263.490 45.088 58.187 o
9 6 16 2378.940 2319.210 93.645 13.142 o
9 7 9 118.168 97.216 22.736 225.862 o
9 7 10 6.042 -5.461 20.709 286.367 o
9 7 11 755.973 796.834 45.673 53.973 o
9 7 12 69.453 48.701 28.291 150.828 o
9 7 13 521.423 518.296 49.591 47.513 o
9 7 14 205.349 127.294 30.690 124.693 o
9 7 15 1120.070 1177.750 65.370 26.986 o
9 8 9 0.762 52.965 21.317 268.201 o
9 8 10 7859.780 7730.290 133.466 6.215 o
9 8 11 0.914 -10.558 26.527 174.910 o
9 8 12 6704.090 6854.170 153.522 4.868 o
9 8 13 216.757 220.426 35.529 93.442 o
9 8 14 6007.250 6186.130 172.661 3.926 o
9 9 9 260.686 233.597 27.273 152.450 o
9 9 10 85.363 110.362 25.947 176.633 o
9 9 11 626.128 730.052 43.124 60.734 o
9 9 12 14.381 20.734 29.796 138.019 o
9 9 13 484.955 458.298 48.999 48.825 o
9 9 14 0.089 41.097 33.177 111.488 o
9 10 9 74.993 103.524 25.810 179.052 o
9 10 10 7261.300 7138.820 138.890 5.826 o
9 10 11 57.970 89.294 27.370 160.622 o
9 10 12 5797.740 6019.320 156.457 4.740 o
9 10 13 21.917 50.646 34.864 100.622 o
9 11 9 1094.780 1058.840 55.158 37.117 o
9 11 10 35.842 24.630 25.893 181.425 o
9 11 11 693.431 698.950 48.401 48.877 o
9 11 12 7.502 43.048 33.109 111.806 o
9 12 9 1142.610 1088.550 59.491 32.193 o
9 12 10 2166.500 2227.600 83.246 16.448 o
9 13 9 778.973 783.631 50.564 44.694 o
10 0 10 640.568 663.192 57.332 35.672 o
10 0 12 443.106 467.825 54.420 40.024 o
10 0 14 144.544 122.561 52.405 44.267 o
10 0 16 6.560 32.493 54.576 41.278 o
10 1 10 587.337 668.257 44.104 58.602 o
10 1 11 8543.010 8638.940 146.155 5.228 o
10 1 12 285.928 368.243 43.127 63.482 o
10 1 13 7843.150 7754.480 165.733 4.179 o
10 1 14 331.494 376.598 47.751 51.990 o
10 1 15 7252.620 7581.990 183.517 3.462 o
10 1 16 145.120 101.154 40.523 73.490 o
10 2 10 389.675 369.754 33.972 98.400 o
10 2 11 1025.010 1093.040 59.092 32.765 o
10 2 12 62.005 41.411 31.744 120.501 o
10 2 13 360.326 350.857 42.586 64.658 o
10 2 14 40.689 24.980 43.485 64.795 o
10 2 15 27.628 40.297 35.291 98.211 o
10 3 10 1662.130 1707.070 68.436 24.098 o
10 3 11 5009.420 4955.640 120.885 7.751 o
10 3 12 1577.330 1640.260 79.130 18.466 o
10 3 13 3203.420 3375.480 115.510 8.688 o
10 3 14 1980.830 2168.510 94.399 13.056 o
10 3 15 3943.820 4210.410 136.907 6.228 o
10 4 10 19.008 43.415 22.415 241.713 o
10 4 11 266.210 205.417 32.288 111.429 o
10 4 12 36.650 49.100 33.534 108.476 o
10 4 13 355.286 373.160 43.399 62.335 o
10 4 14 139.530 162.225 44.884 59.999 o
10 4 15 28.042 44.447 32.261 117.329 o
10 5 10 5218.750 5270.110 107.699 9.520 o
10 5 11 1325.930 1349.890 55.359 36.180 o
10 5 12 4209.460 4234.320 112.470 8.972 o
10 5 13 420.883 434.078 47.156 52.804 o
10 5 14 3172.620 3505.720 117.424 8.419 o
10 5 15 298.510 300.610 40.070 73.219 o
10 6 10 188.173 151.385 30.258 128.227 o
10 6 11 48.362 106.154 25.925 178.615 o
10 6 12 203.941 174.386 33.100 107.543 o
10 6 13 16.890 1.742 30.459 132.267 o
10 6 14 249.922 173.834 34.112 100.869 o
10 7 10 7199.220 7190.130 163.252 4.322 o
10 7 11 303.455 383.242 36.414 87.339 o
10 7 12 6174.910 6315.620 145.363 5.420 o
10 7 13 144.490 189.552 37.376 85.647 o
10 7 14 5806.750 5815.110 141.506 5.725 o
10 8 10 108.308 110.399 31.846 118.173 o
10 8 11 502.986 600.279 42.896 62.312 o
10 8 12 32.798 34.336 29.682 138.405 o
10 8 13 10.224 18.867 32.112 119.005 o
10 9 10 8199.060 8198.170 151.532 4.914 o
10 9 11 4.693 7.008 26.625 173.329 o
10 9 12 5037.280 5046.130 137.514 6.097 o
10 10 10 1.765 -1.637 27.060 168.058 o
10 10 11 91.273 129.916 30.398 129.534 o
10 11 10 3325.640 3096.670 99.058 11.573 o
11 0 11 4230.870 4155.530 152.591 5.055 o
11 0 13 6671.090 7060.240 240.369 2.069 o
11 1 11 669.355 675.806 46.345 53.112 o
11 1 12 33.983 28.659 30.197 133.816 o
11 1 13 88.463 112.326 35.614 95.229 o
11 1 14 13.269 21.068 39.577 78.395 o
11 2 11 7894.650 7810.760 154.047 4.783 o
11 2 12 459.144 441.215 44.753 58.137 o
11 2 13 3880.320 3989.280 129.094 6.971 o
11 2 14 1284.320 1401.050 85.979 15.931 o
11 3 11 157.320 112.401 36.547 89.749 o
11 3 12 20.478 -18.039 34.432 103.536 o
11 3 13 406.464 325.394 42.349 65.154 o
11 3 14 15.390 7.564 35.822 95.694 o
11 4 11 4773.200 4979.820 123.438 7.475 o
11 4 12 3337.610 3507.330 120.035 8.062 o
11 4 13 2522.660 2521.320 101.872 11.173 o
11 5 11 57.195 20.061 26.904 167.454 o
11 5 12 154.506 117.958 35.594 94.483 o
11 5 13 3.343 63.021 33.302 110.421 o
11 6 11 2057.690 2057.020 79.097 18.162 o
11 6 12 4447.970 4785.660 138.318 6.067 o
11 7 11 662.392 828.181 58.286 34.397 o
11 7 12 8.740 16.367 32.668 115.049 o
11 8 11 3.683 -49.236 33.104 112.272 o
12 0 12 5.398 68.500 52.571 44.437 o
12 1 12 283.996 346.095 48.057 51.583 o
12 2 12 242.356 232.190 41.879 67.853 o
12 3 12 1419.820 1463.790 77.565 19.296 o
;
_iucr_refine_instructions_details
;
TITL os_a.res in P2(1)/n
REM Old TITL os_a.res in P2(1)/n
REM SHELXT solution in P2(1)/n
REM R1 0.068, Rweak 0.003, Alpha 0.021, Orientation as input
REM Formula found by SHELXT: C35 Os P2
CELL 0.71073 10.8918 13.7619 17.0714 90 98.563 90
ZERR 4 0.0001 0.0001 0.0002 0 0.001 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H Os P
UNIT 96 176 4 8
RIGU H8 Os
RIGU H7 Os
L.S. 10
PLAN 20
CONF
BOND $H
FMAP 2
MORE -1
ACTA
LIST -3
EXTI 0.000129
SHEL 99 0.7
WGHT 0.0005 0.253084
FVAR 0.255173
REM
REM
REM
P002 4 0.64836 0.59859 0.20080 11.00000 0.01163 0.01058 0.01601 =
0.00060 0.00192 -0.00101
P003 4 0.33818 0.40608 0.26843 11.00000 0.01181 0.01112 0.01491 =
0.00021 0.00306 -0.00065
C004 1 0.37841 0.32778 0.35559 11.00000 0.01517 0.01514 0.01753 =
0.00239 0.00317 -0.00173
C005 1 0.30571 0.31745 0.18632 11.00000 0.02100 0.01634 0.01728 =
-0.00205 0.00388 -0.00333
C006 1 0.76659 0.65205 0.27749 11.00000 0.01591 0.01556 0.02275 =
-0.00078 -0.00184 -0.00000
C007 1 0.61739 0.69827 0.12930 11.00000 0.01619 0.01312 0.01769 =
0.00128 0.00298 -0.00100
C008 1 0.73932 0.51139 0.14854 11.00000 0.01983 0.01445 0.02277 =
-0.00026 0.00679 0.00087
C009 1 0.33192 0.23311 0.35882 11.00000 0.02210 0.01670 0.02076 =
0.00444 0.00359 -0.00184
C00A 1 0.25019 0.36648 0.10853 11.00000 0.03698 0.03248 0.01799 =
0.00148 -0.00230 -0.01103
C00B 1 0.50071 0.70520 0.08316 11.00000 0.02062 0.01948 0.01730 =
0.00283 0.00005 0.00011
C00C 1 0.18089 0.45036 0.28141 11.00000 0.01401 0.01580 0.03178 =
0.00071 0.00638 0.00139
C00D 1 0.82254 0.57581 0.33744 11.00000 0.02737 0.02484 0.03082 =
0.00089 -0.00931 0.00451
C00E 1 0.70657 0.76883 0.11930 11.00000 0.02331 0.01616 0.02642 =
0.00418 0.00428 -0.00497
C00F 1 0.45240 0.36467 0.42293 11.00000 0.02903 0.02445 0.01881 =
0.00283 -0.00203 -0.00791
C00G 1 0.66231 0.47373 0.07233 11.00000 0.03089 0.02407 0.02223 =
-0.00563 0.00963 -0.00095
C00H 1 0.67815 0.84544 0.06641 11.00000 0.03772 0.01567 0.02619 =
0.00487 0.00913 -0.00493
C00I 1 0.71497 0.73711 0.32002 11.00000 0.02595 0.01922 0.02702 =
-0.00740 -0.00219 0.00003
C00J 1 0.56035 0.85269 0.02266 11.00000 0.04448 0.01801 0.01810 =
0.00424 0.00430 0.00201
C00K 1 0.07854 0.37350 0.26791 11.00000 0.01489 0.02122 0.04271 =
0.00043 0.00707 -0.00216
C00L 1 0.35925 0.17718 0.42723 11.00000 0.02665 0.02105 0.02668 =
0.00990 0.00662 0.00143
C00M 1 0.42150 0.25935 0.17563 11.00000 0.03066 0.02262 0.03316 =
-0.00739 0.01487 0.00011
C00N 1 0.18281 0.49646 0.36308 11.00000 0.02570 0.02881 0.04466 =
-0.01209 0.01876 -0.00158
C00O 1 0.47182 0.78187 0.03019 11.00000 0.03266 0.02497 0.01803 =
0.00531 -0.00102 0.00265
C00P 1 0.43237 0.21515 0.49388 11.00000 0.02992 0.03294 0.02282 =
0.01273 0.00373 0.00109
C00Q 1 0.47864 0.30928 0.49169 11.00000 0.03727 0.03625 0.01983 =
0.00768 -0.00525 -0.00704
C00R 1 0.86358 0.55063 0.13037 11.00000 0.02112 0.02622 0.04734 =
-0.00320 0.01546 0.00066
H00i 2 0.79773 0.76675 0.15373 11.00000 0.03589 0.03255 0.08029 =
0.01317 -0.00236 -0.00959
H00n 2 0.74769 0.89909 0.06011 11.00000 0.06001 0.04030 0.06208 =
0.01072 0.00489 -0.02546
H00r 2 0.53887 0.91496 -0.01628 11.00000 0.09775 0.03966 0.04243 =
0.01603 0.00637 0.00769
H00 2 0.37918 0.78605 -0.00416 11.00000 0.02976 0.05053 0.04236 =
0.00146 -0.01354 0.01769
H00d 2 0.43127 0.65240 0.09066 11.00000 0.02246 0.03035 0.04916 =
-0.00457 0.00976 -0.00711
H00j 2 0.49126 0.43603 0.41834 11.00000 0.06600 0.03479 0.03126 =
-0.00094 -0.01791 -0.00855
H2 2 0.53311 0.34048 0.54263 11.00000 0.08020 0.06408 0.04182 =
0.00905 -0.02961 -0.02058
H1 2 0.45340 0.17218 0.54709 11.00000 0.05644 0.06617 0.04520 =
0.04184 0.01254 0.01741
H00v 2 0.32367 0.10368 0.42829 11.00000 0.06068 0.03942 0.06661 =
0.00950 -0.00250 -0.00825
H009 2 0.27384 0.20294 0.30809 11.00000 0.07234 0.05290 0.02571 =
-0.00892 0.00126 -0.02241
H005 2 0.23562 0.26647 0.20341 11.00000 0.02507 0.02063 0.04108 =
-0.01828 0.00877 -0.00140
H006 2 0.84225 0.68066 0.24569 11.00000 0.03971 0.03559 0.03600 =
-0.00449 0.00852 0.01535
H008 2 0.75895 0.45132 0.19119 11.00000 0.05074 0.01672 0.03563 =
0.01224 0.02130 0.01478
H00a 2 0.16782 0.40727 0.11523 11.00000 0.05295 0.07338 0.04762 =
-0.00379 0.00618 0.00673
H00b 2 0.31844 0.41378 0.08681 11.00000 0.07217 0.07202 0.04018 =
0.02342 0.00331 -0.03288
H00c 2 0.22473 0.30946 0.06344 11.00000 0.09929 0.08311 0.02574 =
-0.02693 -0.00407 -0.02912
H00e 2 0.16136 0.50718 0.23688 11.00000 0.02551 0.03151 0.04930 =
0.01516 0.00278 -0.00375
H00f 2 0.75248 0.55168 0.37162 11.00000 0.04221 0.07845 0.06774 =
0.04226 0.00626 -0.01623
H00g 2 0.85569 0.51294 0.30954 11.00000 0.07452 0.03289 0.08503 =
-0.01743 -0.01215 0.01812
H00h 2 0.89932 0.60724 0.37762 11.00000 0.03537 0.06405 0.04632 =
0.00220 -0.02620 -0.00535
H00k 2 0.57674 0.44014 0.08275 11.00000 0.06103 0.05885 0.04901 =
-0.01031 0.00895 -0.03644
H00l 2 0.63896 0.53239 0.03043 11.00000 0.07111 0.03987 0.03817 =
0.00261 0.00058 -0.00025
H00m 2 0.71761 0.41904 0.04578 11.00000 0.06423 0.04172 0.05125 =
-0.01459 0.02340 0.01198
H00o 2 0.66979 0.79271 0.27948 11.00000 0.05923 0.01511 0.03939 =
-0.00309 -0.00617 0.01410
H00p 2 0.64759 0.71390 0.35624 11.00000 0.04779 0.05780 0.06670 =
-0.02265 0.03690 -0.00904
H00q 2 0.78952 0.77061 0.36052 11.00000 0.05338 0.04349 0.05289 =
-0.02008 -0.00559 -0.01289
H00s 2 0.06152 0.34803 0.20737 11.00000 0.03464 0.08107 0.05832 =
-0.01876 0.00047 -0.00761
H00t 2 0.10127 0.31255 0.30454 11.00000 0.04752 0.03332 0.07609 =
0.00193 0.00758 -0.01800
H00u 2 -0.00872 0.40359 0.28133 11.00000 0.02644 0.05101 0.10380 =
-0.00891 0.01464 -0.00645
H00w 2 0.49191 0.30537 0.16183 11.00000 0.05746 0.04689 0.09163 =
-0.00185 0.04757 -0.00140
H00x 2 0.45863 0.22090 0.22965 11.00000 0.06698 0.06514 0.03880 =
0.01632 0.00731 0.04291
H00y 2 0.39783 0.20685 0.12701 11.00000 0.07930 0.04705 0.05446 =
-0.03936 0.03082 -0.02406
H00z 2 0.19834 0.44123 0.40951 11.00000 0.08516 0.06553 0.04638 =
0.01413 0.02068 0.00833
H 2 0.25432 0.55135 0.37549 11.00000 0.04806 0.07006 0.04453 =
-0.02359 0.02705 -0.01769
Ha 2 0.09147 0.53010 0.36392 11.00000 0.05463 0.05896 0.08795 =
-0.00091 0.05081 0.01860
H3 2 0.84955 0.61371 0.08990 11.00000 0.05202 0.03692 0.08651 =
0.02242 0.04760 0.01146
Hb 2 0.92571 0.57185 0.18226 11.00000 0.01695 0.07617 0.05742 =
-0.02921 0.01779 -0.01307
Hc 2 0.91233 0.49520 0.10207 11.00000 0.04460 0.04828 0.08060 =
-0.01760 0.03206 0.00961
Os 3 0.47833 0.53002 0.24900 11.00000 0.01480 0.01244 0.01854 =
0.00025 0.00507 -0.00294
H5 2 0.39279 0.57580 0.30674 11.00000 0.09080 0.09846 0.11832 =
-0.03507 0.07548 -0.00982
H9 2 0.55030 0.52990 0.33195 11.00000 0.03284 0.10862 0.08632 =
0.00556 -0.00464 -0.03452
H4 2 0.48570 0.64346 0.26493 11.00000 0.03079
H7 2 0.46005 0.48236 0.16732 11.00000 0.07007 0.03727 0.04028 =
-0.01121 0.01933 -0.04286
H8 2 0.56855 0.44207 0.26060 11.00000 0.04507 0.03847 0.08385 =
0.03047 0.03809 0.01218
H6 2 0.37089 0.57818 0.19047 11.00000 0.03391 0.04991 0.07124 =
0.02548 0.01415 0.00388
HKLF 4
END
Q2 1 0.475 0.66 0.23438 11 0.05 0.43
Q3 1 0.525 0.38 0.26563 11 0.05 0.36
Q10 1 0.425 0.42 0.23438 11 0.05 0.28
Q4 1 0.4 0.5 0.1875 11 0.05 0.31
Q7 1 0.675 0.74 0.26563 11 0.05 0.29
Q5 1 0.55 0.92 -0.0625 11 0.05 0.31
Q9 1 0.475 0.76 0.265625 11 0.05 0.29
Q1 1 0.525 0.5 0.25 11 0.05 0.5
Q11 1 0.525 0.32 0.4375 11 0.05 0.28
Q12 1 0.7 0.44 0.359375 11 0.05 0.28
Q8 1 0.35 0.18 0.390625 11 0.05 0.29
Q6 1 0.575 0.8 -0.046875 11 0.05 0.3
REM The information below was added by Olex2.
REM
REM R1 = 0.0119 for 7199 Fo > 4sig(Fo) and 0.0143 for all 7723 data
REM 636 parameters refined using 6 restraints
REM Highest difference peak 0.5047, deepest hole -0.5003
REM Mean Shift 0.0000, Max Shift 0.0003.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0143
REM R1_gt = 0.0119
REM wR_ref = 0.0189
REM GOOF = 1.0722
REM Shift_max = 0.0003
REM Shift_mean = 0.0000
REM Reflections_all = 7723
REM Reflections_gt = 7199
REM Parameters = 636
REM Hole = -0.5003
REM Peak = 0.5047
REM Flack = n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_restr_RIGU_atom_site_label_1
_restr_RIGU_atom_site_label_2
_restr_RIGU_target_weight_param
_restr_RIGU_U13_diff
_restr_RIGU_U23_diff
_restr_RIGU_U33_diff
Os H7 0.004000 -0.001104 0.008843 -0.013484
Os H8 0.004000 -0.002098 0.001392 -0.012715